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Silicone/SiO2 organic-inorganic hybrid sol have been prepared from tetraethyl orthosilicate as inorganic precursor, methyl triethoxysilane and diphenyl dimethoxy silane as organic precursor, the hydrochloric acid and water as catalysts, by sol-gel method through the hydrolysis-polycondensation reaction.

采用溶胶-凝胶法,以正硅酸乙酯为无机相前驱体,甲基三乙氧基硅烷和二甲基二甲氧基硅烷为有机相前驱体,盐酸和水为催化剂,通过水解-缩聚反应制备了有机硅/SiO2有机-无机杂化溶胶

It was found that sol-gel transition may occur to electrostatically stabilized silicon carbide suspensions when their pH values are shifted from alkaline region to neutral.

发现静电稳定的碳化硅浆料在碳化硅粉体表面的无定形氧化硅层的影响下,可以象氧化硅溶胶一样发生溶胶-凝胶转变,并将这一发现用于碳化硅陶瓷的成型。

The characteristics of the AP include (1) in addition to the formation of hydrogel in aqueous alkaline or polar organic solution, AP can form carbonaceous hydrogel in neutral and acidic aqueous solutions, which extents the application of carbonaceous sol-gel;(2) AP contains a large amount of nitric groups which decomposes quickly by thermal initiation, releasing a large amount of gases and heat, indicating explosive properties of the AP;(3) metal salt-containing AP is also explosible by thermal initiation, and the metal in AP promotes the explosion.

以沥青为碳源,用氧化法制备水性沥青过程中,浓硫酸和浓硝酸的比例、用量、氧化温度及氧化时间对水性沥青的收率皆有影响。经过氧化后,沥青上含有许多含氧官能团,导致水性沥青溶于水。含氧官能团越多,水性沥青越易溶于水。调节制备条件,可使水性沥青不仅可以在碱性水溶液中形成凝胶,而且可以在中性和酸性水溶液中形成溶胶、凝胶,从而拓宽了炭基溶胶—凝胶法制备炭基纳米材料的应用范围。

The results showed that fumaric acid is most favorable to prepare MnO2 sol.

结果表明,富马酸是制备MnO2溶胶比较合适的还原剂,Span80和Tween80复配乳化剂的效果最好,在油∶溶胶=4∶1,乳状液∶三乙胺=8∶3的条件下制得的纳米MnO2微粒,其形貌为规整的球体,粒径均匀,几乎为单分散性。

Ni-P-mCMC/mCS bipolar membrane was prepared from carboxymethyl cellulose modified with phosphorylated agent as a cation exchange layer and chitosan modified with glutaraldehyde as an anion exchange layer. The electrolysis cell was constituted by Ni-P-mCMC/mCS BPM as a septum for electrogenerating furfural alcohol and furoic acid.

以磷酸化试剂改性羧甲基纤维素钠制备了阳膜层,以戊二醛改性壳聚糖制备了阴膜层溶胶,将阴膜层溶胶流延于阳膜层上,制备了P-mCMC/mCS双极膜,而后以化学镀方法在阳膜层表面镀镍,制备了Ni-P-mCMC/mCS双极膜,并应用于成对电合成糠醇、糠酸。

Metal/ oxide composite aerogels can be used as catalysts because of their high specific surface area. In this paper, Co-rich Co/SiO2 composite aerogels in which mass fraction of Co can reach 66%were firstly prepared by sol - gel process of Co-containing tetraethyl orthosilicate. The influence of H2O, catalyst, solvent and composition of Co-containing tetraethyl orthosilicate on the sol-gel process are discussed.

本工作首次采用含钴硅酸乙酯进行溶胶~凝胶反应来制备高钴含量的纳米级Co/SiO2复合气凝胶,制备的Co/SiO2复合气凝胶中n:n的比例最高可达2:1,且复合气凝胶中的Co含量可在小于66%的范围内任意调节,并系统研究了水量、催化剂浓度、溶剂量及含钴硅酸乙酯的组成对溶胶-凝胶过程的影响。

The invention relates to a fabric nanometer following cleaning agent for obtaining TiO2/ZnO composite hydrosol, and relative production and cleaning method, wherein it uses butyl titanate and zinc acetate as predecessor, uses glacial acetic acid as catalyst and peptizer, uses water as solvent, uses absolute ethyl alcohol as the solvent of butyl titanate, and uses ethanolamine as deposit agent and supplies OH-, to be hydrolysed and polycondensated to form TiO2/ZnO composite hydrosol. And its components and mass percents are: butyl titanate at 1-15%; zinc diethyl at 1-12%; absolute ethyl alcohol at 1-20%; glacial acetic acid at 5-15%; and aminoethyl alcohol at 0.1-5%, and the left is water. The invention has lower cost and simple process.

本发明涉及一种可以得到TiO 2 /ZnO复合水溶胶的纺织品纳米后整理试剂及其制备工艺及对织物的整理方法,以钛酸丁酯和乙酸锌为前驱物,冰乙酸为催化剂和胶溶剂,水为溶剂,无水乙醇为钛酸丁酯的溶剂,乙醇胺为沉淀剂并提供OH -,经过水解、缩聚反应形成的TiO 2 /ZnO纳米溶胶整理剂,其组分和重量百分比含量如下:钛酸丁酯占1~15%;二水乙酸锌占1~12%;无水乙醇占1%~20%;冰乙酸占5%~15%;乙醇胺占0.1%~5%;水余量,具有耐洗性、无毒、无刺激、成本低廉、制作工艺简单可靠的优点,可实现对对织物的抗紫外、抗菌、抗静电功能整理。

Stable and transparent boric silicate、Er~(3+)-doped phosphosilicate, Er~(3+)-doped aluminasilicate glass sol was prepared by the sol-gel route.

实验中采用溶胶-凝胶工艺制备了透明、稳定的硼酸盐、掺铒的磷硅酸盐、掺铒的铝硅酸盐溶胶

The effects of the sol viscosity,mass ratio of buty1 titanate to active carbon, TiO 2 content of the sol and heat-treatment temperature on the photoactivity of TiO 2/AC composites were studied.

研究了TiO 2溶胶黏度、钛酸丁酯与活性炭的质量比、溶胶中TiO 2的量及热处理温度对TiO 2/ AC 复合体光催化活性的影响。

The sol gel materials are prepared through the hydrolysis and polycondensation of tetramethoxy silicane.

溶胶 凝胶技术是将金属醇盐等原料配制成均质溶液,在饱和条件下经水解缩聚等化学反应,生成物聚集成溶胶,再经蒸发、干燥转变为凝胶,这是一项在低温下制备纳米粉末或多孔玻璃的技术[1] 。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。