溶胶

SiO 2/TiO 2 superhydrophilic coating on glazed tile substrate was prepared by solgel method,the surface chemical composition, contact angle of water and photographs of surface of the coating were studied by use of XPS,photomicroscopy and SEM.

用溶胶 -凝胶方法在釉面砖上制备了SiO2 /TiO2 超亲水涂层，用XPS、光学显微镜和SEM研究了涂层的表面化学组成、水润湿角和表面形貌。

Piezoelectrically driven micropump using PbO3 film has been successfully fabricated by Sol-Gel techniques.

摘 要：采用溶胶-凝胶法制备技术制作了PbO3压电薄膜，并以PZT薄膜为驱动制作了微泵。

Piezoelectrically driven micropump using PbO3 film has been successfully fabricated by Sol-Gel techniques.

采用溶胶-凝胶法制备技术制作了PbO3压电薄膜，并以PZT薄膜为驱动制作了微泵。

Ti-PILCs were also obtained with pillaring agent prepared from Ti(n-C4H9O)4 and HC1 by Sol-Gel, using purified Na-montmorillonite in Hubei as the starting clay.

以鄂东钙基膨润土经提纯钠化后所得的精制钠基蒙脱石d_(001=1.28nm为基质粘土，以钛酸正丁酯[Ti(n-C_4H_9O)_4]为钛源，采用溶胶—凝胶法制备了一系列钛交联蒙脱石纳米复合材料；并对Ti／土比、H／Ti摩尔比和盐酸浓度等主要合成条件进行了讨论。

Two times hydrolyzation of Fe~(3+) and Cr~(3+) was firstly pointed out in the process of pillar preparation with hydrothermal method. In order to improve the thermal stability, Fe/Cr-Si-pillaring agent solution was synthesized by hydrolyzing Fe~(3+) and Cr~(3+) solution on the surface of silica sol, and Fe/Cr-Si-pillared montmorillonite (Fe/Cr-Si-PILM) was prepared with conventional method and hydrothermal method. Because the technical innovation of preparation is the best way to improve the PILM properties, two novel methods (Microwave method and Ultrasonication method) have been studied to synthesize Fe/Cr-PILM.In order to expand PILMs new application in the field of coal conversion, catalytic activity of Fe/Cr-Si-PILM catalyst in LongKou lignite and ShenHua coal residue liquefaction was discussed and characterized in the last part of this paper.

研究证明：蒙脱石的预处理是可行的，我们以预处理后的Ca-M为原料，研究并优化了PILM的水热法制备工艺，提出了金属离子的二次水解法；为了提高PILM的热稳定性，我们自制了硅溶胶，合成了Fe／Cr-Si三元复合柱化剂，并制备了Fe／Cr-Si-PILM；在PILM合成中，制备技术的革新是改进PILM性能的重要方法，为此我们探索了微波合成法和超声波合成法在制备Fe／Cr-PILM中的应用；最后，我们选择龙口褐煤和神华煤液化残渣为研究对象，探索了Fe／Cr-Si-PILM催化剂在煤炭液化中的应用，希望能开拓PILM应用的新领域。

The in-situ epoxidation and in-situ grafting of unstaturated rubber,in-situ synthetic poly-unstaturated carboxylate,surface in-situ chemical treating of rubber filler,montmorillonite in-situ plugging plyer/peeling,in-situ preparing SiO2 by sol-gel technology were presented.The modification method and effect of rubber were addressed,and the practic application possibility of modificated rubber to rubber goods was researched.

介绍了不饱和橡胶的原位环氧化和原位接枝、原位合成聚不饱和羧酸盐、橡胶填充剂表面原位化学处理、蒙脱土原位插层/剥离、溶胶-凝胶法原位生成SiO2等原位反应合成技术在橡胶加工和改性方面的应用研究工作，讨论了各种改性橡胶方法的特点以及改性效果，并探讨了改性橡胶材料在各种橡胶制品行业实际应用的可能性。

The significance and application of reinforcement of conventional polymers by POSS are reviewed.

综述了多面体低聚倍半硅氧烷改性传统聚合物的作用及其应用；介绍了POSS的纳米级笼形结构、良好的热力学和化学稳定性及耐热、阻燃等以及溶胶-凝胶法合成POSS的优缺点。

The gelatin-siloxane nano-particles are prepared from gelatin and 3-(2,3-epoxy propoxy )propyltrimethoxysilicane by performing chemical combination and hydrolytic reaction in acidic condition to obtain sol; and adjusting the pH value to slightly alkaline for performing polymerization reaction of silicane.

将明胶和3-(2，3-环氧丙氧)丙基三甲氧基硅烷在酸性条件进行化合、水解反应；将该溶胶的pH值调节至弱碱性，使硅烷发生聚合反应，即可得明胶-硅氧烷纳米颗粒。

The preparation of three different shapes a-Fe2O3 nano-particles by means of force hydrolyzation was discussed in this paper. By controlling the experimental conditions (Fe3+ concentration, acidity, reaction time, reaction temperature etc.), the particles with different shapes (ellipsoidal, pseudocubic, sphere) were obtained.

本论文采用强迫水解法制备了三种不同形貌的α-Fe_2O_3水溶胶，通过对反应条件Fe~(3+浓度、酸度、反应温度、反应时间等的控制获得了不同形貌(椭球形、球形、准立方体形)和粒径的α-Fe_2O_3，并利用浸渍—提拉法制备了α-Fe_2O_3纳米粒子薄膜。

The results show that Zn7Sb2O12 and ZnCr2O4 phases can be formed at a lower annealing temperature (550℃) by the solution doping, and the pyrochlore phase is not detected by XRD from 550℃ to 950℃.

结果表明，采用溶胶掺杂在550℃退火条件下可形成Zn7Sb2O12及ZnCr2O4相，且在退火温度范围内(550~950℃)基本上没有焦绿石相形成。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。