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The properties of C_(60) colloid and nanoparticles were characterized by UV-vis spectra and TEM.

结果表明在相同油水配比条件下,改变超声波输出功率可以调节[60]富勒烯水溶胶的浓度,并控制[60]富勒烯纳米粒子的直径。

Optimization of polyester condensation process and reactor design;2. The Structure Characters of the Sulfonated Condensation Polymer Series High Performance;3. The pH value of the solution was adjusted,and the co- condensation reaction was taken place between the hydroxy groups forming transparent organic-inorganic hybrid films on polycarbonate.

以甲基丙烯酰氧基丙基三甲氧基硅烷(KH-570)水解聚合产物作为主要成膜物质,引入正硅酸乙酯水解产物硅溶胶作为无机增强物,调节两种混合溶液pH值,利用两者羟基之间的共缩聚反应在聚碳酸酯板表面制备有机/无机复合透明耐磨薄膜;采用TG/DTA、FT-IR、SEM及UV-V IS对成膜过程、薄膜性能与结构进行表征。

Cordierite ceramics with low dielectric constant and loss were developed.

溶胶-凝胶法制备了低介低烧堇青石陶瓷材料。

The results indicated that hydrogen bond and covalence bond were formed between PVA and TEOS through the sol-gel reaction.

结果表明PVA与无机相发生溶胶-凝胶反应生成氢键和共价键Si-O-Si,形成交联有机聚合物/无机杂化体系,使杂化膜的结晶度减少,控制了膜的溶胀,提高膜的溶解选择性能,但膜的溶胀减少会使通量有所下降。

In this paper aerogels were obtained through sol-gel process of resorcinol, m-cresol and cresol mixture and substantially supercritical fluid drying.

本文以间苯二酚、间甲酚、混合甲酚为原料,与甲醛在碱性条件下经溶胶—凝胶过程、超临界干燥得到气凝胶。

In the aspects of research method, we took the method of preparing sol at first and then impregnating the wood to obtain ceramic-wood composite; this method made the wood use efficiently and increased the wood's weight gain percent. The ceramic-wood composite with performances of well decay resistance, dimensional stability, effloresce resistance and high strength was obtained by importing the cymene to the net of gel as the result of co-hydroxylation between MTES and TEOS. Making use of XPS ,we found that the apex of Si2p、O1s、C1s had evident chemical shift , which validated the existence of Si-O-C bonding.Key Words: Sol-gel, Ceramic-wood composite, Modified sol, Ecomaterials

在工艺方法上,采用先制备溶胶,然后浸注木材的工艺方法具有原料利用率高、提高增重率的优点;采用甲基三乙氧基硅烷和正硅酸乙酯共水解的方法,将甲基引入陶瓷化复合木材的凝胶内部,所制备的材料具有尺寸稳定性好、具有耐风化和耐腐朽性,强度高的特点;首次利用X射线光电子能谱,发现了Si2p、O1s和C1s谱峰发生了明显的化学位移,证实了Si-O-C键合作用的存在。

Single Al-Ni-Co decagonal quasicrystal particles were prepared by the combination use of conventional casting and ball milling. The coated Al-Ni-Co quasicrystalline particles were prepared by sol-gel processing.

采用常规铸造法和球磨法制备得到单相Al-Ni-Co十次准晶颗粒,并采用溶胶-凝胶法在准晶颗粒表面成功的添加了涂层。

The optical property of CdS nanocrystals in ZrO 2 thin film has been studied. The film was fabricated by sol gel technique. Photoluminescence and photoluminescence excitation spectra of the samples with different annealing temperature were measured. Photoluminescence decay curve of CdS nanocrystals at different annealing temperatures was studied.

研究了用溶胶凝胶方法制备的CdS超微粒/ZrO2薄膜的发光特性,测量了不同退火温度处理的样品的荧光光谱、荧光激发光谱和荧光衰减曲线的变化,通过荧光衰减曲线研究了140 ps左右的CdS的带间跃迁发射和较慢的表面态发射。

The composite film appeared semitransparent and brown to yellow from optical microscopy. Results show that shorter time sol-heating results in thiner film with less surface roughness, less conglutination to base, and easily to disconnect, while longer time sol-heating results in thicker film with better conglutination to base and worse roughness. RDX distributes in the film everywhere on the whole but discretely on the scale of 2.4 μm according to EDS results. XRD curve of RDX/RF film shows the superposition of RF non-crystal bread curve and RDX crystals diffraction curve. RDX diffraction peaks are broadened and its crystal size is calculated to be lower to 43 nm.

实验所得薄膜半透明,呈棕红色至黄色;实验表明,溶胶恒温加热时间较短时,所得薄膜的单层厚度较小,较平整,但附着力小,干燥后易脱落;恒温加热时间较长时,所得薄膜的单层厚度较大,不易脱落,但表面平整性较差;能谱测试表明,薄膜中的RDX整体上分布较为均匀,但在测试点位间距为2.4μm的微观尺度上呈离散状分布;XRD测试表明,RDX/RF复合物薄膜表现为RF的非晶态馒头峰与RDX衍射峰的叠加,RDX衍射峰明显宽化,其晶粒度可低至43 nm。

The rheological characteristics of sol solution have been studied. It turns out that the relation of viscosity with temperature can be expressed by the relation μ=μ〓exp , and that the solution's rheological characteristics during the sol—gel transiton are as follows: at first the dilatant fluid changes to Newton fluid, then to pseudoplastic, and finally to gel.

本文对溶胶溶液流变特性进行了研究,结果表明:温度对粘度的影响可用Arrhenius方程来表示;随放置时间的增加,溶液由膨胀型流体向牛顿型流体转变,再向假塑性流体转变,最后成为凝胶。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。