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Result: The nm-HAP-sol present the dispersed and uniformity needle. A431cells inhibition ratio was maximizing at the 5 day in the 400mg/L nm-HAP-sol group, the 200mg/L nm-HAP-sol group and the 100mg/L nm-HAP-sol group, inhibition ratio of the 400mg/L nm-HAP-sol group, the positive control group and the 50mg/L nm-HAP-sol group was respectively (77.89±6.29)%,(77.46±8.26)% and (1.23±0.15)%. It was detected that the number of A431 cells were persistently increasing in the 50mg/L nm-HAP-sol groups while decreasing in the 400mg/L nm-HAP-sol group, the positive control group and abidingly increasing for 4 and 3 days then decreasing in the 100mg/L and 200mg/L nm-HAP-sol group by inverted microscope.

结果:超声乳化法配制的HAP纳米溶胶呈均匀分散的针状;400mg/L、200mg/L和100mg/L溶胶组对A431细胞抑制率在第5天达到各组最大值,此时400mg/L溶胶组与阳性对照组的抑制率分别为(77.89±6.29)%和(77.46±8.26)%, 50mg/L溶胶组抑制率为(1.23±0.15)%;倒置显微镜下见50mg/L溶胶组细胞数目持续增加,聚集成簇,细胞呈现多角形或梭形,胞浆透亮,而100mg/L 和200mg/L溶胶组的细胞数目分别增加至第4天和第3天开始下降,400mg/L溶胶组和阳性对照组细胞数目持续减少,细胞体积缩小,漂浮细胞增多。

M^(-2). The polarization curves show that the corrosion current density of sol sealed film is about 2 orders of magnitude lower than that of the film sealed by sodium bichromate, the reason is that sol particles can not only seal pores of anodized film, but also form sot-gel coating on anodized film.

m^(-2)。极化曲线显示溶胶封闭膜的腐蚀电流密度比重铬酸盐封闭膜的降低2个数量级,其原因是溶胶不仅封闭了氧化膜的孔隙,而且在氧化膜的表面形成溶胶凝胶涂层。

The polarization curves show that the corrosion current density of sol sealed film is about 2 orders of magnitude lower than that of the film sealed by sodium bichromate, the reason is that sol particles can not only seal pores of anodized film, but also form sol-gel coating on anodized film.

极化曲线显示溶胶封闭膜的腐蚀电流密度比重铬酸盐封闭膜的降低2个数量级,其原因是溶胶不仅封闭了氧化膜的孔隙,而且在氧化膜的表面形成溶胶凝胶涂层。

It was shown that the photocatalytic activity of TiO_2 catalysts that were prepared by sol-hydrothermal method was better than that prepared by sol-gel method from the comparison investigations of sol-hydrothermal and sol-gel methods, which result in the better dispersiveness of the former.

通过对溶胶-水热法和溶胶-凝胶法的比较研究,发现溶胶-水热法的制备样品的活性要高于溶胶-凝胶法,分析认为主要与前者的分散性较好有关。

Polyringlpyrrolidoneas a viscosity increaser is used to adjust the viscosity of the sols.When the molar ratio of PVP:Al(OC_3H_7)is up to 1:1,the viscosity of the PVP assisted sol increases from 2.3 to 31.5 mPa·s,and homogeneous,uniform and crack-free 1 mol%Er~(3+)-10 mol%Yb~(3+)codoped Al_2O_3 thin films with the thickness of 1.6μm are formed by 10 dipping and drying cycles sintered at 1000℃.

以聚乙烯吡咯烷酮为增粘剂,调节DCPA改性溶胶的粘度,PVP(K-90):Al_3的摩尔比为1:1时,溶胶粘度由原始溶胶的2.3增加到含PVP溶胶的31.5mPa·s,仅经过10次循环提拉、干燥,1000℃烧结,制备出表面均匀完整,无开裂厚度约为1.6μm的1 mol%Er~(3+)-10 mol%Yb~(3+)共掺杂Al_2O_3薄膜。

The A13 sol and Al(0H)3—Zr4 sol is prepared by peptization method with A1(NO3)3 , ZrOCl2 and NH3H2O as starting materials, using A1(NO3)3 solution and Zr4 sol as peptizing agents, and the preparation process, preparation conditions and colloid structure are analyzed.

本文以Al(NO_3)_3,ZrOCl_2和氨水为原料,分别以Al(NO_3)_3溶液和Zr_4溶胶作为胶溶剂,通过胶溶法制备Al_3溶胶和Al_3—Zr_4溶胶,并对两种溶胶的制备过程,制备条件和胶团结构进行了分析。

The technological process in preparation of the delafossite structure p-TCO thin films by sol-gel method is discussed systematically. The relative advantages and disadvantages of the systems of sol about organic alkoxide and inorganic salt are analyzed, and further development are discussed. It is pointed out that sol-gel method is an effective and feasible means to prepare p-TCO thin films.

本文介绍了铜铁矿结构p-TCO的结构特性以及溶胶凝胶法的基本原理和特点;系统地介绍了溶胶凝胶法制备铜铁矿结构p-TCO薄膜的工艺;分析比较了有机醇盐、无机盐溶胶体系的优缺点;最后讨论了进一步的发展方向,指出溶胶凝胶法是一种高效可行的制备p-TCO薄膜的方法。

The effects of concentration, time on the reaction was measured by UV-visible absorption spectra , the morphology of the silver nanoparticles was characterized by transmission electron microscopy; The structure of Sesbania Gum and silver colloid was measured by Fourier transform infrared spectroscopy .

通过紫外-可见吸收光谱研究了反应物浓度、反应时间对反应的影响;通过透射电子显微镜对银纳米粒子形貌进行表征;利用傅立叶变换红外光谱仪对田(来源:A116161BC论文网www.abclunwen.com)菁胶和反应所得到的银溶胶的结构进行表征;对溶胶的拉曼光谱进行检测,结果显示溶胶具有很好的Raman信号,室温下得到的溶胶表现出银纳米粒子对田菁胶的Raman信号增强作用。

METHODS: Acetic acid solution was added into chitosan to prepare 8% chitosan acetic acid hydrosol, which was then stayed for one day. Flowing the immersion into the hydrosol and immediate dislodgement, plastic tube was soaked in 1 mol/L sodium hydroxide for 3 minutes. Hydrosol out of the tube etiolated and coagulated into jells, the tube was removed when the jells were semi-dried.

利用乙酸溶液制备8%壳聚糖乙酸水溶胶溶胶放置1 d,将硬塑料管浸入溶胶后迅速取出放入1 mol/L氢氧化钠液内3 min,见管外溶胶变白凝固成胶冻状,取出后晾到五分干后轻轻退下内管,晾干后即成为壳聚糖导管。

The methods of preparing stable boehmite sol and zirconium hydroxide sol by anionic exchange method using inorganic compounds as raw materials were investigated in this dissertation,and forming-membrane capability of the sols were also investigated on the base of the it.

本论文主要研究了以无机盐为原料,采用离子交换溶胶-凝胶法制备稳定勃姆石溶胶和氢氧化锆溶胶的方法,并在此基础上对溶胶的成膜性进行研究。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。