溶剂分解

Silver behenate nanocrystals with a diameter of 50~100nm, were first prepared by chemical precipitation in a water tert-butyl alcohol mixed solvent.

本文详细考察了影响山嵛酸银晶体生长的因素，研究了山嵛酸银晶体的形成机理，首次通过化学沉淀法在水-醇混合溶剂中制备出粒径为50~100nm的山嵛酸银晶体，进一步研究了山嵛酸银的热行为以及热分解机理，考察了山嵛酸银纳米晶体在热敏成像体系及制备银薄膜方面的应用。

In order to avoid such defects,a new process for the preparation of dicarboxylic acids has been studied.In this experiment,the effects of solvent, ozonolysis temperature, catalyst, oxidation decomposition temperature etc.

实验中考察了溶剂、臭氧化温度、催化剂、氧化分解温度、反应时间等因素对反应的影响，确定了最佳工艺条件，为工业化生产提供了可供参考的工艺参数。

In this paper, initiator is dissolved in 1-bromopropane which is solvent. Then the propene and hydrogen bromide that can be dissolved in 1-bromopropane are inlet in l-bromopropane when initiator is decomposing. The reaction occurs in fluid phase and high-purity 1-bromopropane is synthesized by one step method. In this paper, the material HBr is synthesized with NaBr and sulfuric acid at the presence of hydrobromic acid.

本论文以1-溴丙烷为溶剂，将引发剂溶于其中，加热到引发剂开始分解时再通入丙烯和HBr，使二者溶解于1-溴丙烷中，在液相中进行反应，实现丙烯&一步法&合成高纯1-溴丙烷利用NaBr与硫酸在氢溴酸存在下反应制备HBr气体，以作为合成1-溴丙烷的原料。

AC impedance for anode result shows that the SEI film is incrassated and compacted,and the impedance is increased from 183.1 to 310Ω.

储存后电解液中LiPF_6发生了一定程度的分解，溶剂被氧化生成小分子物质。

Products have good thermal stability anddecomposition temperature above 200℃; Selected lauryl amine as a case, then optimizedthe synthesis conditions by orthometric trial, and obtained the best synthesis technichs: themolar ratio of 1: 2.1, the reaction temperature was controlled at 80℃and the reaction timeof 16 h, reaction to the solvent n-propanol.

并对其热稳定性进行了分析，合成产物具有较好的热稳定性，分解温度都在200℃以上；以十二胺为例，用正交实验法优化合成条件，获得最佳合成工艺为：摩尔配比为1：2.1，反应温度控制在80℃，反应时间为16h，反应所用的溶剂为正丙醇。

The content of scutellarin was offline analyzed by HPLC.

实验结果表明，所建立的方法可以防止被测物的分解，减少萃取时间和溶剂的消耗。

The grafting effect and mechanism was charac- terized by FTIR,The heat stability of unvulcanized and dynamical mechanical proper- ty of vulc- lcanizates of SBR and SBR-g- were tested by TG and DMA respectively. medium-resistance properties of SBR and SBR-g- vulcan- izates were also investigated.The results showed that addition of St accelerated GMA grafting onto SBR and control the decomposition of SBR. When the conditions were GMA/St/DCP was 8/4/0.3 and grafting temperature was 160℃.

结果表明，St对提高接枝率、抑制SBR的降解起到了积极的作用；SBR中聚丁二烯的α－H和双键共同参与了GMA/St熔融接枝反应；当SBR/GMA/St/DCP=100/8/4/0.3、接枝温度为160℃时，SBR的接枝率较高（23.78%），SBR–g–硫化胶的拉伸强度和撕裂强度比SBR硫化胶的分别提高了119%和27.4%；SBR–（GMA--co-St）未硫化胶的Tg比SBR未硫化胶的高，而耐热分解性能优于SBR未硫化胶；SBR–g–硫化胶在低温条件下的刚性增大、弹性降低、具有较低的内耗，在常温下的阻尼性能较高，但弹性性能保持较好；SBR–g–硫化胶的耐热稳定性以及耐非极性有机溶剂的性能优于SBR硫化胶。

The combined discrete-continuum model overcomes the lack and annihilates the error in continuum methods. In addition, the computation of the short-range solute-solvent interaction also causes errors. Therefore a high-level quantum calculation is necessary.IV(4) This model can also provide insight into many fundamental details where cluster model and continuum model fail to provide unique pictures.

4，离散一连续组合模型的价值还在于其把溶剂效应分解为短程作用和长程作用，对于一些分子簇模型以及传统连续介质模型不能解释的现象给出更清晰的图像。

Carboxymethyl cellulose was used for pulping agent and water was used for dissolvent in this process. The organic pulp on the surface of the ZnO nanotapers film was decomposed fully, and the ZnO nanotapers were neither curving nor conglobating at high temperature. Moreover, this method had the advantages of low fabrication cost and simple process.

该工艺以羧甲基纤维素为制浆剂，以水为溶剂，所制备的ZnO纳米锥薄膜表面上的有机浆料已基本分解，ZnO纳米锥在高温下既不会弯曲也不会团聚，且成本低，工艺简单。

It can't solve in organic solvents and decomposes before melting.

它在有机溶剂中不溶解，分解温度以下不熔融。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了