溶剂

The third part studied the influence of polar modifier and column temperature on enantioseparation of benzoin on Chiralcel OD-RH primarily.

第三章研究了极性有机溶剂及温度对安息香在Chiralcel OD-RH柱上拆分的影响。

The influence of polar modifier and column temperature on enantioseparation of benzoin on Chiralcel OD-RH systematically was also studied in the thesis.

另外，安息香对映体在Chiralcel OD-RH柱上的色谱拆分保留机理，特别是极性有机溶剂及柱温度对安息香拆分的影响也是本论文的研究内容。

Benzoin condensation reaction of benzaldehyde using simple imidazolium based ionic liquids as catalyst has been successfully achieved. The reaction factors such as solvent, base and ionic liquids have been studied in detail.

成功地实现了简单咪唑基离子液体对苯甲醛自缩合成苯偶姻的催化反应，以及详细探讨了溶剂、碱、离子液体种类及用量等各种影响因素。

Cu complex of the surfactant have water soluble ability and surface activity, can catalyze the air oxidation of benzyl alcohol or Benzoin not only in DMF solution but also in alkali water solution.

表面活性剂铜配合物具有较好的水溶性和表面活性，不但在DMF溶剂中有效催化苯甲醇、安息香的空气氧化反应，而且在稀碱溶液中形成的金属胶束也可催化氧化苯甲醇。

It is prepared from pentachluorobenzonitrile by using KF as fluoride to substitute chlorine in the presence of benzonitrile under high temperature. But owing to the low solubility of KF and rigor synthesis condition, and the parallel auxiliary reactions, the speed of reaction as well as the yield is very low.

五氟苯甲腈的合成开发以五氯苯甲腈为原料在较高的温度下用氟化钾做氟化剂，通过取代苯环上氯原子而得到的，由于氟化钾在溶剂中溶解度低，合成条件要求苛刻，反应速度较慢，同时存在有平行竞争副反应，因而反应收率较低，国内尚无厂家生产。

Benzonitrile was selectively hydrogenated into benzylamine under mild conditions over activated amorphous nickel aluminium alloy catalyst which was prepared by rapidly quenching method.

由铜鼓快速淬冷法制备的非晶态NiAl合金催化剂经活化后用于催化苯甲腈加氢制苄胺的反应，考察了溶剂种类、苯甲腈初始浓度、催化剂用量、反应温度及反应压力等因素的影响，并测定了该催化加氢反应的表观活化能。

Suitable water-immiscible organic solvents include aromatic hydrocarbons, eg toluene, xylene, naphthalene, tetrahydronaphthalene and methyl naphthalene; chlorinated aromatic hydrocarbons, eg chlorobenzene, fluorobenzene, chloronaphthalene and bromonaphthalene; esters, eg butyl acetate, ethyl acetate, methyl benzoate, ethyl benzoate, benzyl benzoate, butyl benzoate, phenylethyl acetate, butyl lactate, benzyl lactate, diethyleneglycol dipropionate, dimethyl phthalate, diethyl phthalate, dibutyl phthalate, di(2-ethylhexyl) phthalate; alcohols having six or more carbon atoms, eg hexanol, octanol, benzyl alcohol, phenyl ethanol, phenoxy ethanol, phenoxy propanol and phenoxy butanol; ethers having at least 5 carbon atoms, preferably C 5-14 ethers, eg anisole and phenetol; nitrocellulose, cellulose ether, cellulose acetate; low odour petroleum distillates; turpentine; white spirits; naphtha; isopropylbiphenyl; terpene; vegetable oil; mineral oil; essential oil; and natural oil; and mixtures of any two or more thereof.

适用于水互溶的有机溶剂包括芳香族碳氢化合物，如甲苯，二甲苯，萘，四氢萘和甲基萘；氯代芳香族碳氢化合物，如氯苯，氟，氯萘和萘；酯类，如醋酸丁酯，醋酸乙酯，苯甲酸甲酯，苯甲酸乙酯，苄酯，苯甲酸正丁酯，苯，醋酸丁酯乳酸，乳酸苄，二甘醇二丙酸酯，邻苯二甲酸二甲酯，邻苯二甲酸二乙酯，邻苯二甲酸二丁酯，二（2乙基己基）酯；醇有6个或更多碳原子，如己醇，辛醇，苯甲醇，苯乙醇，苯氧基乙醇，丙醇和苯氧基苯氧丁醇；醚至少有5个碳原子，最好荤5-14醚，如苯甲醚和phenetol；硝化棉，纤维素醚，醋酸纤维素，低气味石油蒸馏；松节油；白酒，石脑油isopropylbiphenyl；萜类，植物油，矿物油，挥发油；和天然油，以及任何两个或两个以上其混合物。

The paper studied that flavonoid was separated from the bergamot with normal experiment using alcohol to be the solvent.

以佛手为原料，以乙醇为溶剂对佛手进行了黄酮提取的正交实验，结果表明：乙醇浓度30%，固液比1：15，在80℃条件下提取2h的工艺条件较好。

Based on the retrieval and review of the bibliographer, the original process for the preparation of Dimethyl Phosphite in Zhejiang Xinan Chemical co., Ltd was evaluated.

论文在文献阅译和工艺原理分析的基础上，结合浙江新安化工集团股份有限公司原亚磷酸二甲酯生产装置的实际，研究了以甲醇、三氯化磷为原料的无溶剂的连续化生产新工艺。

The effects of the composition of catalyst (the structure and amount of bident ligand and strong acid, the cocatalytic activity of Cu〓, the roles of methanol and phenol etc.) and the copolymerization condition (the reaction time, temperature, amount of ST and CO, the structure and amount of solvent etc.) on catalytic activity were studied. The principle of the copolymerization was investigated.

研究了催化体系组成（含氮双齿配体的结构与用量、强酸的结构与用量、铜盐的助催化作用、甲醇和酚类化合物作用等）和共聚反应条件（共聚反应的温度与时间、溶剂种类与用量、苯乙烯与一氧化碳量等）对溶液共聚反应的催化活性的影响，探索溶液聚合反应规律。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。