溶剂

Liquids may be used as such or as accurately prepared solutions in appropriate anhydrous solvents.

液体样品也可以像这样操作或者精确的配制溶液至适当的无水溶剂中。

Anion exchange and solvent extraction are used to separate and purify Re.

Re的分离方法仍然是离子交换和溶剂萃取法。

Methods This title compound was prepared using the O-phenylene diamine and the anisaldehyde as the raw material,methanol as the solvent,and the phosphoric acid makes the oxidant.

方法本课题以邻苯二胺和对甲氧基苯甲醛为原料，在甲醇为溶剂，磷酸为催化剂的酸性条件下，一步反应制得2-(4-甲氧基苯基)苯并咪唑。

The yield of the 3, 4-dihydropyrimidine-2(1H)-one was up to 95.4% under mole ratio of anisaldehyde, methyl acetoactate and urea is 1:2:5, ion-exchange membrane is 3 g, ethyl alcohol as solvent and refluxing for 2 h.

当对羟基苯甲醛、乙酰乙酸甲酯与脲的摩尔比为1：2：5，乙醇作溶剂，3 g离子交换膜，回流2 h，产物收率达95.4%。

Anisaldehyde was synthesized from p-hydroxybenzaldehyde with dimethyl carbonate by microwave irradiation under phase transfer catalyst tetrabutylammonium bromide, The effect of power, time, solvent and catalyst of reaction on yield were researched.

以四丁基溴化铵为相转移催化剂，采用对羟基苯甲醛和碳酸二甲酯为原料，微波辐射下合成大茴香醛。考察了反应溶剂、功率、时间和催化剂对反应产率的影响。

To study the performance of inorganic composite catalyst for the SPC oxidation of p-methyl anisole, Cu2-Co2-KBr is used as catalyst of sodium percarbonate oxidation for p-methyl anisole synthesized by paracresol methylating. Effect of reaction conditions, such as the factors of catalyst composition, catalyst quantity, solvent, reaction temperature and time on oxidation of p-methyl anisole, is investigated.

研究了无机复合催化剂催化SPC氧化对甲基苯甲醚的反应性能：以Cu2-Co2-KBr为催化剂，利用过碳酸钠氧化对甲酚甲基化产物对甲基苯甲醚，系统研究了催化剂组成比例、催化剂用量、溶剂、反应温度、反应时间等因素对反应的影响。

In order to improve the efficiency of the system, we use anisole/toluene/ TBP as the solvent, in which the concentration of EAHQ is improved to 1.0 mol/L during the recycles of EAQ/EAHQ redox system.

二甲苯／TBP N门，体积比）溶剂中，EAHQ的饱和浓度为 0石2 mol几，用于丙烯环氧化时丙烯相对于 EAHQ的转化率为 96％，生成环氧丙烷的选择性为 88％。

But the concentration of Li2CO3 remains nearly consistent and a new component, CH3OLi, is found in SEI. It can be concluded from these results that anisole reacts with the reduction product of EC and DEC, RCO3Li, in the first process of Li＋ intercalating into the carbon electrode. The obtained CH3OLi is helpful in building up a more effective and stable SEI of the carbon electrode, reducing the cointercalation of solvent molecular. All these contribute to the improvement of the cycle performance of lithium-ion battery.

根据以上分析结果，提出了苯甲醚对锂离子电池循环性能的影响机理：在Li＋嵌入石墨电极的初次过程中，苯甲醚和EC、DEC的还原分解产物RCO3Li发生基团交换反应，生成CH3OLi，该产物能有效提高石墨电极表面SEI的稳定性，减少锂离子嵌入石墨过程中引起的溶剂分子共嵌入，从而改善电池的循环性能。

The second reaction we tested was diastereoselective Michael-Aldol annulation of -keto ester 121 with methacrolein to give a key intermediate for synthesizing (--Huperzine A.

通过对反应条件的筛选，我们得到的最好的结果是以-乳酸苄酯为手性辅基的β-酮酯121i为底物，以(1R， 2R)-环己二胺衍生的手性胍85i为催化剂，以无水四氢呋喃为溶剂，在-20℃反应，得到的产物的de值为73.2%。

So the energy is transferred from the excited naphthalene to the ground anthracene.

在不同的有机溶剂中，分别做了该系列化合物的荧光光谱随浓度的变化。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。