溶剂

Methods: from prepation of crude drug as start, study the technology of extract and defat with L9 (3~4) orthogonal test. With EtOH extraction and water sed, alkali washing, EtOAC extraction as main methods of eliminate dopant. Finally with alky AlzO3 chromatographic column, rich and gain anticancer active site. The maximum response was achieved at a 40 min extracting time with 10 times volume 90% EtOH added to the sample for the first time and 30 min for the second time. Adding 10 times water will produce precipitation; Place the precipitation into 6 times petroleum benzin to de-fat at 60℃.

云南红豆杉中抗癌活性物制备工艺研究方法：利用正交设计试验L9(3~4)确定原料药提取工艺为：10倍量90％乙醇提取两次，第一次40分钟，第二次30分钟；醇提液用10倍量水沉；沉淀加6倍量石油醚40℃脱脂；用1mol／L的NaOH溶液碱洗，除去酸性杂质；以碱性氧化铝柱，以环己烷／丙酮为洗脱溶剂，在环己烷-丙酮(6：4)段富集到所需活性部位，洗脱剂用量为3VB。

Novel chitosan derivative with long alky groups as the hydrophobic moieties and carboxymethyl groups as the hydrophilic moieties was synthesized. The chemical structure of N-octyl-O, N-carboxymethyl chitosan was characterized via FTIR, 1H NMR and elemental analysis. The physical properties were analyzed with wide angle X-ray diffraction and differential scanning calorimetry.

以天然可生物降解的壳聚糖为原料，通过在壳聚糖6位羟基上引入羧甲基，在2位氨基上引入疏水烷基链，制得N-辛基－O，N-羧甲基壳聚糖两亲性衍生物，分别用FTIR、1H NMR和元素分析等技术对其结构进行表征，用广角X射线衍射和差示扫描量热法对具物理性质进行分析，并考察其在各种溶剂中的溶解性能及其对难溶性药物的增溶能力。

Determination of total content of rare earth in rare earth drier and content of hydroxyl in solvent- free alkyd resin are introduced and then compared with the traditional methods.

介绍了稀土催干剂中总稀土含量和无溶剂醇酸树脂中羟基含量的测定，并和传统方法作了比较。

The effects of above-mentionedconditions on alkylene reaction are studied to obtain the optimum reactive conditionsby orthogonal experiments having seven factors and three levels. GCLE is chosen as material to prepare 7-phenyl acetamideyl vinyl cephalkyl acidp-methoxy benyl eatsr in the experiment. The process is as follow: GCLE reacts withiodide in solvent, and produce 3-iodid, then reacts with PPh_3 to produce Witting agent,and reacts with HCHO to produce 7-phenyl acetamideyl vinyl cephalkyl acid p-methoxy benyl eatsr in alkaline conditions.

试验选用GCLE作为原料制备7-苯乙酰氨基-3-乙烯基头孢烷酸对甲氧苄酯，反应过程如下：GCLE与碘化物、PPh3在溶剂中反应生成3位膦盐，在碱性条件下生成Wittig试剂再与HCHO反应生成7-苯乙酰氨基-3-乙烯基头孢烷酸对甲氧苄酯。

A young man saw Edison, said : I wanna develop a sort of all-purpose

一位年轻人看到爱迪生，说：我想去开发一种可以溶解所有物质的溶剂。

Low concentration of allyl alcohol helped to increase the reaction rate and high concentration of H2O2 could decrease the selectivity to glycidol using water as a solvent.

当催化剂用量一定时，以水为溶剂，较低的烯丙醇浓度更有利于反应的进行，而较高的双氧水浓度则会降低产物的选择性。

The resin was used as a selective oxidant for oxidation of allyl alcohol to allyl aldehyde.

合成了铬酸氢根季铵盐树脂，以它作为一种选择性氧化剂应用于烯丙醇的氧化反应，考察了温度、时间、溶剂、树脂与醇的物料比对氧化反应的影响。

For most of the enones and allylic alcohols, the reaction could be completed within several hours with good yields.

反应无需有机溶剂，对于大部分的烯酮和烯丙基醇反应可以在数小时内完成，产率良好。

ObjectiveTo study the anticancer effects of different solvent extracts from Alocasia macrorrhiza in vitro.

目的研究海芋不同溶剂提取物的抗肿瘤作用。

A method for the determination of sodium stearate in sodium aluminate solution was developed.

用溶剂浮选-气相色谱法测定铝酸钠溶液中的硬脂酸钠。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。