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Polyvinylidene fluoride was used to prepare solvent base fluorocarbon coating, and the solvent constitution of PVDF coating was screened and optimized.

摘要用聚偏氟乙烯树脂制备了溶剂型氟破涂料,筛选并优化了PVDF涂料的溶剂组成。

C-formaldehyde is widely used in rubber, paint, plastics, medicine, spices, agriculture, textile and other industries; propanol mainly to do organic solvents, organic chemical raw materials, spices, synthetic propylamine, Bromopropane etc.; n-butyl alcohol is widely used in the preparation of esters, plastics, plasticizers, pharmaceuticals, and used as a solvent, such as spray paint.

丙醛广泛用于橡胶、油漆、塑料、医药、香料、农业、轻纺等行业;丙醇主要做有机溶剂,有机化工原料、香料、合成丙胺、溴丙烷等;正丁醇广泛应用于制取酯类、塑料增塑剂、医药、喷漆以及用作溶剂等。

The activity of the reaction performed in protonic solvent was higher than that of non-protonic solvent.

发现在质子型溶剂中的反应活性要优于在非质子型溶剂中的活性。

To the reaction performed in protonic solvent, the catalytic activity decreased in the turn of methanol, ethanol and isopropanol, the highest TOF (933h〓) was achieved in methanol.

对于质子型溶剂醇中的反应,HCOOH的生成速率的顺序为甲醇>乙醇>异丙醇,在甲醇为溶剂中的反应,HCOOH的TOF值最高,为933h〓。

The resin is prepared by swelling chlorine balls in a solvent such as nitrobenzene; adding catalyst to obtain polystyrene-divinylbenzene adsorptive resin; removing reaction mother solution; washing to remove residual solvent and catalyst; swelling; adding pyrane reagent to further react with chloromethyl residual on inner and outer surfaces of the resin to obtain the pyranyl modified adsorptive resin with the composite function.

该树脂的制备方法:将氯球溶胀于硝基苯等溶剂中,加入催化剂,得到聚苯乙烯-二乙烯苯吸附树脂;抽尽反应母液,洗去残留的溶剂和催化剂;溶胀,加入吡喃试剂与树脂内外表面残留氯甲基进一步反应,可制得吡喃基修饰复合功能吸附树脂。

Two sorts of polyacrylate derivates were designed and systhesized. One has benzoic acid groups linked to backbone via an alkyl chain of different length, the other has pyridyl groups at its side chain. On the basis of hydrogen-bonding between carboxyl and pyridyl groups, multilayer film was fabricated in mixed solvents. We studied the effect of either the composition of mixed solvents or length of alkyl chain on the structure of a multilayer film.

设计合成了两类聚丙烯酸酯类高分子,一种侧链含有通过不同个数的亚甲基和主链相连的苯甲酸基团,另一种侧链含有吡啶基团,基于羧基和吡啶基之间的氢键相互作用,在混合溶剂中制备了多层膜,并研究了溶剂组成与高分子侧链间隔基长度对多层膜结构的影响。

To a liquid. Supercritical fluid can separate the extracts effectively without the recollective process, not like the general organic solvents with the residues.

超临界流体能有效将萃取物分离,不需要一般液体萃取时的有机溶剂回收过程,不会产生有机溶剂残留的缺点。

The influences of the type and dosage of the aldehyde, organic acids, as well as the water content in the reaction system on the racemization were examined in detail, and L-Glu was racemized quickly in the presence of 0.2 molar ratio of L-Glu to salicylaldehyde in acetic acid containing 20% water.

详细考察了腔的种类及用量、羧酸溶剂的种类、反应体系的含水量对消旋化的影响,结果表明L谷氨酸在含20%水的乙酸溶剂中,以水杨醛作为催化剂(水杨醛与L-谷氨酸的物质的量比为0.2)的优化条件下可以快速地被消旋化。

A new fullerene derivative containing energy-producing groups was prepared, and the reaction conditions affecting the yield were studied by the kroenecker method. The optimal reaction conditions with a 53.5% yield (based on consumed C60) are: 1:3:6 of molar ratio of C60 , o–nitrobenzaldehyde and sarcosine , 55℃ of reaction temperature, 12 h of reaction time, 40mL of toluene solvent.

利用N-甲基甘氨酸、邻-硝基苯甲醛和C60反应,合成分离出了含有硝基的新型富勒烯吡咯烷衍生物,通过正交试验对其工艺条件进行了研究,探讨了反应物剂量比、温度、时间和溶剂体积对产物产率的影响,得到了合成产物的最佳工艺条件:反应物剂量比为1:3:6、温度为55℃、反应时间为12h、溶剂甲苯体积为40mL,此时产物产率可达到53.5%(以消耗的C60计)。

7 typical Chinese coal samples were extracted by NMP/CS2 system at around 90 ℃ by Soxhlet method.

在90 ℃~100 ℃温和实验条件下,采用溶剂N-甲基-2吡咯烷酮及其与二硫化碳(NMP+CS2)混合溶剂体系对我国7个典型煤种进行抽提研究。

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