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For different solute-solvent-supercritical CO_2 systems, there are some generalities of the effects of the process parameters, for example, PS decreases with the increase of saturator pressure. But the effects of the process parameters are not same relating to the characteristics of the solutes and solvents.

不同的溶质-溶剂-超临界CO_2系统,其操作参数的影响规律有相同之处,如随着混合器压力升高微粒粒径减小等,但又不尽相同,这跟溶质和溶剂的性质有关。

Zinc Selenide hexagonal flakes and hexagonal prism have been synthesized by solvothermal method using ethylenediamine as solvent.

以乙二胺-乙醇为溶剂采用溶剂热法成功合成了具有六方结构的六边形硒化锌薄片和六边形棱柱。

Lead selenide nanocubes were successfully prepared on a large scale via a facile solvothermal route using formamide as both solvent and complexing agent.

用甲酰胺作溶剂和配位剂,通过温和的溶剂热路线成功地大量合成了PbSe纳米立方块。

The procedure involves the use of a capillary chromatography column (HP-INNOWAX, 30 m×0.53 mm×1.0 um) and FID detector. The result showes that 4 solvents are completely separated, the regression equation coefficients of 4 solvents are above 0.99, the recoveries are 90%~110% and the RSDs are less than 2.0% respectively.

实验的色谱柱为HP-INNOWAX(30 m×0.53 mm×1.0μm)毛细管色谱柱,检测器为氢火焰离子化检测器。4种溶剂均达到完全分离,各溶剂线性实验所得回归方程的相关系数均大于0.99,加标回收率为90%~110%,RSD.0%(n=6)。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

Impact of solvent soakage on charge storage stability and filtration efficiency is thoroughly discussed according to the Flory-Huggins solvent swelling theory.

根据Flory--Huggins的溶剂溶胀理论探讨了溶剂浸泡对材料电荷存储能力和过滤效率的影响规律。

PEG400, which is poisonless, low cost with good capability of carrying sodium ion, was used as catalyst, and sodium cyanide owing to its less toxicity, stability, less amount in the reaction, was used as cyanating reagent in the reactions.

在有机卤代化合物或酯与PEG400、NaCN的用量比分别为1∶0.03和1∶1.3的条件下,获得了高收率(84%-96%)和高纯度(≥98%)的腈化物。通过几种不同溶剂下反应的对比,选择了以苯为溶剂,在酰氯与PEG400、 NaCN的用量比分别为1∶0.05和1∶1.2及反应温度为室温的条件下,合成了酰基腈化物。

A Simple titanium resource and a soft preparation method is very important in the preparation of titania, hydrogen titanium oxide hydrate and sodium...

本文以无水乙醇作为溶剂,以钛酸四丁脂为钛源,采用溶剂热法制备氧化钛纳米粒子、钛酸纳米管,讨论了产品的形成机理。

Please use the soft cloth soaked with detergent to wipe off this unit if the stains are found on the bag boy's surfaces of this unit.

如果本产品袋身表面出现污脏,请用沾有洗洁精的软布擦洗,严禁使用强溶剂,如汽油、溶剂等物。

When solation or hydration affects bioaailability, appropriate manufacturing and control procedures should be established.

其它方法提供的信息可能也是必要的,因为有些溶剂化物通常在溶剂的沸点以上是稳定的。

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