溶剂

The results also show that subtituent position on the benzene ring has a great influence on the transfer volume. The trends of change of δ〓ΔΦ〓〓 for mand p-isometers with the composition of the mixed solvent are similar. However, the position and amplitude of the limit valve are different from each other. These are discussed according to the inductive effect and the resonance effect.

研究发现：取代基在苯环上的取代位置对迁移偏摩尔体积有明显影响，间、对位取代的异构体在DMF-水混合溶剂中的δ〓Δφ〓〓随混合溶剂的组成变化规律相似，但极值点的位置及幅度有所不同，根据诱导效应和共轭效应对此进行了讨论。

The non-desorbing fractions dominated the total residues of acenaphthene, and AM promoted the transformation between acenaphthene forms. The desorbing fractions and non-desorbing fractions of acenaphthene were 17.0%-37.8% and 5.4%-26.6% lower than the control, while the bound residual was 12.2%-89.5% higher than the control.

有机溶剂提取态是土壤中危残留的主要部分，AM作用促进了苊各形态之间的转化；接种AM后土壤1、2中范可脱附态和有机溶剂提取态残留量分别比对照降低了17.0%~37.8％和5.4%~26.6%，而结合态残留量比对照增加了

Under the optimized parameters,i.e.,resorcinol to potassium carbonate molar ratio of 1∶0.5,reaction temperature of 155℃-160℃,reaction time of 6 hours-7 hours,and dimethyl acetamide as solvent,the yield of 2,6-dihydroxybenzoic acid was up to 29.38%.

溶剂羧化法Kolbe-Schmitt反应，是在有机溶剂氛围中，由酚的成盐和酚盐的羧化两步完成，一直应用在农药、医药以及化肥的合成过程中。

They may be dissolved in most common organic solvents,excluding methanol.Examples of suitable solvents include acetonitrile or acetone.

该化合物可以溶解在除甲醇以外的大多数普通有机溶剂中，适宜的溶剂有乙腈和丙酮。

The method comprises: adding 4-(3,4-dichlorophenyl)-1-tetralone and solvent at a ratio of 1:(3-4) into a three-necked flask with a stirrer, heating under stirring until 4-(3,4-dichlorophenyl)-1-tetralone is completely dissolved, heating to 60-100 deg.C, refluxing for 0.5-2 h, cooling the filtrate to -5-10 deg.C, filtering, recrystallizing to obtain refined 4-(3,4-dichlorophenyl)-1-tetralone, and drying at 40-80 deg.C to obtain dry 4-(3,4-dichlorophenyl)-1-tetralone.

该方法的步骤是：在带搅拌的三颈瓶中依次加入4-(3，4-二氯苯基)-1-萘满酮和溶剂，溶剂与4-(3，4-二氯苯基)-1-萘满酮的L∶W为3～4∶1，将上述4-(3，4-二氯苯基)-1-萘满酮及混合精制溶剂搅拌下升温，使4-(3，4-二氯苯基)-1-萘满酮全部溶解，升温至60～100℃，回流0.5-2h；滤液用冰水冷却至-5～10℃，过滤，所得物料再用上述方法进行一次重结晶得到精品4-(3，4-二氯苯基)-1-萘满酮，40～80℃干燥后即得到干品4-(3，4-二氯苯基)-1-萘满酮。

The results showed: when TLC solvent system was: chloroform - methanol - diethyl amine = 90:9:1, alkaloids from lotus leaves were well isolated, and five components were isolated and identified by spraying Dragendorff reagent. The optimal conditions of HPLC solvent system were: methanol- water - diethyl amine = 75:25:0.0125. Under the conditions, components of alkaloids from lotus leaves were separated very well, and ideal RP-HPLC peaks were obtained.5、Methods of High Speed Counter Current Chromatography and preparative High Performance Liquid Chromatography applied to identify and purify alkaloids from lotus leaves were set up. When solvent system of HSCCC was: chloroform - methanol - water (pH=4.00)= 4:3:2, speed of chromatogram was 700rpm, flow speed of the mobile phase was 2mL/min, four pure components relatively were attained by isolation and purification.

结果表明：薄层层析溶剂系统为氯仿：甲醇：二乙胺=90：9：1，使荷叶中的生物碱达到了较好的分离效果，并用改良的碘化铋钾试剂喷雾显色，共分离鉴别出了5种荷叶生物碱；分析型HPLC分析检测的较优溶剂系统为甲醇：水：二乙胺=75：25：0.0125，使荷叶生物碱的各个组分达到了基线分离，并获得了较好的峰形。5、建立了高速逆流色谱和制备型HPLC技术分离纯化荷叶生物碱的具体方法。H(来源：ABC46论文网www.abclunwen.com)SCCC法在溶剂系统为氯仿：甲醇：pH4.00的水=4：3：2，色谱仪转速为700rpm，流动相流速为2mL／min的条件下，分离纯化得到了4个纯度较高的化合物。

Production of environmentally-benign solvent naphtha up to the international quality specification,with low aromatics and low sulfur,will be the trends in this aspect.

目前，我国溶剂油质量与国际溶剂油质量差距较大，生产符合国际质量标准的低芳烃和低硫含量的环保型溶剂油是今后发展的方向。

Was founded in early 2001, with a total investment of more than 500 million yuan, covers an area of 6600 square meters, is specialized production solvent oil businesses, products include: high boiling point aromatic solvent naphtha, solvent oil aliphatic series and related products.

石家庄市鑫安精细化工有限公司始建于2001年初，总投资500余万元，占地面积6600平方米，是专业化生产溶剂油的企业，产品有：高沸点芳香烃溶剂油、脂肪族系列溶剂油及相关产品。

Fluorescence emission spectra and UV absorb spectra analysis have been undertaken to test the influence of solvent polarity on the lowest excited singlet state of the tertiary amines. The absorption maxima were red-shafted slightly, and the emission maxima were red-shafted strongly, which showed all of the three compounds were found to be essentiallyππ* in character, which makes for the formation of triplet-exciplex state and the subsequent reactions,?known as photo-reduction and hydrogen-abstraction.

本文借助光谱检测的手段测试了新合成的增感剂的光物理化学性能，利用荧光发射光谱和紫外吸收光谱测试了溶剂极性对叔胺的最低激发单重态的影响，实验结果表明叔胺的紫外最大吸收波长随溶剂极性的增强产生轻微的红移，荧光最大发射波长随溶剂极性的增强产生明显的红移，表明三种叔胺的最低激发单重态具有ππ*跃迁的特性，这对于激态复合物的生成以及其后的光致还原反应和提氢反应的发生都非常有利。

The optimum conditions were obtained as follows : the weight ratio of fatty acids of rapeseed oil and 85%acetic acid is 1:4, ozonolysis temperature is 20-25

本文使用植物油脂肪酸为原料，原料丰富，价格低廉；使用含水溶剂不但提高了产品收率，而且降低了溶剂挥发性和溶剂的腐蚀性；使用活性炭吸附壬二酸粗品大大提高了壬二酸纯度，此方法简便易行，用此方法处理壬二酸粗品，壬二酸的纯度可达96.1%。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了