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The stability and the distribution of vitamin C in aqueous systems of cetyltrime-thylammonium bromide and sodium oleate were studied.

研究了维生素C在表面活性剂十六烷基三甲基溴化铵和油酸钠体系中的稳定性及其在双水相中的分配规律。

The experimental result showed that the optimal conditions were the molar ratio of potassium bromide to cyclohexanol 1:0.8, H2O 1.5mL,concentrated sulfuric acid 5mL , reflux reaction for 4h, the separated yield was high up to 93%.

结果表明,当反应条件为:溴化钾与环己醇摩尔比1:0.8,水1.5mL,浓硫酸5mL,回流反应4h,分离产率高达93%。

Silver nano powder was produced by salt of silver and bromide in anhydrous organic solvent.This method can reduce the tendency for silver nano particle to grow during drying.

在无水的条件下,以有机物为溶剂,从银盐和溴化物出发制备银纳米微粉,避免银纳米粒子干燥过程中易长大的倾向。

The critical crossover behavior in the ternary electrolyte solutions of water+3-methylpyridine+sodium bromide is a matter of debate.

对水+3-甲基吡啶+溴化钠三元电解质溶液的临界跨接行为的认识存在着争议。

The calcium was determined by xylenol orange-CTMAB-absolute ethyl alcohol complexation color in the gelatin.

以二甲酚橙—十六烷基三甲基溴化胺—无水乙醇络合显色体系测定了明胶中的钙。

The super microporous tin-doped zirconium oxides were successfully synthesized by sol-gel method using zirconyl chloride as Zr source, tin chloride as Sn source and cetyltrimethylammonium bromide as template under hydrothermal or refluxing conditions.

以二氯氧锆和四氯化锡为金属源,十六烷基三甲基溴化铵为模板剂,用溶胶-凝胶法在水热或回流条件下成功合成出了锡掺杂的超微孔二氧化锆材料。

Using modified apple fruit RNA extraction method based on CTAB by adding a step of using KAc and absolute ethanol to precipitate pectin, high-quality total RNA was extracted from the leaf and the inflorescence of jackfruit (Artocarpus heterophyllus Lam.). The yields of total RNA were 74.7 μg/g FW for the leaf and 31.6 μg/g FW for the inflorescence.

以菠萝蜜的叶片和花序为材料,采用改良的十六烷基三甲基溴化胺法(在原来的提取方法基础上,使用乙酸钾和无水乙醇预先沉淀果胶),成功提取菠萝蜜叶和花序的总RNA,平均产率分别为74.7μg/gFW和31.6μg/gFW。

The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.

本发明属于无机多孔材料、吸附材料和催化材料技术领域,涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料,用偏硅酸钠的水溶液在30~60℃反应10~300分钟,使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片,加入模板剂十六烷基三甲基溴化铵,然后调节母液pH值为10~12,老化1~8小时,然后加入高压釜于80~130℃进行水热合成反应。反应24~72小时后,分离出固体,水洗、干燥,然后于500~600℃焙烧5~10小时,得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料,所合成的材料经过质子交换可以具有较强的酸性,在吸附和催化领域具有广泛应用前景。

Direct burning bromization absorption cold and hot water unit is choosed to achive the aim of two use,which can offer refrigerated water in the summer and hot water in the winter.

制冷机房设于架空层,选用直燃型溴化吸收式冷热水机组来达到一机两用,夏季供冷冻水,冬季供热水,冷却塔置于屋顶。

It was observed that the optimum temperature for the fluorous biphasic regioselective nitrations of toluene, ethylbenzene, flurobenzene, chlorobenzene, bromobenzene, odobenzene and diphenyl ether were 80℃, 60℃, 60℃, 60℃, 80℃, 80℃ and 70℃ respectively. The catalyst had almost no activity when the reaction system contained 25% of water. Simultaneously, increasing the volume ratio of fluorous phase and organic phase in the system in which the fluorous phase can miscible with organic phase could decrease ortho-para ratio.

发现甲苯、乙苯、氟苯、氯苯、溴苯、碘苯加二苯醚的最佳氟两相选择性硝化温度分别为80℃、60℃、60℃、60℃、80℃、80℃和70℃,当加入25%的水时,催化剂已基本失去活性,在氟相和有机相能完全互溶的体系中升高氟相和有机相的体积比有利于降低邻对位比值。

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