溴水

Take for the amount of test materials, precision that set, place beaker, unless otherwise specified, may be added 40ml of water and hydrochloric acid solution (1-2) 15ml, and then set on a magnetic stirrer, stirring allows the dissolved, together with potassium bromide 2g insert platinum - platinum electrode, it will insert the solution of the following buret tip is about 2 / 3, using sodium nitrite titration solution (0.1mol / L, or 0.05mol / L) rapid titration, side drops while stirring, to near point, Burette tip surface will be presented with a small amount of water leaching cutting-edge, lotion, and solution and continue titration slowly until the sudden deflection of galvanometer pointer, namely, titration end point.

取供试品适量，精密称定，放置烧杯中，除另有规定外，可加水40ml与盐酸溶液（1-2）15ml，而后置电磁搅拌器上，搅拌使溶解，再加溴化钾2g，插入铂-铂电极后，将滴定管的尖端插入溶液下面约2/3处，用亚硝酸钠滴定液（0.1mol/L或0.05mol/L）迅速滴定，边滴边搅拌，至近点时，将滴定管的尖端提出液面，用少量水淋洗尖端，洗液并溶液中，继续缓缓滴定，至电流计指针突然偏转，即为滴定终点。

Through esterification of functionality —COOM on side chains of xanthan gum by 1-bromooctane,water soluble hydrophobically modified xanthan gums of octyl substitution 11 and 21 per 100 structural units,HMXG-C8-11 and-21,are prepared.

用1-溴代辛烷使黄原胶XG侧链上的—COOM基团酯化，得到以100结构单元计取代度为11和21的水溶性疏水改性黄原胶HMXG-C8-11和-21。

It provides a route tothe compounds which contains three functional groups, two carbon-nitrogentriple bonds and one carbon-carbon double bond. In water, metallic indiumpromotes carbon-sulfur bond coupling reaction of aromatic sulfonyl chloride withsuitable organic halides to afford sulfones. In the last chapter, metallic tin mediated allylation of aldimines with allylbromide was revealed.

第三章，我们研究了在水相介质中金属铟促进的烯丙基溴对1，1-二氰基-2-芳基乙烯的Michael加成反应，生成一个含碳碳双键和二个碳氮叁键的三官能团化合物，另外，金属铟在水介质中还可以促进芳基磺酰氯与卤代烃发生碳硫键的偶联，生成砜。

Pyruvaldehyde was synthesized with acetone or 1,2 propanediol as starting material respectively.With n∶n=1 00∶0 79,3 0-4 0 g potassium chlorate as catalyst,and water and glacial acetic acid as solvent,refluxing on water bath of 60-75 ℃ for 4 h,bromoacetone was obtained in 63 5% yield.

分别用丙酮和 1，2 丙二醇做原料合成了丙酮醛。n∶n =1 0 0∶0 79，加入 3 0～4 0g氯酸钾做催化剂，水和冰醋酸做溶剂，水浴温度为 6 0～ 75℃，回流 4h ，制得产率为 6 3 5 %的溴丙酮。V∶V =11 9∶1 0 ，通入空气，在 6 5～ 70℃反应 5～ 8h ，制得产率为 5 9 6 %的丙酮醛。

Universal indicator paper,special indicator paper,ammonium fluoride,ammonium hydrogen difluoride,nbenzyldimethylamine,disinfectant paper,nacetylphenylhydrazine,mcresol purple,bromocresol green,fluorescein,eosin Y,ninhydrin,phenedons,potassium phthalate,pamimobenzene sulphonic acid anhydrous.

广泛试纸，精密试纸，氟化铵，氟化氢铵，N苄基二甲胺，消毒试纸，N乙酰苯肼，间甲酚紫，溴甲酚绿，荧光素，曙红Y，水合茚三酮，菲尼酮S，苯甲酸氢钾，无水对氨基苯磺酸。

To investigate the effect of surfactant self-assembling properties on the template synthesis of porous inorganic materials, the critical micelle concentration of surfactant cetyl trimethylammonium bromide was measured in both water and aqueous ethanol solvent using steady-state fluorescence techniques.

为了研究乙醇－水混合溶液中表面活性剂的自组装特性对多孔无机材料模板法合成的作用，采用稳态荧光法测定了乙醇－水混合溶剂的组成变化对十六烷基三甲基溴化铵临界胶束浓度的影响。

The effect of short chain monohydric alcohols (ethanol, n-butanol) and dihydric alcohols (ethyleneglycol, 1,4-butanediol) on the aqueous two-phase system of cationic and anionic surfactants is studied.

研究了短链一元醇和二元醇(乙二醇、1，4-丁二醇)对正负离子表面活性剂混合溶液(十二烷基硫酸钠-十六烷基三甲基溴化铵-水)双水相的影响。

Bromo-2-sulfolene (2) reacted with substituted benzoic acid salt s 3a～3c or alizarin yellow (3d) to give four novel allylic substitution products 4a～4d by esterification reaction, respectively.

以3，4-二溴环戊砜(1)为原料，在无水吡啶作用下发生消除反应，得到反应中间体4-溴-2-环戊烯砜(2)，再分别与一系列取代苯甲酸盐3a～3c以及茜素黄GG(3d)发生酯化反应，合成出4种新环戊烯砜衍生物4a～4d，并用IR，1HNMR，MS，元素分析等表征了它们的结构。

Melting point 3410 ℃, boiling point 560 ℃, relative density of 1935, F the external electronic structure of 5d46s2, in the chemical reaction time is very easy to lose 1-6 electronic, but also can get 1-2 electronic, so oxidation number of 0,± 1,± 2, 3, 4 , 5 and 6, with 6 price of the most stable compounds, such as WO3 does not dissolve in water, the air will form in the tungsten trioxide thin protective layer of tungsten, tungsten with fluorine at room temperature, chemical combination, red hot when there is no moisture and Bromine iodide together, red hot when you can and water reaction WO3, at room temperature reaction of tungsten with aqua regia, but the hot concentrated hydrochloric acid and sulfuric acid can only be played with its weak response, but molten nitrate, nitrite, too Hydrogen peroxide, sulfur steam, steam and other phosphorus can play intense reaction, high temperature can not be carbon, boron and silicon reaction of binary compounds, widely used in industrial tungsten steel and tungsten carbide, pure tungsten filament is used to the system, and X-ray tube Tube heating components, semiconductor components can be prepared tungsten silicide, tungsten industrial production is white or black tungsten ore tungsten ore refining.

熔点3410℃，沸点560℃，相对密度1935，F外围电子结构为5d46s2，在化学反应时很容易丢掉1—6个电子，也能得到1—2个电子，所以氧化数为0、±1、±2、＋3、＋4、＋5和＋6，以＋6价化合物最稳定，如WO3不溶于水，空气中的钨会形成薄层三氧化钨保护层，钨能与氟在室温下化合，红热并无潮气时能与溴、碘化合，红热时还能和水反应生成WO3，室温下钨可与王水反应，但热的浓盐酸和硫酸只能与其起微弱反应，但对熔融的硝酸盐、亚硝酸盐、过氧化氢、硫蒸汽、磷蒸汽等能起激烈反应，高温下不能与碳、硼和硅反应生成二元化合物，工业上广泛使用钨钢和碳化钨，纯钨用来制灯丝、电子管和X射线管的发热元件，硅化钨可制半导体元件，钨工业生产是将白钨矿石或黑钨矿石精炼。

Mesoporous tin oxide was synthesized by using cetyltrimethyl ammonium bromide or CTAB and Tween-20 as the template or hydrothermal process. Hollow tin dioxide micospheres were synthesized by using resorcinol-formaldehyde gel as the template or hydrothermal process. Thermogravimetric analysis, X-ray diffraction and electron microscopy have been used to characterize the materials.

本文分别采用十六烷基三甲基溴化铵模板法、CTAB和吐温20复合模板法及水热法来合成介孔氧化锡；用间苯二酚和甲醛凝胶模板法及水热法合成空心球氧化锡，并用热分析、X射线衍射、电镜等对以上材料作了形貌及结构表征。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。