溴水

Macerate 1.0g of the powdered sample with 20.0 ml of chloroform plus 0.3ml of 25％ NH_4 OH in a glassstoppered flask overnight.

本文报道用不含粘合剂的氧化铝薄层，以二甲苯-丙酮-无水乙醇-二乙胺(50：40：10：0.6)为展开剂分离茄科植物中的莨菪碱、东莨菪碱、山莨菪碱、樟柳碱及红古豆碱等五种莨菪烷生物碱，用改良Dragendorff试剂-Wagner试剂(1：1)显色，定量收集莨菪碱、东莨菪碱及山莨菪碱的斑点，莨菪碱和东莨菪碱用氨甲醇洗脱，蒸干洗脱液后分别用pH 5.6及pH 4.5的溴甲酚绿溶液作比色测定；山莨菪碱用4％醋酐氯仿洗脱，蒸干洗脱液后用pH 5.6的溴甲酚绿溶液作比色测定。

As the second part of a series of studies on the synthesis of 2-phenoxyisobutyric acid ethyl ester by tri-liquid-phase catalysis, this work examines the factors affecting the reaction between 2-bromoisobutyric acid ethyl ester and sodium phenolate with tetra-n-butylammonium bromide as a phasetransfer catalyst.

本文为以三液相催化技术合成2-苯气基异丁酸乙酯之研究系列的第二部份，主要在探讨各变因对以溴化正四丁基铵为相间转移触媒，催化2-溴异丁酸乙酯与酚化钠（NaOPh，水相亲核试剂）反应的影响。

Bromobutane was synthesized from potassium bromide and n-butyl alcohol by adding concentrated sulfuric acid in water. Various affecting factors were investigated.

以溴化钾、正丁醇为反应原料，水为溶剂，滴加浓硫酸合成溴代正丁烷。

Pd combined with tetrabutyl ammonium bromide and potassium bromide into a ternary ion association precipitate in the aqueous solution. The precipitate was floated well on the surface of water phase to make a distinct boundary layer between liquid and solid phases.

在水溶液中，钯与溴化钾和四丁基溴化铵形成不溶于水的三元离子缔合物，此三元离子缔合物浮于盐水相上层形成界面清晰的液－固两相。

In the process of laboratory study, oxycodone was prepared by oxidating thebaine at 6,14-position under oxydol, hydrodeoxidizing 7,8-position double bond and 14-position ether under palladium catalyst. Furthermore, N-methyl of oxycodone was isolated byα-chloro-ethyl chloroformate under anhydrous condition and protection of 14-position hydroxyl to obtain noroxycodone, which was further converted into methylnaltrexone by N-alkylation in presence of cyclopropyl bromomethane, then by isolating 3-position methyl of methylnaltrexone under boron tribromide, becoming hydrochloride to prepare target compound, natrexone hydrochloride.

实验室工艺方面，本文首先用双氧水氧化蒂巴因的6-位和14-位、在钯炭催化下加氢还原7-8位双键和14-位醚合成羟考酮，然后提出并优化了在无水和14-位保护的情况下，用氯甲酸-α-氯乙酯脱去羟考酮的N-位甲基合成去甲羟考酮，再用环丙甲基溴将去甲羟考酮的N-位烷基化合成甲基纳曲酮，最后采用三溴化硼脱去甲基纳曲酮的3-位甲基和成盐酸盐合成盐酸纳曲酮。

This experiment chooses a kind to contain 1 ％ bromine phenol orchid and the methanol solution of 5 ％ water serve as bromic phenolic chemistry to enhance reagent.

本实验选取一种含有1％溴酚兰和5％水的甲醇溶液作为溴酚化学增强试剂。

Bis-(4′-bromobenzoyl)benzene was synthesized from terephthaloyl chloride and bromobenzene using aluminum chloride as a catalyst.

以对苯二甲酰氯和溴苯为原料，无水氯化铝粉末为催化剂，合成了1，4-双(4′-溴苯酰基)苯，其结构经1HNMR，IR和DSC表征。

Benzyl bromide was synthesized from dibenzyl ether and hydrobromic acid with SO42-/ TiO2 as catalyst and cyclohexane as dehydrant.

以二苄醚和氢溴酸为原料，SO42-/TiO2为催化剂，环已烷为带水剂，合成了溴化苄。

Reaction of 9-bromofluorenewith diethyl malonate and sodium carbonate gives diethyl 2-(9-Fluorenyl)malonate.Aminolysis of diethyl 2-(9-Fluorenyl)malonate in ethylenediamine and propylene diamine give〓 and 〓, respectively.〓 and 〓 were synthesized by the reaction of 9-bromofluorene with oxalyl bisethylenediamine. Copper and nickel complexes of 〓 and 〓 were obtained by the reaction of 〓 and 〓 with copper and nickel salt, respectively, in aqueoussolution and extrusion of two hydrogen ions from the amide groups.

使9-溴芴与丙二酸二乙酯在无水碳酸钠存在下反应合成出2-(9-芴基)丙二酸二乙酯。2-(9-芴基)丙二酸二乙酯在乙二胺中胺解得到配体〓，2-(9-芴基)丙二酸二乙酯在1，2-丙二胺中胺解得到配体〓，使9-溴芴与草酰二乙二胺作用得到配体〓和〓与相应的金属盐作用分别得到它们的铜、镍配合物。

One-step synthesis of the high molecular weight bromated epoxy resins for flame retardants is studied with tetrabromobisphenol A and epichlorohydrin as raw materials in mixed solvent comprising 1,4-dioxan and water.

研究以四溴双酚A和环氧氯丙烷为原料在二氧六环和水混合溶剂中一步法合成了高分子量溴化环氧树脂阻燃剂。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新