溴化的

2 The analysis step by 25.0mL sample lixivium, moved in the direction of arsenic in the bottle, plus 10 ml of hydrochloric acid and 10 ml of potassium iodide solution and 5 drop acid stannochlor solution, shake the place 10min, together with 2 g of arsenic-free zinc metal, immediately mounted a good lead acetate paper turns red cotton and mercury bromide from log that arsenic tube placed in the 25-38, f μh of the dark side, remove the test strip and standard mercury bromide a color not deeper than standard.

7.2 分析步骤取25.0mL样品浸泡液，移入测砷瓶中，加5mL盐酸、5mL碘化钾溶液及5滴酸性氯化亚锡溶液，摇匀后放置10min，加2g无砷金属锌，立即将已装好乙酸铅棉花及溴化汞试纸的测砷管装上，放置于25～30℃的暗处1h，取出溴化汞试纸和标准比较，其色斑不得深于标准。

We successfully improved the methods of departing O-methyl using boron tribromide, of isolating hydrogen bromide byα-chloro-ethyl chloroformate, and of related in synthesis of natrexone, new medicine, using boron tribromide. This resulted in generation of hydrogen cyanide becoming impossible.

改进了以氯甲酸-α-氯乙酯脱代替溴化氰以及改进的三溴化硼法作为新药纳曲酮合成中相应的方法，去除了合成过程中产生氰化氢气体的可能性。

As the second part of a series of studies on the synthesis of 2-phenoxyisobutyric acid ethyl ester by tri-liquid-phase catalysis, this work examines the factors affecting the reaction between 2-bromoisobutyric acid ethyl ester and sodium phenolate with tetra-n-butylammonium bromide as a phasetransfer catalyst.

本文为以三液相催化技术合成2-苯气基异丁酸乙酯之研究系列的第二部份，主要在探讨各变因对以溴化正四丁基铵为相间转移触媒，催化2-溴异丁酸乙酯与酚化钠（NaOPh，水相亲核试剂）反应的影响。

Methods The mercury in urine, which is the total amount of inorganic mercury in urine, including those produced from organic mercury after treated by potassium bromate and potassium bromide, is determined by atomic absorption spectrophotometer after reduction into mercury atom with sodium borohydride.

方法］尿样中汞（尿中无机汞和经溴酸钾－溴化钾处理尿中有机汞生成的无机汞之和）以硼氢化钠还原生成汞原子蒸气，用原子吸收光谱仪测定其汞的含量。

Pd combined with tetrabutyl ammonium bromide and potassium bromide into a ternary ion association precipitate in the aqueous solution. The precipitate was floated well on the surface of water phase to make a distinct boundary layer between liquid and solid phases.

在水溶液中，钯与溴化钾和四丁基溴化铵形成不溶于水的三元离子缔合物，此三元离子缔合物浮于盐水相上层形成界面清晰的液－固两相。

Seven 1-phenyl-(4-pyridinyl)acetylene derivatives were conveniently synthesized in this paper using corresponding styrylpyridines as starting materials by bromination, rearrangement and debromination.

本文采用简单易行的方法从苯乙烯基吡啶类衍生物通过溴化、重排和脱溴化反应合成了7种苯乙炔基吡啶类单体，研究了它们在1mol/L盐酸水溶液中的光环加成反应。

A process for preparingp-fluo-2-(2-methyl-3-propionyl)-4-oxy-N,3-diphenyl-phenylbutylamide includes such steps as Friedle-Craft acylating of newly prepared phenylacetyl chloride and fluorobenzene under catalysis of AlCl3 to obtain 4-fluoro-phenylbenzyl ketone, brominating at carbonyl alpha position under catalysis of less AlCl3 to obtain alpha-bromo-4-fluo-phenylbenzyl ketone, and condensing with isobutyryl acetanilide under action of sodium ethoxide.

本发明涉及一种制备对氟－2－(2－甲基－3－氧丙基)－4－氧－N，3－二苯基－苯丁酰胺(1)的方法，其包括以下步骤：新制的苯乙酰氯与氟苯在AlCl3催化下进行Friedle－Craft酰化反应，得到对4－氟－苯基苄基酮(4)；化合物(4)在少量AlCl3催化下进行羰基α位溴化，得到α－溴－4－氟－苯基苄基酮(5)；然后(3)异丁酰乙酰苯胺在乙醇钠作用下与化合物(5)进行缩合。

The floatation separation behaviuor of Pd (superscript 2+) by KBr-cetyl pyridinium bromide system in the presence of NaNO3 and the conditions for the separation of Pd (superscript 2+) from other metal ions were studied.

研究了硝酸钠存在下，溴化十六烷基吡啶－溴化钾体系浮选分离钯的行为及与一些金属离子分离的条件。

The results show that Pd (superscript 2+) combines with KBr and cetyl pyridinium bromide into a ternary ion association precipitate2(PdBr4) in the aqueous solutions, which floated above the surface of water phase with clear interface.

结果表明，在水溶液中，Pd(上标2+)与溴化钾、溴化十六烷基吡啶形成不溶于水的三元缔合物2(PdBr4)，此三元缔合物可浮于水相上层分成界面清晰的液－固两相。

For example, alpha -chloronaphthalene is a suitable solvent for reaction between phthalonitrile and gallium triiodide or tribromide to provide iodogallium phthalocyanine or bromogallium phthalocyanine.

例如，α－氯萘为用于邻苯二甲腈和三碘化镓或三溴化镓之间的反应以得到碘镓酞菁或溴镓酞菁的适宜溶剂。

And discuss some key point of integrated management system design, include hazard identification and risk assessment and risk control in the occupational health and safety management, the measure of satisfaction target of customer, the flawlessness of law system, the integration of the integrated management system and enterprise standardization system, unify lead institution and work orgnization, integreted internal audit and integrated management review.

同时，论述了一体化管理体系构建中的几个主要问题，包括职业健康安全管理中的危险源辨识、风险评价和风险控制、顾客满意度的科学监测、法律、法规体系的完善、一体化管理体系与企业标准化体系的有机结合、统一的领导机构和工作机构、一体化的内部审核和管理评审。

Deepwater Taranaki is investigated for its petroleum potential, using all available seismic data tied to shallow-water wells.

运用与浅水井相关的现有全部震波探测数据考察了深海区塔拉纳基盆地的油藏前景。