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PH of filtrate is kept below 0.65 in order to avoid the reaction between sodium formate and iodine bromide. Then iodine bromide halogenation method is used to determine quantitatively the content of the third monomer, i.

控制滤液pH在0.65以下,以防止甲酸钠和溴化碘起反应,然后用溴化碘卤化法定量测定滤液中的第三单体甲基丙烯磺酸钠的含量。

Tianrun company's existing 120 employees, of whom 15 were engineers, 3 senior engineers who enjoy special government allowances of experts one person, the company brominated long-term commitment to new product research and development, with a full range of laboratory facilities, laboratory room, to carry out most of bromine series products, small-scale test, pilot and laboratory experiments, subjects are as follows: high-quality three-bromo-phenol in the test, hydrogen bromide by-product utilization in the test, 1,000 tons of bromine dodecane-generation pilot project.

天润公司现有职工120余人,其中工程技术人员15人,高工3人,享受省政府特殊津贴专家1人,公司长期致力于溴系新产品的科研开发,拥有设施齐全的实验室、化验室,能够进行大部分溴系列产品的小试、中试实验及化验,现正进行的课题为:高品质三溴苯酚的中试,副产溴化氢的综合利用中试,1000吨溴代十二烷项目中试。

To investigate the pitting and metastable pitting rules of type 304 stainless steel, potentiodynamic polarization method was employed to study the behavior of metastable pitting and stable pitting on 304 stainless steel in sodium bromide solution and borate/phosphate buffered bromide solutions. The influence of the concentration of Br-、the pH value、the buffer capacity and general environmental factor to pitting potential and metastable pitting was studied as well.

为了更深入地了解304不锈钢的稳态及亚稳态孔蚀规律,本文采用动电位慢扫描法测得了304不锈钢的阳极极化曲线,研究了不锈钢在纯溴化钠溶液及含溴化钠的硼酸盐或磷酸盐缓冲溶液中的亚稳态孔蚀以及稳态孔蚀行为,分析了溴离子浓度、pH值、缓蚀性阴离子、以及缓冲容量和综合环境因子对孔蚀电位以及亚稳态孔蚀特征参数中的形核数目、峰值电流、生长寿命的影响。

The total synthesis of the title compound 10 was accomplished starting from 3,5-dimethoxybenzoic acid (1) and p-hydroxybenzaldehyde (6). In the process, esterification, reduction, bromination and Wittig-Homer reaction were performed.

以3,5-二甲氧基苯甲酸为起始原料,经过甲醇酯化、氢化铝锂还原、四溴化碳溴代和Wittig-Homer反应,高产率的合成了Wittig-Homer试剂(5)。

The effects of solvent on the bromization reaction and oxidant on the formolation reaction of the target product were studied. The results show that the optimum solvent for the bromization reaction and the optimum oxidant for the formolation reaction of the target product were carbon tetrachloride and ceric ammonium nitrate, and their yields were 86.7% and 89.3% respectively.

同时就溴化反应中的溶剂以及甲酰化反应中的氧化剂对两类反应的影响分别进行了研究,结果表明溴化反应的最佳溶剂为四氯化碳,反应产率达到86.7%,甲酰化反应的最佳氧化剂为硝酸铈铵,产率达到89.3%。

Study on an efficient process for the preparation of trifloxystrobin starting from 2-methylacetophenone bypartial oxidation,esterification,reaction with methoxyamine,bromization and condensation with 3'- acetophenone oxime.

以邻甲基苯乙酮为原料,经过高锰酸钾的碱性氧化,甲醇酯化,再与甲氧基胺盐酸盐肟化后,用N-溴丁二酰亚胺溴化,最后和间三氟甲基苯乙酮肟缩合得到目标产物肟菌酯。

The monomer ofbromostyrene was synthesized fromβ-bromobenzene by eliminating hydrogenbromide under sodium hydrate.

溴乙基溴代苯在氢氧化钠的作用下,发生溴化氢脱除反应,得到溴代苯乙烯单体。

It was found that tribromide quaternary ammonium salt was an excellent bromide reagent, which was easy to handle and had low toxicity. The reaction can process rapidly and has high bromide rate.

研究结果表明,三溴季铵盐是一种性能优良的固体溴化剂,操作方便,对人体的危害性小,反应速度快,溴化率高。

Drug intervention groups received either daily inhalation of budesonide, ipratropine or heparin respectively, starting on the 8th day or TGF-β1 monoclonal antibody(TB21)0.5 mg twice (6th and 19th day) via the tail veinous injection.

其它各药物干预组于制作模型第8 d起分别雾化吸入布地奈德(布地奈德组,12只)、溴化异丙托品(溴化异丙托品组,12只)和肝素(肝素组,6只)溶液。4周后检测小支气管平滑肌及胶原厚度,用免疫组化法及原位杂交法观察各生长因子在支气管肺内的表达,用放免法检测血清和BALF中细胞外基质成分Ⅲ型前胶原、层粘连蛋白及透明质酸。

Flame retardant properties and mechanical properties of ABS which was incorporated into different molecular weight bromated epoxy resins flame retardant agent were evaluated.

与十溴二苯醚对比试验研究表明,添加高分子量溴化环氧树脂阻燃剂的ABS材料溴含量为7.9%时与添加十溴二苯醚阻燃剂的ABS材料溴含量为10.1%的阻燃性能相当。

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