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The originalprocedure has subsequently been replaced by milder and more environmentallyfriendly conditions. We tried to alkylate 3,4,5-trimethoxytoluene by2-allylphenylbenzyl ether in the presence of N-bromosuccinimide.

本实验是在溴代琥珀酰亚胺的作用下使2-烯丙基苯基苄基醚产生苄正离子,苄正离子亲电进攻3,4,5-三甲氧基甲苯从而进行傅氏烷基化反应的。

The effects of different PTC,reacting time,temperature,the concentration of potassium hydroxide and the bromoethane amout on the reaction were studied.

考察了不同相转移催化剂、反应时间、反应温度、氢氧化钾浓度、溴乙烷用量诸因素对2-甲基吲哚进行N-烷基化反应的影响。

In this thesis, three different chain length hybrid monomers, containing acrylate and propenyl ether group, was synthesized by three-step reaction through 1.3-propanediol, 1.4-butanediol, 1.6-hexanediol, allyl bromide and acryloyl chloride.

本文以1.3-丙二醇、1.4-丁二醇、1.6-己二醇、烯丙基溴及丙烯酰氯为主要原料,通过三步反应合成了三种不同链长的丙烯酸酯-丙烯基醚杂化单体。

More prophase and prometaphase cells may be obtained by this technique.

在培养基中加入5-溴脱氧尿嘧啶核苷使细胞同步化6—8小时,可以得到较多的前期和前中期分裂细胞。

Phosphine generally require long exposure periods, whereas methyl bromide and sulfuryl fluoride provide a rapid fumigation that can be completed in less than 4 days, often within 24 hours.

磷化氢一般需要较长的密闭时间,而溴甲烷和硫酰氟则适合快速熏蒸,可在不到4天之内完成熏蒸工作,一般在24小时内完成。

The allylation reactions of aldehydes with allyl bromide were carried out in 76%~93% yields with Nd-SnCl2-H2O under ultrasound irradiation at room temperature for 50~60 min.

在Nd-SnCl2-H2O体系中,用烯丙基溴超声诱发下进行了一系列芳香醛的烯丙基反应,室温反应50~60min得76%~93%烯丙基化产物;而不用超声波时同样体系中搅拌3~4h高烯丙基醇产率为30%~86%。

The target compound 1 was successfully prepared via esterification, reduction, bromization and cyanation processes by using L--malic acid (2), which is an inexpensive and easily available starting material. The overall yield was 56.7%.

以廉价、易得的L--苹果酸为起始原料,经酯化、还原、溴代和氰化四步反应得到目标化合物-4-氰基-3-羟基丁酸乙酯,合成总收率为56.7%。

In the hydrocarbylation reaction,bromoethane was used instead of the expensive iodoethane with the yield 90% and the cost was reduced.

在烃化反应中,以溴乙烷代替价格昂贵的碘乙烷,收率达90%,降低了生产成本。

We have the most advanced test equipment such as Bromid mass spectrum testing instrument ,Ca6+ Lumionosity testing instrument and ICP heavy metal testing instrument.

为了一个环保的地球家园,公司不惜世资引入溴合化物质谱测试仪、六价镉光度测试仪、ICP重金属检测仪等测试设备。

QN 〓PHAL,〓PHAL and 〓PHAL were quaternized by refluxing with benzyl bromide to give ligands 8, 9 and 10 respectively. 2. The chiral ligands were applied to the AD reaction of olefins with NMO as co-oxidant and PEG (400 MW) or PF〓 as reaction media.

以奎宁和奎尼定为原料分别与1,4-二氯-2,3-二氮杂萘反应制备〓PHAL和〓PHAL,然后通过〓PHAL、〓PHAL及〓PHAL与苄基溴的季铵化反应制备单季铵盐手性配体8、9和10。

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And discuss some key point of integrated management system design, include hazard identification and risk assessment and risk control in the occupational health and safety management, the measure of satisfaction target of customer, the flawlessness of law system, the integration of the integrated management system and enterprise standardization system, unify lead institution and work orgnization, integreted internal audit and integrated management review.

同时,论述了一体化管理体系构建中的几个主要问题,包括职业健康安全管理中的危险源辨识、风险评价和风险控制、顾客满意度的科学监测、法律、法规体系的完善、一体化管理体系与企业标准化体系的有机结合、统一的领导机构和工作机构、一体化的内部审核和管理评审。

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运用与浅水井相关的现有全部震波探测数据考察了深海区塔拉纳基盆地的油藏前景。

If you're huffing and puffing at any point during the run, slow down and make sure you can take deep breathes.

如果你任何时候在跑步过程中气喘如牛,降低速度并且确保你能够深呼吸。