溴化的

The measurements of self-diffusion coefficient,spin-spin relaxation and interproton distance at 318 K suggest that N,N′-bis-α,ω- alkane propane diammonium dibromide (16-3-16) quasi-global micelles are formed in the dilute solution at a concentration of 0.26 mmol/L and the head groups are in a saw-toothed form staying at the surface of the micelle to overcome the strong electrostatic repulsion force.

从自扩散系数、横向弛豫和质子距离等NMR测定参数推测，在浓度为0.26 mmol/L（318 K）的N，N′-双-α，ω-丙烷溴化铵(16-3-16)溶液中形成了近似球形的胶束，胶束表面的带正电荷的铵基极性头呈锯齿状排列以减弱分子间静电排斥力的影响。

Table 1 medical packaging materials, containers, scope of pharmaceutical packaging materials, containers, in the form of the name preparation notes plastic bottle kalidehydroandrogropholidi = 50ml material with PP, LDPE Infusion bags, kalidehydroandrogropholidi = 50ml material is PVC, polyalkene glass infusion bottle 50ml clorsulon = injection bottle kalidehydroandrogropholidi 50ml, kalidehydroandrogropholidi = 50ml-molded, control of glass bottle kalidehydroandrogropholidi kalidehydroandrogropholidi 50ml kalidehydroandrogropholidi 50ml ampule medical plastic bottle of tablets, capsules, tablets, colour.10pills glass ampoules, pills and capsules, syrup, oral solution, nanosuspensions, immunoembolization, tincture, linimentum, lotio hard PVC medicinal Tablet and capsule-plastic blister packaging PVC/PE/PVDC medicinal compound hard Tablet and capsule-plastic blister packaging Composite PVC/PVDC medicinal Tablet and capsule hard-plastic blister packaging cold metal forming hard medicinal compound tablets, capsules, suppository materials have nylon/aluminium/PVC double aluminum packaging Tablet and capsule PVC/hard LDPE medicinal compound tablets, capsules, suppository glass bottle ciinincal ciinincal ciinincal plastic bottle medicinal ciinincal medicinal eardrops plastic bottle eardrops medicinal nasal drops plastic bottle nose drops for external use liquid medicinal plastic bottle tincture, linimentum, lotio koufuye of medicinal plastic bottle syrup, oral solution, nanosuspensions, immunoembolization glass control oral bottle syrup, oral solution, nanosuspensions, immunoembolization packaging for medicine bag laminating film, puivis bletillae, feian and Tablet foil Tablet and capsule of unguentum Al fighting、smoke aluminium pipe, oculentum, puivis bletillae, Tin aerosolon, nabulization materials have aluminum, plastic valve pyritionate, nabulization stopple kalidehydroandrogropholidi 50ml, 50ml clorsulon = material bromide, CIIR synthesis of oprene 50ml clorsulon = gasket aluminium caps combination Cap koufuye falchion, kalidehydroandrogropholidi 50ml, 50ml prestrain kalidehydroandrogropholidi = potting needle kalidehydroandrogropholidi 50ml desiccant tablets, capsules, pills and aluminium bottles vinpocetione polyethylene film and bag vinpocetione b, package management and standards on the management of the drug packaging mainly has two modes: a mode of government management, such as Singapore, Indonesia adopted a market access system, United States, Canada, the European Union through the implementation of the medicine on the packaging of the strict management, that is, the drug registration, declare to use medical packaging of related materials; Government departments on the packaging manufacturer production system to carry out spot checks.

表1 药品包装材料、容器适用的范围药用包装材料、容器名称制剂形式备注塑料输液瓶注射剂≥50ml 材料有PP、LDPE 输液膜、袋注射剂≥50ml 材料有PVC、聚烯烃玻璃输液瓶注射剂≥50ml 冻干注射剂瓶注射剂0ml、注射剂≥50ml 模制、管制玻璃注射剂瓶注射剂0ml 安瓿注射剂0ml 口服固体药用塑料瓶片剂、胶囊、丸剂玻璃药瓶片剂、胶囊、丸剂、糖浆剂、口服溶液剂、混悬剂、乳剂、酊剂、搽剂、洗剂 PVC药用硬片片剂、胶囊铝塑泡罩包装 PVC/PE/PVDC药用复合硬片片剂、胶囊铝塑泡罩包装 PVC/PVDC药用复合硬片片剂、胶囊铝塑泡罩包装冷冲压成型药用复合硬片片剂、胶囊、栓剂材料有尼龙/铝/聚氯乙烯双铝包装片剂、胶囊 PVC/LDPE药用复合硬片片剂、胶囊、栓剂玻璃滴眼剂瓶滴眼剂药用滴眼剂塑料瓶滴眼剂药用滴耳剂塑料瓶滴耳剂药用滴鼻剂塑料瓶滴鼻剂外用液体药用塑料瓶酊剂、搽剂、洗剂口服液体药用塑料瓶糖浆剂、口服溶液剂、混悬剂、乳剂玻璃管制口服液瓶糖浆剂、口服溶液剂、混悬剂、乳剂药品包装用复合膜、袋散剂、颗粒剂、片剂药品包装用铝箔片剂、胶囊铝管、铝塑管软膏、眼膏剂、散剂、罐气雾剂、喷雾剂材料有铝、塑料阀门气雾剂、喷雾剂胶塞注射剂0ml、注射剂≥50ml 材料有溴化、氯化丁基橡胶合成聚异戊二烯垫片注射剂≥50ml 铝盖、铝塑组合盖口服液、注射剂0ml、注射剂≥50ml 预灌封注射针注射剂0ml 干燥剂片剂、胶囊、丸剂铝瓶原料药聚乙烯膜、袋原料药二、包装管理及标准各国对药品包装的管理主要有两种模式：一种模式是政府管理，如新加坡、印度尼西亚采取市场准入制的方式，美国、加拿大、欧盟通过对药品的管理实施对药品包装的严格管理即在药品注册时，申报所使用药品包装的相关材料；政府部门对药品包装生产企业的生产体系进行现场检查。

METHODS: Pulmonary function tests were performed in 20 children with asthmatoid bronchitis (2 months-2.5 years of age) before and 30, 60, and 120 minutes after salbutamo and ipratropium bromide inhalation. The indexes of pulmonary function measured included tidal breathing flow volume loop, percent of tidal volume to peak tidal expiratory flow, terminal flows per peak expiratory flow (25/PF), peak tidal expiratory flow, rate of mid-expiratory to mid-inspiratory flow, respiratory rate and tidal volume per kilogram. RESULTS: Before drug inhalation, the descending branch of the TBFV loop was depressed.

20例2个月至2岁6个月的喘息性支气管炎患儿，在吸入药物沙丁胺醇+溴化异丙托品前、吸入后30，60，120min各行一次潮气流速容量环检查，并进行肺功能各项指标比较，包括潮气呼吸流速容量环的形态，反映小气道功能的敏感指标到达潮气呼气峰流速时的呼气量/潮气量，呼出75%潮气量时的呼气流速/潮气呼气峰流速(25/PF)，潮气呼气峰流速，反映大气道功能的指标潮气呼气中期流速/潮气吸气中期流速，潮气呼吸状态下的通气功能，包括呼吸频率，每公斤体重潮气量。

Effect of different surfactants on the UV intensity of Al(superscript 3+)-MXFX have been studied. Is Cetyl Trimethy-lammonium Bromide can increase the UV intensity of Al(superscript 3+)-MXFX is discovered. Based on this reaction, the reaction conditions in detail and proposed a simple, rapid and sensitive new method for the determination of MXFX by UV method is inve stigated. This method has been applied for the determination of MXFX in tablet with satisfactory results.

通过研究不同表面活性剂对Al(上标 3+)-莫西沙星体系紫外特性的影响，发现十六烷基三甲基溴化铵对该体系有显著的增敏作用；系统研究了CTMAB-Al(上标 3+)-MXFX反应体系的紫外特性，利用这一反应体系，建立了简单、快速、灵敏的测定莫西沙星的紫外分光光度法，选择了最佳实验条件，并将此方法用于莫西沙星片剂的测定，结果满意。

The preparation process includes the following steps: mixing 10 mM concentration water solution of chloropalladic acid and 12.5-25 mM concentration water solution of ammonium hexadecyl trimethyl bride in the volume ratio of 1 to 20, heating to 65-95 deg.c, adding 100 mM concentration water solution of ascorbic acid in the volume ratio to the water solution of chloropalladic acid of 0.16 to 1 to react for 30 min, centrifugal separation to collect precipitate, water washing, and drying to obtain cuboidal nanometer Pd material.

该钯纳米长方体材料的制备方法的步骤和条件法如下：把体积比为1∶20的10mM氯钯酸水溶液和12.5-25mM十六烷基三甲基溴化铵水溶液混合，加热至65-95℃，然后加入与10mM氯钯酸水溶液的体积比为0.16∶1的100mM抗坏血酸水溶液，反应30分钟，将溶液离心分离，收集到的沉淀用水洗涤，干燥，得到钯纳米长方体。

To the best of our knowledge, the relationship of surface acitivity of catanionic surfactant with temperature has not been revealed, and the catanionic surfactant has not been employed in organic reaction also.In this work, surface tensions of equimolar cetyl trimethylammonium bromide-sodium dodecyl sulfate at different temperatures were determined and compared with those of corresponding individual surfactants.

为扩展复配体系的应用，本论文选取等摩尔十六烷基三甲基溴化铵—十二烷基硫酸钠复配体系及它们的单一体系为研究对象，观察到随着温度的升高，CTAB及SDS表面活性变化不大，而等摩尔CTAB-SDS的表面活性显著增强，这是由于升温减弱了其强烈的静电作用，并通过溶解性实验结果进一步证实。

The micelle shape transformation of tert-octylpheny phenol polyethylene glycol ether (TX-100), sodium dodecyl benzene sulfonate and tetradecyl trimethyl ammonium bromide in heavy water solutions was studied by 1H nuclear magnetic resonance spectroscopy, including an NMR self-diffusion experiment. These experiments showed that the surfactants formed several shapes of micelles (spherical, ellipsoidal, and rodlike) at the respective concentrations which were far above their critical micelle concentration.

运用核磁共振一维氢谱和自扩散实验方法研究了聚乙烯乙二醇异辛酚醚(TX-100)、十二烷基苯磺酸钠和十四烷基三甲基溴化铵三种不同类型的表面活性剂在重水溶液中的胶束形状转变，发现它们在临界胶束浓度以上的各自相应浓度都有胶束形状的变化（由球状转变为椭球状或棒状）。

In this paper, the improvement of synthetic method of 2-acetylaminotropone is introduced. 3-Acetyltropolone reacted with low concen-tration methylamine solution and solvent was directly evaporated in reduce pres-sure to give 2-acetyl-7 -methylaminotropone in good yield. The compound reacted with phenyltrimethylammonium tribromide to give two new compounds.

本文介绍2-乙酰基-7-甲胺基酮合成方法的改进——用挥发性小的低浓度甲胺溶液与3-乙酰基酚酮反应；和采用直接减压蒸除溶剂法分离产品，得到较好产率的2-乙酰基-7-甲胺基酮；用化合物与三溴化苯基三甲铵反应，得到两种至今未见文献报道的新化合物。

Besides, n-butyl and sec-butyl tosylate that are difficult for oxidative addition can react with phenylmagnesium bromide to form corresponding cross-coupling products. Primary alkyl halide which contains β-hydrogen and is relatively hard to undergo the reaction , n-butyl chloride for instance, can react with aryl Grignard reagents in the presence of NiB alloy as well.

此外，难以进行氧化加成的对甲苯磺酸正丁酯和对甲苯磺酸仲丁酯可以与苯基溴化镁作用生成相应的交叉偶联产物；反应相对困难的含β-H的伯卤烷，如：正氯丁烷也可以在NiB催化下与芳基格氏试剂发生偶联。

When proper amount of tetraethyl ammonium bromide is added to anode, specific energy of the battery could go up to 46.8Wh/kg.

当在电池的正极中添加适量的含四乙基溴化铵的混合添加剂时，电池的比能量高达46.8 Wh／kg。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新