溴化的

The highest ee value of 71% was achieved by using chiral molybdenum 2'-pyridingyl alcoholate complex at 0 ℃. After addition of phase transfer catalyst Bu4NBr, the yield and ee value were remarkably increased.

其中手性吡啶醇二氧合钼在0℃下的对映选择性ee值达到71%；加入相转移催化剂四正丁基溴化铵，催化剂的活性和对映选择性有显著提高，其中手性吡啶醇二氧合钨在50℃下ee值由54％提高到78%。

"To achieve such a miracle, the semiconductor industry has gone to extremes, using the world's most toxic substances like Arsine, Phosphine, Hydrofluoride, Hydrobromide and the like."

但是，为了这种"奇迹"，半导体技术也到了无所不用其极的地步，世上最剧毒的物质如砷烷(AsH3)、磷烷(PH3)、氟化氢、溴化氢，等一长串毒品全都用上。

To achieve such a miracle, the semiconductor industry has gone to extremes, using the world's most toxic substances like Arsine, Phosphine, Hydrofluoride, Hydrobromide and the like.

但是，为了这种"奇迹"，半导体技术也到了无所不用其极的地步，世上最剧毒的物质如砷烷（AsH3）、磷烷（PH3）、氟化氢、溴化氢，等一长串毒品全都用上，很快连同步加速器也要用上去了。

A novel method for palladium-catalyzed cyclotrimerization of alkynes in supercritical carbon dioxide (scCO2) has been developed.

摘要研究了以超临界二氧化碳为反应介质溴化钯催化炔烃环三聚反应的新方法。

A chiral phase transfer catalyst, N-benzyl quinine bromide, was synthesized from natural chiral compound. And 2,5-bimethyl-4-(3-nitrobenzene)-1,4-bihydrogenation pyridine-3--4-methyl formate (viz. nitrendipine) was synthesized by this chiral phase transfer catalysis, and characterized by elemental analysis, infrared spectrum,1H nuclear magnetic resornace, and X-ray single-crystal diffraction.Key words: ammonium; chiral phase transfer catalyser; crystal structure

通过对天然手性物质进行修饰合成手性相转移催化剂N-苄基溴化奎宁，并对目标分子2，5-二甲基-4-(3-硝基苯)-1，4-二氢吡啶-3-甲酸乙酯-5-甲酸甲酯进行不对称催化合成，并通过红外光谱和核磁共振氢谱对化合物进行了表征，用X射线单晶衍射法测定了该化合物的晶体结构。

Objective To observe the effect of inhaled ipratropium bromide on airway and lung tissue muscarinic receptors in a rat model of chronic obstructive pulmonary disease.

目的 观察吸入溴化异丙托品对大鼠慢性阻塞性肺疾病模型气道和肺组织M受体的影响及其规律。

A variety of aldehydes were converted into acylals in good yields with anhydride in the presence of a catalytic amount of zinc bromide under solvent-free conditions.

以醛和酸酐为原料，溴化锌为催化剂，无溶剂条件下高产率地合成了偕二酸酯（其中醛与苯甲酸酐的反应是首次报道）。

The samples from 784 patients with tuberculosis, 160 patients with lung cancer were detected by using AmpliSensor-PCR, PCR, smear and culture methods, and the results were compared.

采用AmpliSensor-PCR对784例结核病患者及160例肺癌患者的标本进行检测，并与PCR(凝胶电泳后，经溴化乙锭染色)、涂片、培养等法比较。

The samples from 784 patients with tuberculosis, 160 patients with lung cancer were detected by using AmpliSensor-PCR, PCR, smear and culture methods, and the results were compared.

采用AmpliSensor-PCR对784例结核病患者及160例肺癌患者的标本进行检测传染病，并与PCR(凝胶电泳后，经溴化乙锭染色)、涂片、培养等法比较。

0 G of cyclopentyl bromide and 19.4 g of magnesium are reacted in ether or THF to give a cyclopentyl Grignard reagent.

一百十九点零克的环戊基溴化镁和克一十九点四顷反应乙醚或四氢呋喃给予一个环戊格氏试剂。

And discuss some key point of integrated management system design, include hazard identification and risk assessment and risk control in the occupational health and safety management, the measure of satisfaction target of customer, the flawlessness of law system, the integration of the integrated management system and enterprise standardization system, unify lead institution and work orgnization, integreted internal audit and integrated management review.

同时，论述了一体化管理体系构建中的几个主要问题，包括职业健康安全管理中的危险源辨识、风险评价和风险控制、顾客满意度的科学监测、法律、法规体系的完善、一体化管理体系与企业标准化体系的有机结合、统一的领导机构和工作机构、一体化的内部审核和管理评审。

Deepwater Taranaki is investigated for its petroleum potential, using all available seismic data tied to shallow-water wells.

运用与浅水井相关的现有全部震波探测数据考察了深海区塔拉纳基盆地的油藏前景。