溴化氢的

The influence of each condition on the reaction speed and yield was studied, and the optimal conditions were: the ratio of the amount of substance of aromatic amine and heptafluoro-isopropyl iodine was 1:1.1~1.5, the amount of substance of sodium dithionite, sodium bicarbonate, aniline compounds were respectively 1.1~1.3, the amount of substance of phase transfer catalyst TBAB and aniline compounds was 0.05~0.1, the concentration of aniline compound was 0.5~1.0 mol/L, reaction temperature was 10~20 ℃, and the solvent was aether.

最佳结果为：芳胺与七氟异丙基碘的物质的量比1：1.1~1.5，连二亚硫酸钠、碳酸氢钠与苯胺的物质的量分别为1.1~1.3，相转移催化剂四丁基溴化铵与苯胺的物质的量比在0.05~0.1，溶剂总用量使苯胺浓度在0.5~1.0 mol/L；反应温度10~20℃；溶剂采用乙醚。取代基供电子性越强，反应时间越短，产率越高；氨基的对位优先反应，氨基的邻位较难发生反应；且七氟异丙基总是优先取代在芳环电子云密度较高的位置上。

It is anticipated that most treatments conducted to meet the regulatory requirements will employ methyl bro mide fumigation , although some other fumigants such as phosphene, or a number of preservatives, may be employed.

尽管可以使用一些其他熏蒸剂如磷化氢或多种防腐剂，但期望大多数为满足这些强制性要求的处理采用溴甲烷熏蒸。

The effects of different PTC,reacting time,temperature,the concentration of potassium hydroxide and the bromoethane amout on the reaction were studied.

考察了不同相转移催化剂、反应时间、反应温度、氢氧化钾浓度、溴乙烷用量诸因素对2－甲基吲哚进行N－烷基化反应的影响。

Phosphine generally require long exposure periods, whereas methyl bromide and sulfuryl fluoride provide a rapid fumigation that can be completed in less than 4 days, often within 24 hours.

磷化氢一般需要较长的密闭时间，而溴甲烷和硫酰氟则适合快速熏蒸，可在不到4天之内完成熏蒸工作，一般在24小时内完成。

Novel sodium 2-2-(alkylaryloxy-alkylamidoethanesulfonates (m+nAr-T, m, n: carbon numbers; Ar: aromatic nucleus; T: taurine) with high purity were synthesized through bromization, esterification, Fries rearrangement, Pd-catalyzed hydrogenation, Williamson reaction, and acylation, et al, using carboxylic acid, phenol and taurine as starting materials. The structures and purities were characterized.

以羧酸、苯酚和牛磺酸为原料，通过溴代反应、酯化反应、Fries重排反应、催化氢化反应、Williamson反应以及催化酰胺化反应等过程，首次成功合成并表征了系列结构明确的高纯度N-酰基牛磺酸钠(m+nAr-T，m、n为烷基链碳数，Ar为芳环，T表示taurine)。

The uniform nano-sized titanic oxide mesoporous thin film which can be coated repeatedly was prepared by adding tetrahydrofuran which acts as dispersant to micro-emulsion system consisting of water,cyclohexane,hexadecyl trimethyl ammonium bromide and butyl alcohol.

通过在水、环己烷、十六烷基三甲基溴化铵、正丁醇4组分构成的微乳液体系中加入起分散作用的四氢呋喃，制备出均匀、可重复成膜的纳米氧化钛介孔薄膜。

20% Hydrobromic acid was selected as the optimum condition for O-demethyltion. A total yield raised 59.90% was obtained.

采用20%的氢溴酸作为去氧甲基化试剂的新工艺，收率高、成本低、操作简便，适合规模生产。

The micelle shape transformation of tert-octylpheny phenol polyethylene glycol ether (TX-100), sodium dodecyl benzene sulfonate and tetradecyl trimethyl ammonium bromide in heavy water solutions was studied by 1H nuclear magnetic resonance spectroscopy, including an NMR self-diffusion experiment. These experiments showed that the surfactants formed several shapes of micelles (spherical, ellipsoidal, and rodlike) at the respective concentrations which were far above their critical micelle concentration.

运用核磁共振一维氢谱和自扩散实验方法研究了聚乙烯乙二醇异辛酚醚(TX-100)、十二烷基苯磺酸钠和十四烷基三甲基溴化铵三种不同类型的表面活性剂在重水溶液中的胶束形状转变，发现它们在临界胶束浓度以上的各自相应浓度都有胶束形状的变化（由球状转变为椭球状或棒状）。

In this project, we have prepared conveniently Si-Mg 1,1-difunctional group reagents-α-silylvinyl Grignard reagents by hydromagnesiation of alkynylsilanes; Se-Br 1,1-difunctional group reagents-α-bromovinylselenides by hydrobromination of alkynylselenides; Sn-Br and Sn-I 1,1-difunctional group reagents by hydrozirconation of alkynylstannanes followed by halogenating reaction.

本项目通过炔基硅烷的镁氢化反应，方便地制得了Si-Mg 1，1-双官能团试剂-α-硅基烯基镁化物；通过炔基硒醚的溴氢化反应，方便地制得了Se-Br 1，1-双官能试剂-α-溴代烯基硒醚；通过炔基锡烷的锆氢化反应，继而卤代方便地制得了Sn-Br和Sn-I 1，1-双官能试剂。

0 G of cyclopentyl bromide and 19.4 g of magnesium are reacted in ether or THF to give a cyclopentyl Grignard reagent.

一百十九点零克的环戊基溴化镁和克一十九点四顷反应乙醚或四氢呋喃给予一个环戊格氏试剂。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新