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溴化作用

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Objective:To observe the effect of aerosol inhalation of β 2 receptor stimulant combined with anticholinergic in treating asthma attack.

目的 :观察β2 受体激动剂硫酸特布他林和抗胆碱能药物溴化异丙托品联合雾化吸入治疗哮喘急性发作的作用。

Bromopropane is produced from hydrogen bromide and propene in the presence of catalyst by free radical addition process.

丙烯与溴化氢在催化剂作用下,进行自由基加成反应生产1-溴丙烷。

In the medium of H_2SO_4 and catalyzed by potassium bromide, iodate can oxidize and decolorize methyl orange very well.

基于硫酸介质中,碘酸根在溴化钾的催化作用下对甲基橙有较好的氧化褪色作用。

Sodium fatty alcohlo ether sulfate, S-80, fatty alcohol-polyoxyethylene ether and S-60 resulted in slow photodecomposition of rotenone in aqueous solution revealing a photo-extinction effect, sodium dodecylberzenesulfonate, tween-60, hexadecyl trimethyl ammonium bromide and poyl vinyl pyrrolidone made the photolysis of rotenone in aqueous solution fast showing an obvious photosensitized effect.

室内条件下研究了鱼藤酮水溶液存在不同表面活性剂时,鱼藤酮的紫外光降解,结果表明:脂肪醇聚氧乙烯醚硫酸钠、司本-80、长链脂肪醇聚氧乙烯醚和司本-60对鱼藤酮在水溶液中的光解速率表现出显著的光猝灭降解效应;十二烷基苯磺酸钠、吐温-60、十六烷基三甲基溴化铵和聚乙烯吡咯烷酮对鱼藤酮在水溶液中的降解表现出一定程度的光敏化作用。

A process for preparingp-fluo-2-(2-methyl-3-propionyl)-4-oxy-N,3-diphenyl-phenylbutylamide includes such steps as Friedle-Craft acylating of newly prepared phenylacetyl chloride and fluorobenzene under catalysis of AlCl3 to obtain 4-fluoro-phenylbenzyl ketone, brominating at carbonyl alpha position under catalysis of less AlCl3 to obtain alpha-bromo-4-fluo-phenylbenzyl ketone, and condensing with isobutyryl acetanilide under action of sodium ethoxide.

本发明涉及一种制备对氟-2-(2-甲基-3-氧丙基)-4-氧-N,3-二苯基-苯丁酰胺(1)的方法,其包括以下步骤:新制的苯乙酰氯与氟苯在AlCl3催化下进行Friedle-Craft酰化反应,得到对4-氟-苯基苄基酮(4);化合物(4)在少量AlCl3催化下进行羰基α位溴化,得到α-溴-4-氟-苯基苄基酮(5);然后(3)异丁酰乙酰苯胺在乙醇钠作用下与化合物(5)进行缩合。

In the presence of alkalinity and tetraethyl ammonium bromide, 2,4-dihydroxy benzophenone reacts with allyl glycidyl ether to form an ethylenic derivative of benzophenone, 2-hydroxy-4-(β-hydroxy-γ-allyloxy) propyloxy benzophenone, which can further undergo hydrosilylation with polyhydromethylsiloxane.

在相转移催化剂四乙基溴化按作用下,利用2,4-二羟基二苯甲酮与烯丙基缩水甘油醚在碱性水溶液中的开环加成反应,合成了中间体4-丙氧基-2-羟基二苯甲酮,将其进一步与聚甲基氢硅氧烷进行硅氢化加成反应。

Formylation and diformylation of dithieno [2,3-b:3',2'-d] thiophene were prepared by two methods. Firstly, aromatic carbanions were prepared by 1 Br/Li exchange of bromo dithieno[2,3-b:3',2'-d]thiophene with n-BuLi in THF at low temperature; 2 deprotonation of dithieno[2,3-b:3',2'-d]thiophene with LDA.

二噻吩并[2,3-b:3',2'-d]噻吩单醛与双醛的制备首先通过两种方法产生芳基负离子:1溴代并三噻吩在四氢呋喃中与正丁基锂发生的溴锂交换;2用LDA对二噻吩并[2,3-b:3',2'-d]噻吩去质子化作用。

Surfactants of Hexadecyl trimethyl ammonium bromide and alkyl polyoxyethylene have a slow dying at a higher temperature and have accelerated dying at a lower temperature while leather dying with the curcuma dye.

而表面活性剂十六烷基三甲基溴化铵及平平加O对姜黄素在皮革的染色在较低温度下有一定的促染作用,在较高温度下有一定的缓染作用。

Methods n-Cetyl-l-thio-β-D-galactoside was synthesized by a series of reaction from galactose and incorporated into Small Unilamellar Vesicles which was prepared by sonication at the ratio for L-α-PC∶Chol∶L-α-PE as 7∶2∶1, with or without 10 mol%Cetyl-gal.

半乳糖经乙酰化、溴化、缩合、亲核取代反应制备半乳糖新糖脂质并与其他脂质制备脂质体,在二氯化锡还原作用下用99mTc标记脂质体,进行动物体内靶肝实验,用γ计数器检测各脏器放射性,计算摄取率。

Then, it was condensed with-valine methyl ester to form a chiral imine, which was reacted with allyl zinc bromide in the presence of CeCl3·7H2O to afford the corresponding chiral homoallylic amine with high optical activity.

-N-Boc-3-苯基-2-氨基丙醛与-缬氨基酸甲酯缩合生成手性亚胺,在七水合三氯化铈(CeC13·7H2O)催化以及底物的手性诱导作用下,该手性亚胺与烯丙基溴化锌经不对称加成反应合成了高光活性的单烯丙基化手性胺。

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