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The preparation process includes the following steps: mixing 10 mM concentration water solution of chloropalladic acid and 12.5-25 mM concentration water solution of ammonium hexadecyl trimethyl bride in the volume ratio of 1 to 20, heating to 65-95 deg.c, adding 100 mM concentration water solution of ascorbic acid in the volume ratio to the water solution of chloropalladic acid of 0.16 to 1 to react for 30 min, centrifugal separation to collect precipitate, water washing, and drying to obtain cuboidal nanometer Pd material.

该钯纳米长方体材料的制备方法的步骤和条件法如下:把体积比为1∶20的10mM氯钯酸水溶液和12.5-25mM十六烷基三甲基化铵水溶液混合,加热至65-95℃,然后加入与10mM氯钯酸水溶液的体积比为0.16∶1的100mM抗坏血酸水溶液,反应30分钟,将溶液离心分离,收集到的沉淀用水洗涤,干燥,得到钯纳米长方体。

We devote in the research, development, production and marketing of precious metal compound and related products with reliable quality, such as; potassium gold noncyanide, Rhodium sulphate, potassium tetrabroaurate, Chloroplatinic acid, gold chloride, Ammonium chloropalladate, Ammonium tetrachloropalladate, recycled and refined precious metals etc.

公司主要从事贵金属材料相关产品的研究、开发、生产和销售,主要产品有无氰金盐和其他贵金属化合物,包括:硫酸铑、金酸钾、氯铂酸、三氯化金、二氯化二氨络钯、二氯化四氨络钯等,并提供贵金属资源二次回收服务。

The apparent enlargement of the ventricles seen here is due to atrophy of the head of the caudate from neuronal loss with Huntington's disease, an autosomal dominant condition characterized clinically by choreiform movements.

明显的脑室扩张是因为Huntington病时二乙基乙酰胺丧失使尾状核头萎缩,常染色体显性遗传,临床上伴有典型的舞蹈症。

In the presence of CPB, the chromogenic reaction of V with DPCO has been studied.

研究在化十六烷基吡啶存在下,钒与二苯偶氮羰酰肼显色反应的分析特性。

Anthraquinone is prepared by the liquid phase oxidation of anthracene with oxygen in the presence of cobaltous salt,manganous salt and bromide.

在液相中,钴盐、锰盐、化物催化氧气氧化蒽制取蒽醌,当压力为0.5~0.8 MPa,溶剂是芳香性卤代烃和丁酸的混合物(其中丁酸质量分数为15%~20%)时,蒽醌的产率可达90%,纯度99.2%。

In the ammonifying procedure, al cohol is used as solvent or phase transfer catalyst is added. The results sh ow that the reaction time decreases evidently and the yield of bactericide in creases further.

在产品制备的胺化步骤,作者采用乙醇作为溶剂或加入相转移催化剂,明显缩短了合成时间,使产品双烷基二甲基化铵的产率得到了进一步提高。

The results showed that,polybromostyrene has higher thermal stability than the congeneric products in the market .

结果表明:文中合成的聚化苯乙烯比市场同类产品具有更优异的热稳定性。

Raman spectrum, UV-Vis spectra, IR, NIR and XPS spectra were used to characterize the material. The result indicates that there is a conjugative effect between MWNT and bromine, which induces the change of electron distribution on the MWNT surface. It increased the car- rier density and the electrical conductivity of MWNT became higher.

通过拉曼光谱,紫外可见光谱,红外吸收光谱,近红外吸收光谱和X光电子能谱等方法研究,结果表明:与多壁碳纳米管之间存在共轭作用,使多壁碳纳米管表面的电子云分布发生了变化,导致空穴载流子的产生,增加了载流子浓度,提高了多壁碳纳米管的导电性能。

Objective to evaluate the functional recovery of acute spinal cord injuried rats treated with exogenous wnt-3a signal protein administration and to explore its mechanism.methods moderate spinal cord contusion injury was made in 40 adult sprague dawley rats at t10.twenty rats served as contusion controls(group 1).twenty rats were treated with wnt-3a for three days after injury (group 2).the functional recovery of the rats was observed through basso,beattie,bresnahan open field locomotor score.rats were killed at 14 or 28 days after injury,then spinal cords were removed for histopathological examinations,and the expression of the bromodeoxyuridine plus neural cell markers was stained with immunohistochemical method.results rats of two groups receiving a contusive injury recovered substantial function within 1 week.by 28 days,rats in groups 2 scored 7.0 points better on the bbb scores than rats in group 1 group 2=16.94,after 28 days vs.

目的 研究外源性wnt-3a信号蛋白对脊髓损伤的修复作用,并探讨其作用机制。方法取40只成年雌性sd大鼠在t10节段制备适度脊髓挫伤模型。随机从中取20只为损伤对照组(group 1),另外20只为损伤治疗组(group 2)。脊髓损伤3天后用wnt-3a蛋白治疗。这些大鼠的功能恢复通过basso、beattie、bresnahan开放视野运动评分来观察。这些大鼠分批在损伤后14天或28天被处死,取出损伤节段脊髓用来组织病理学检查,同时用5-脱氧尿嘧啶核苷和神经细胞标记物进行免疫组化染色。结果两组大鼠在伤后一周运动功能有明显的恢复。不过,到损伤后28天,我们观察发现,损伤治疗组中的大鼠bbb评分比损伤对照组中的评分高出7.0分左右(group 2∶16.94±1.18,group 1∶9.89±1.29;p.05),光镜和电镜检查发现wnt-3a蛋白对髓鞘形成和轴突再生有一定的修复效果。

An unusual intramolecular nucleophilic reaction of α carbon anion of crotonate was discovered and the imidazo[1,5 a ]pyridine derivatives were sythesized with a novel tandem reaction.

发现 5 咪唑甲醛(1)与γ代巴豆酸酯(2 )在弱碱条件下首先进行亲核取代反应生成 3,继而生成γ碳负离子并转移到α位,然后进行分子内亲核进攻成环、脱水生成 4的串联反应。

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