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acute of disease of lung of sex of 58 chronic block is aggravating period the patient is divided randomly for hydrochloric acid ammonia bromine alls alone remedial group and groovy treatment group each 29, two groups all give absorb oxygen, fight infection, smooth asthma, correct agent of spasmolysis of soda acid unbalance, bronchus and whole body or local application the convention such as coriaceous hormone treats candy integratedly, group of treatment of all alone of bromine of hydrochloric acid ammonia is added on groovy cure foundation all alone with bromine of hydrochloric acid ammonia drop of vein of inject fluid 30mg(100ml) is noted, 1 ~ 2 / D, period of treatment 7 ~ 14d.

方法58例慢性阻塞性肺疾病急性加重期患者随机分为盐酸氨索治疗组和常规治疗组各29例,两组均给予吸氧、抗感染、平喘、纠正酸碱失衡、支气管解痉剂及全身或局部应用糖皮质激素等常规综合治疗,盐酸氨索治疗组在常规治疗基础上加用盐酸氨索注射液30mg(100ml)静脉滴注,1~2次/d,疗程7~14d。

In this paper, through a series of experiments, two series of quaternary-ammounium Gemini surfactants were synthesized, namely the pair alkylene double quaternary ammonium salt surfactant m-s-m·2Br and the pair the alkylene double quaternary ammonium salt surfactant -s-·2Br. We has carried on the attribute with the infrared spectrum to its structure, and to affected the factor which the synthesis pair the alkylene double quaternary ammonium salt surfactant responded to carry on the discussion. We has discovered the synthesis pair the ethylene double quaternary ammonium salt surfactant m-2-m·2Br optimum condition: The bromo alkane and a tetramethyl ethylene diamine mole of ratio is 3.0: 1.0, makes the solvent by the ethyl alcohol, 80℃ under responds for 48 hours in the backflow temperature; Synthesis pair alkylene double quaternary ammonium salt surfactant 12-S-12 ·2Br optimum condition: 12 tertiary amine and 1, 3- propylene dibromide (1, 4- two bromines butane) a mole of ratio is 2.2: 1.0, makes the solvent by the ethyl alcohol, responds for 48 hours in the constant temperature 80 ℃ under backflow.

本文通过一系列的实验,合成了两个系列的Gemini型表面活性剂,即双烷撑双季铵盐表面活性剂m-s-m·2Br和双烷撑双季铵盐表面活性剂-s-·2Br,用红外光谱对其结构进行了表征,并且对影响合成双烷撑双季铵盐表面活性剂反应的因素进行了讨论,找出了合成双乙撑双季铵盐表面活性剂m-2-m·2Br的最佳条件:代烷与四甲基乙二胺的摩尔比为3.0:1.0,以乙醇作溶剂,在回流温度80℃下反应48小时;合成双烷撑双季铵盐表面活性剂12-s-12·2Br的最佳条件:十二叔胺与1,3-二丙烷(1,4-二丁烷)摩尔比为2.2:1.0,以乙醇作溶剂,在恒温80℃下回流反应48小时。

Results: The detection limites of chloroform, bromodichloromethan, dibromochloromethane and bromoform were blow 1μg/ml.

结果:三氯甲烷、一二氯甲烷、二一氯甲烷和仿最低检出浓度<1μg/L。

Also, the type of dispersion of four gasliquid-liquid systems: air-decane-aqueous solution of sodium sulfite and surfactant, airmixture of decane and dodecene-aqueous solution of rhodium complex, ligand, and surfactant, air-mixture of decane, dodecene and tridecyl aldehyde-aqueous solution of rhodium complex, ligand and surfactant, and air-mixture of decane and dodeceneaqueous solution of trisodium salt of tri (m-sulfophenyl) phosphine, and surfactant is determined by electric conductivity.

本文采用电导率测量的方法实验研究了空气—正癸烷—亚硫酸钠和十六烷基三甲基化铵水溶液、空气—正癸烷和1-十二碳烯混合物—铑膦络合物催化剂和十六烷基三甲基化铵水溶液、空气—正癸烷、1-十二碳烯和十三醛混合物—铑膦络合物催化剂和十六烷基三甲基化铵水溶液、空气—正癸烷和1-十二碳烯混合物—三间磺化苯基膦三钠盐和十六烷基三甲基化铵水溶液四个三相体系的液液分散特性。当有机相与水相体积比分别为7/3、1/1和3/7时,前三个体系均形成水包油型分散,并有稳定的乳状液生成。

A new process for the preparation of 5-bromo-vanillin with vanillic aldehyde as raw material,AlBr3 as activator,HBr and H2O2 as brominating agent and anhydrous alcohol as solvent was developed in this paper.

摘 要:以甲基香兰素为原料,氢酸与过氧化氢为化剂,化铝为催化剂,无水乙醇为溶剂制备5-香兰素。

The interfaces electric circuit and the control program can be transplantated to other micro voltage control equipment very easily.Then we take the C_2H_5Br and the hydrogen (H_2) as the source gas to deposite the gradient bromating amorphous hydrogenated carbon film in the improved low-pressure plasma polymerization unit.

然后在改进的低压等离子体聚合装置中以乙烷(C_2H_5Br)和氢气(H_2)为源气体沉积了掺非晶碳氢薄膜和梯度掺非晶碳氢薄膜,用Perkinelmer Lambda12型紫外/可见分光光谱仪测量了样品的透光谱,并利用透光谱计算了薄膜的光学厚度和光学带隙:利用NICOLET MX—1E傅立叶变换红外光谱仪和XSAM800型X射线光电子能谱仪分析了薄膜的化学键和结合态以及薄膜中氧碳元素比和碳元素比。

A new process for catalytic synthesis of decabromodiphenylethane was developed by brominating diphenylethane with bromine chloride and bromine solution to decrease bromine consumption and simplify post-treatment process.

开发了用氯化-溶液催化合成化二苯乙烷新工艺,以降低消耗和简化工艺过程。

When ATRP of styrene was investigated with 1-phenylethyl bromide/benzyl a,a-dibromide mixture as initiator, the GPC chromatogram shows two elution peaks and the molecular weighs of the peaks are approximately in a 2/1 ratio. It suggests that benzyl dibromide is a difunctional initiator of ATRP of styrene. The analysis of end group using 1H-NMR also proves the result above.

采用1-苯基乙烷/α,α-二化苄混合引发剂进行苯乙烯的ATRP反应时,所得聚苯乙烯的GPC谱图为双峰,分子量相差一倍,初步证明了α,α-二化(来源:ABf399C论文网www.abclunwen.com)苄引发苯乙烯ATRP反应时是双官能引发剂,并用~1H-NMR对聚合物结构进行分析,进一步证明了α,α-二化苄引发苯乙烯ATRP时是双端同时增长的。

With a twin-screw extruder to prepare polypropylene / 8 ether bromide pellet, and injection molding into sheet samples, quantitative analysis of different PP / 8 the sample surface, eight bromine bromine ether ether precipitation changes with time, Using X-ray photoelectron spectroscopy on the sample surface concentrations of bromine atoms ...

用双螺杆挤出机制备了聚丙烯/八醚粒料,并注塑成片状样品,定量测定了不同PP/八醚样品表面上八醚析出量随时间的变化,用X-射线电子能谱对样品表面的原子浓度。。。

N-methylmaleimide was prepared by using dimethyl sulfate as methylation reagent.The paper investigated the addition of N-methyl-3,4-dibromomaleimide and indolylmagnesium bromide,and then 2-bromo-3-(1H-indolyl-3-yl)-N-methylmaleimide and 3,4-bis(1H-indolyl-3-yl-)-N-methyl-maleimide were obtained.

对吲哚在乙烷和镁作用下生成吲哚化镁,而后与3,4-二-N-甲基马来酰亚胺的加成反应进行了研究,合成了2--3-(1H-吲哚-3)-N-甲基马来酰亚胺,并对反应条件进行了改进,研究了反应温度和原料配比对反应的影响。

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