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It is based on the facts that in the presence of sulfuric acid and sodium dodecyl benzene sulfonate, vanadium activated by vitamin C can catalyze potassium bromate to oxidize safranine O, the oxidation products of safranine O can emit intense and stable fluorescence on nitrocellulose membrane.

基于在硫酸介质和十二烷基苯磺酸钠存在下，抗坏血酸活化钒催化溴酸钾氧化番红花红O发射强而稳定的荧光的特性，建立了ⅤC活化溴酸钾氧化番红花红O催化荧光法测定痕量钒的新方法。

P-Bromobenzaldehyde was synthesized from p-bromotoluene by direct oxidation with manganese sesquioxide The factors affecting the yields of p-bromobenzaldehyde were investigated.

用三氧化二锰直接氧化法将对溴甲苯氧化对溴苯甲醛，讨论了合成过程中影响产率的各种因素，确定反应的优化条件为温度338K，硫酸的浓度7.5mol/L，三氧化二锰1.8g，产率可达73.89%。

OBJECTIVE To establish a new method for determining the levels of benzalkonium bromide and sodium nitrite in benzalkonium bromide solution.

目的 建立苯扎溴铵消毒液中苯扎溴铵和亚硝酸钠含量的测定方法。

A series of 5-bromopyrimidinyl-containing new sulfonylureas have been synthesized through bromination of 2-amino-4-methyl pyrimidine, followed by further modification and then coupled with sulfonyl isocyanate.

通过2-氨基-4-甲基嘧啶溴代反应以及进一步的衍生、磺酰基异氰酸酯的胺解，合成了一系列含有5-溴嘧啶基的新磺酰脲。

The results showed that It was feasible to sulfurize hydrotreating catalyst by acidity gas. The bromine number was still less than 0.5gBr_2/100g when the concentration of CO_2 was up to 1.5 times concentration of H2S.

实验证明：酸性气作硫化介质对加氢催化剂进行干法硫化是可行的，当CO2浓度达到H2S 浓度的1.5 倍时，溴价仍满足工业溴价小于0.5 gBr2/100g 的要求。

Ambient conditions that include toxic gases such as hydrogen sulfide, sulfurous acid, nitrous acid, chlorine, bromine, methyl bromide, ammonium, etc.

b 周围环境中有氢化硫、亚硫酸、亚硝酸、氯气、溴气、溴化甲烷、氨气等有毒气体。

Methods Naloxone was synthesized starting from oxidation of thebaine, followed by hydrogenation, acylation, cyanidation, O-demethylation, hydrolyzation and N-allylation. The alternative method of O-demethylation, methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

在以蒂巴因为原料，经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中，分别采用甲磺酸／DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

In the process of laboratory study, oxycodone was prepared by oxidating thebaine at 6,14-position under oxydol, hydrodeoxidizing 7,8-position double bond and 14-position ether under palladium catalyst. Furthermore, N-methyl of oxycodone was isolated byα-chloro-ethyl chloroformate under anhydrous condition and protection of 14-position hydroxyl to obtain noroxycodone, which was further converted into methylnaltrexone by N-alkylation in presence of cyclopropyl bromomethane, then by isolating 3-position methyl of methylnaltrexone under boron tribromide, becoming hydrochloride to prepare target compound, natrexone hydrochloride.

实验室工艺方面，本文首先用双氧水氧化蒂巴因的6-位和14-位、在钯炭催化下加氢还原7-8位双键和14-位醚合成羟考酮，然后提出并优化了在无水和14-位保护的情况下，用氯甲酸-α-氯乙酯脱去羟考酮的N-位甲基合成去甲羟考酮，再用环丙甲基溴将去甲羟考酮的N-位烷基化合成甲基纳曲酮，最后采用三溴化硼脱去甲基纳曲酮的3-位甲基和成盐酸盐合成盐酸纳曲酮。

C. I. Reactive blue KN-R, Alizarin brilliant green G and Hostlam blue R could not be degraded by Zoogloea HP3. Furthermore, ABAS degradation was regressed under the exisitence of the above dyes. 1-Aminoanthraquinone-2sulfonic sodium, 1, 4-dihydroxylanthraquinone-2-sulfonic sodium, 1, 4, 5, 8tetrahydroxylanthraquinone, anthraquinone, aniline, phenol, catechol and ophthalic acid could be degraded by Zoogloea HP3. Aniline was the most degradable substrate among ABAS, aniline, phenol, catechol and o-phthalic acid. However, benzenesulfonic sodium and p-amino benzenesulfonic sodium were not degraded by it.

动胶菌HP3不能降解活性艳蓝KN-R、弱酸性绿GS及毛用活性蓝HW-R等蒽醌型染料，且染料的存在对菌体降解溴胺酸有不同程度的抑制作用；动胶菌HP3可以降解1-氨基蒽醌-2-磺酸钠、1，4-二羟基蒽醌-2-磺酸钠、1，4，5，8-四羟基蒽醌、蒽醌及苯酚、邻苯二酚、苯胺、邻苯二甲酸等苯系化合物，而不降解苯磺酸钠、对氨基苯磺酸钠；在溴胺酸、苯酚、邻苯二酚、苯胺、邻苯二甲酸中，苯胺是动胶菌HP3的天然底物。

The distributions of BFRs in the abiological systems (such as the air and natural sediments) and in the tissues of the biological systems (such as the animals and human beings) were reviewed in this paper.

笔者就溴阻燃剂近十年来在空气、下水道淤泥和沉积物等非生命环境体系以及动物和人等生命体系的分布情况进行了综合分析，结果发现溴阻燃剂在非生命和生命环境体系中均有增加的趋势。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。