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Phase transfer catalyst;Third liquid phase;Solvent effect;Sodium phenolate;Tetrabutylammonium bromide;Butyl bromide

中文关键字相转移触媒;第三液相;溶剂效应;酚化钠;化四丁基铵;正丁烷

As the second part of a series of studies on the synthesis of 2-phenoxyisobutyric acid ethyl ester by tri-liquid-phase catalysis, this work examines the factors affecting the reaction between 2-bromoisobutyric acid ethyl ester and sodium phenolate with tetra-n-butylammonium bromide as a phasetransfer catalyst.

本文为以三液相催化技术合成2-苯气基异丁酸乙酯之研究系列的第二部份,主要在探讨各变因对以化正四丁基铵为相间转移触媒,催化2-异丁酸乙酯与酚化钠(NaOPh,水相亲核试剂)反应的影响。

Add 32 grams of potassium bromide and 0.8 gram potassium iodide to the gelatin solution and stir until dissolved.

溶解化钾和碘化钾:将32克化钾和0.8克碘化钾放入凝胶溶液,并不断搅动直到溶解。

Bromobutane was synthesized from potassium bromide and n-butyl alcohol by adding concentrated sulfuric acid in water. Various affecting factors were investigated.

化钾、正丁醇为反应原料,水为溶剂,滴加浓硫酸合成代正丁烷。

Bromooctane was synthesized from potassium bromide(by-product of synthesizing 2-hydroxy-4-octyloxybenzophenone) and n- octanol using concentrated sulfuric acid as a catalyst.

以生产2-羟基-4-正辛氧基二苯甲酮的副产物化钾和正辛醇为原料,浓硫酸为催化剂,合成了代正辛烷。

Benzyl bromide was synthesized from potassium bromide ,a by-product from synthesis of 2-hydroxy-4-n-octyloxybenzophenone(UV-531),and benzoic alcohol in the presence of concentrated sulfuric acid.

化钾作为工业生产2-羟基-4-正辛氧基二苯甲酮的副产品,在浓硫酸存在的条件下,与苯甲醇进行反应合成苄基

Methods The mercury in urine, which is the total amount of inorganic mercury in urine, including those produced from organic mercury after treated by potassium bromate and potassium bromide, is determined by atomic absorption spectrophotometer after reduction into mercury atom with sodium borohydride.

方法]尿样中汞(尿中无机汞和经酸钾-化钾处理尿中有机汞生成的无机汞之和)以硼氢化钠还原生成汞原子蒸气,用原子吸收光谱仪测定其汞的含量。

Pd combined with tetrabutyl ammonium bromide and potassium bromide into a ternary ion association precipitate in the aqueous solution. The precipitate was floated well on the surface of water phase to make a distinct boundary layer between liquid and solid phases.

在水溶液中,钯与化钾和四丁基化铵形成不溶于水的三元离子缔合物,此三元离子缔合物浮于盐水相上层形成界面清晰的液-固两相。

A novel catalytic resonance light scattering method for the determination of traces of formaldehyde in blood plasma was developed. It was based on the fact that potassium bromate reacted with pyronine Y to form association nanoparticles which gave stronger resonance light scattering effect, and formaldehyde can catalyze potassium bromate oxidizing pyronine Y resulting in decreasing of the intensity of resonance light scattering in sulfuric acid.

在稀硫酸介质中,酸钾与吡啰红Y能聚集成较大粒径的纳米微粒而使共振光散射增强,而甲醛能催化酸钾氧化吡啰红Y而导致体系共振光散射减弱,据此建立了一种灵敏、简单、快速测定血浆中痕量甲醛的新方法。

This is caused by the intercalation of MB to DNA bases which restricts the rotational motion of MB.

化乙锭的存在使MB-DNA体系的荧光强度增强,这是由于化乙锭与MB竞争结合DNA而使MB与DNA的结合反应向左移动,溶液中游离MB浓度增加了的缘故。

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We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。

This is not paper type of business,it's people business,with such huge money involved.

这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。