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A novel method for the synthesis of α-bromo acetophenone s by the reaction of 1,3-dibromo- 5,5-dimethylhydantoin with p-toluenesulfonic acid in methanol at 20~60 ℃ was described.

报道了使用1,3-二-5,5-二甲基海因和对甲苯磺酸在甲醇中和20~60℃的温和条件下合成α-代苯乙酮的新方法。

2 The analysis step by 25.0mL sample lixivium, moved in the direction of arsenic in the bottle, plus 10 ml of hydrochloric acid and 10 ml of potassium iodide solution and 5 drop acid stannochlor solution, shake the place 10min, together with 2 g of arsenic-free zinc metal, immediately mounted a good lead acetate paper turns red cotton and mercury bromide from log that arsenic tube placed in the 25-38, f μh of the dark side, remove the test strip and standard mercury bromide a color not deeper than standard.

7.2 分析步骤取25.0mL样品浸泡液,移入测砷瓶中,加5mL盐酸、5mL碘化钾溶液及5滴酸性氯化亚锡溶液,摇匀后放置10min,加2g无砷金属锌,立即将已装好乙酸铅棉花及化汞试纸的测砷管装上,放置于25~30℃的暗处1h,取出化汞试纸和标准比较,其色斑不得深于标准。

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose, Vecuronium Bromide Oteracil Potassium,Gimeracil,Cinildipine,, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl

主要产品有:异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库铵、盐酸头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、盐酸马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪盐酸盐、4--2-甲基苯甲酸。

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose,Vecuronium Bromide, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl,Oteracil Potassium,Gimeracil,Cinildipine,Manidipine dihydrochloride,Pemetrexed intermediate,Pemetrexed acid,Pemetrexed Disodium, Nisoldipine, Racecadotril, Strontium Ranelate, 1-(3-Trifluoromethylphenyl)piperazine hydrochloride, 4-Bromo-2-methylbenzoic acid.

主要产品有:异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库铵、盐酸头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、盐酸马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪盐酸盐、4--2-甲基苯甲酸。

Main products: Ifosfamide,Ifosfamide acylate,2-Deoxy-D-Glucose,Vecuronium Bromide, Ceftiofur Hcl,Ceftiofur Sodium,Buflomedil Hcl,Oteracil Potassium,Gimeracil,Cinildipine

主要产品有:异环磷酰胺、异环磷酰胺酰化物、2-脱氧-D-葡萄糖、维库铵、头孢噻呋、头孢噻呋钠、氧嗪酸钾、吉莫斯特、西尼地平、马尼地平、培美曲塞、培美曲塞酸、培美曲塞二钠、尼索地平、消旋卡多曲、雷尼酸锶、盐酸丁咯地尔、1-(3-三氟甲基苯基)哌嗪、4--2-甲基苯甲酸。

The prepared pentabromo benzyl bromide may be applied in preparing high efficiency fire retardant.

制备的五苄基可用于制备五苄基丙烯酸酯或烷基醚类聚合物用高效阻燃剂。

Polybrominated dibenzodioxins and furans were also formed from combustion of plastic masterials containing flame-retardants like aromatic and aliphatic bromine compounds .

塑料阻燃剂如代化合物在燃烧过程可导致代二苯并二恶英和代二苯并呋喃的生成。

Under the condition of 3 time mol equivalent magnesium,CuI 15mo1%, 45℃temperature and 10 hours reaction time, this preparation is notefficient to facilitate unsymmetry selenides.

我们选择苯与对甲苯在1倍镁量不同的催化剂的条件下反应,我们在光谱数据进行分析对比,可以看出只有基硒醚,并不能生成不对称有机硒醚。

And the three aspects including heat transfer area,pipe resistance and safety strength were analyzed.

以1台制冷量为35kW的冷机为例,对采用塑料传热管的冷机与传统铜管冷机相关部件的参数进行比较。

No single substance can completely replace methyl bromide at present. The current situation and application of alternatives in abroad and domestic were summarized.

由于用于土壤消毒的甲基会有30%~85%的总用量进入大气,而甲基又是一种消耗臭氧层物质,因此在1992年哥本哈根会议上,甲基被列为受控制物质。

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