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The sample was digested by high-pressure vessel with HNO3/H2O2 as the solvent. By measuring 200Hg/202Hg abundance ratio and adding quantity of the spike, the content of Hg was determined. Moreover, the uncertainty of results were also analyzed and evaluated.

样品处理采用高压密封焖罐酸溶样技术,将样品与202Hg稀释剂混合,通过所加稀释剂的量和测量混合样品中200Hg/202Hg的丰度比,准确计算出样品中Hg元素的含量,同时对测量结果的不确定度进行分析和评定。

When the sodium lauryl sulfate and p-octyl polyethylene glycol phenyl ether is used and its level in 3% and 6: 4 ratio, the polymerization process has the lowest coagulum and the highest monomer conversion. Higher reaction temperature and more level hydroxyl value lead to more coagulum, the latter also lead to larger particle size. The acid value has larger influence on viscosity and coagulum, there exist a best range. The emulsion particle size is larger for its hydrophilicity, most of its particles are connected together.

在含较高亲水单体的乳液聚合体系中,难以制得稳定的预乳化液,不能采用工业生产中常用的预乳化工艺,而只能采用混合单体直接滴加的方法;由于单体混合物的亲水亲油值较高,用阴离子型乳化剂十二烷基硫酸钠和非离子型乳化剂聚乙二醇辛基苯基醚混合,用量为单体总量的3%,且比例在6:4时,乳液聚合时具有最低的凝聚物含量和最高的单体转化率;乳液聚合反应温度升高,可以提高单体转化率,增加反应速度,但凝聚率相应提高;随着羟基单体含量的增加,聚合过程中凝聚率增加,聚合物乳胶粒平均直径增加;羧基单体有一个最佳的用量(2.6%),过高或过低凝聚率均提高;羧基含量对乳液的粘度有较大的影响,当羧基含量较低时,羧基含量增加,乳液粘度增加明显;含羟基乳液粒子由于含亲水基团较多,使得乳胶粒径增大,乳胶粒子大多数互相凝聚在一起,处于凝聚态。

We get the vary rules of mechanics character, study the dilatability and fractal characters of shear surface, analyzed the distortion manner of different kinds mixture, we build the forecast model though test results, while the results are generally same by different test ,so we can use the model to preestimate the mechanics index of mixture quickly.

本文通过试验研究了土石混合料力学特性随岩性、含石量、密实度及颗粒最大粒径等影响因素的变化规律,分析了土石混合料的剪胀性能、剪切面的起伏特征和分形特征、土石混合料的剪切变形破坏方式,经比较现场试验、室内试验及数值模拟的结果基本一致,并依据试验结果建立了不同类别土石混合料力学特性指标的预测模型,可通过模型快速预测不同类型土石混合料的力学特性指标。

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The pugging process experiment of silica brick pug was made in Φ1 600×450 wet pan mill to study the change rule of main component mixing homogeneity and molding performance of the pug. The results showed that the pervasion and mixing concurred when diversified materials acceded to the wet pan mill, prolonging time in dry-mixed and wet-mixed periods had no action for increasing mixing homogeneity with pugging time prolonging, the molding performance was improved and the porosity of silica brick adobe had downtrend, but prolonging time after pugging 14 min the effect was not remarkable.

通过对Φ1 600×450湿碾机混练硅砖泥料过程中泥料主要成分的混合均匀度、泥料成型性能的变化规律研究,发现在各种物料加入湿碾机时,同时存在着扩散混合作用,延长干混、湿混阶段的时间,对于提高混合均匀度实际上没有意义;随捏练时间延长,泥料成型性能改善,砖坯气孔率呈下降趋势,但捏练14 min以后继续延长捏练时间,采用正常压制制度时,砖坯气孔率降低值已经很小。

Three types of base asphalt and six SBS were used to produce SBS modified asphalt. The interaction of SBS modified asphalt was discussed in different states between the base asphalt and SBS based on their compositions. Through the traditional tests, such as penetration, soften point and ductility, and US SHRP tests, the results indicated that influences to affect the temperature susceptibility, high and low temperature performance, aging characteristics are base asphalt, SBS types and their dosages. The functions of penetration to viscosity and complex shear modulus G~* to complex dynamic shear viscosity η~* were set up, and then theviscosity-temperature susceptibility of wide temperature span and the calculation method of low temperature viscosity were obtained."Process" evaluation criterions, high grading critical temperature T_ and low grading criticaltemperature T_ , were suggested according to the high and low temperatureperformances of SBS modified asphalt. Using the experience of Repeated Creep and Recovery Test for Binders, a new high-temperature evaluation index,modification rutting factor G~*~(-9) was obtained. The results after RTFO and PAV aging indicated that traditional tests didnt differentiate base asphalt and SBS modified asphalt, but dynamic mechanics temperature spectrum and G*-5 black chart clearly reflected the influence of aging to the SBS modified asphalt. With the IR and GPC tests, the reason of aging to the SBS modified asphalt were due to asphalt phase oxygenated and SBS phase depredated.

论文选择3种油源的基质沥青和6种SBS改性剂制备改性沥青,通过分析基质沥青和SBS改性剂的组成结构特点,得出了不同状态下SBS改性沥青的SBS与基质沥青的相互作用机理;通过针入度、软化点、延度等常规试验以及美国SHRP试验,分析了基质沥青、SBS改性剂类型与剂量对SBS改性沥青的温度敏感性、高低温特性及老化特性的影响;建立了针入度-粘度、复数模量G~*-复数粘度η~*的换算关系,得出了宽温度域的粘温指数VTS和较低温度下粘度的计算方法;通过高低温性能分析提出了&过程&评价参数高温等级温度T_和低温等级温度T_;借鉴重复恢复与蠕变试验研究成果,得到了SBS改性沥青高温评价指标改进型抗车辙因子G~*~(-9);RTFO和PAV老化后的性能试验结果表明,常规试验难以区分SBS改性沥青与基质沥青的差异,而动态力学温度谱、G~*-δ黑斑图可以反映老化作用对SBS改性沥青的影响,且通过IR试验和GPC试验得出SBS改性沥青老化是沥青相的氧化和SBS的降解共同引起的;通过不同温度下SBS改性沥青混合料的旋转压实SGC试验,根据粘度与剪变率的关系,提出用剪变率60(1/s)测试SBS改性沥青的粘温曲线,并按照0.17±0.02Pa.s和0.28±0.03Pa.s确定施工温度。

And the "three-factor quadratic regression orthogonal rotary method" was adopted to study mixing performance of the mixer,after the machine had been designed and trial-produced. It was showed that the optimum technological parameters for mixing time, block coefficient and rotary speed of the paddle shaft were 180 s, 0.75 and 56 r/min, respectively. At the same time, the remains in the bin was little (0.015%). The effe...

为了提高双轴桨叶混合机的混合性能,采用二次回归正交旋转组合试验,对设计样机进行混合均匀度及机内残留率的试验研究,得出了其工作参数的合理组合:混合时间为180s,充满系数为0.75,桨叶轴转速为56r/min;机内残留量极小(约为0.015%),满足其作为配合饲料生产,尤其是预混合饲料生产的工艺要求,也为进一步改进设计提供了依据。

Not only the traditional feed mixer the efficiency is not high, moreover the ingredient precision is low, the energy consumption quite is big, already could not satisfy the feed industry development request; The turn over type two axle thick liquid leaf type mixer has the mix cycle short, the mix effect good, the energy consumption...

翻转式双轴浆叶式混合机具有混合周期短、混合效果好、能耗低、出料干净和对不同物料混合的适应性强等优点,它把入料口和出料口合二为一,卸料速度快,残留量小,可使物料进行多方位的复合运动和在失重区域内的自由运动,避免了比重和颗粒度差异较大的物料组分在混合中产生偏析与再度分级现象,确保了混合均匀度。

The change of superheavy oil viscosity after mixing light oil was studied by the experiment,and the mixed viscosity was calculated by non-linear mixing method.

采用在注蒸汽过程中向地层掺入稀油的方法来降低地层稠油的粘度,实验研究了超稠油掺稀油后粘度的变化,并按非线性混合方法计算了稠油与稀油混合后的粘度。

A V-mixer is most used in a premix mill and a pharmaceutical factory,in order to study the effects of different load factors and mixing times on the mixing homogeneity of premixes,to find out the rational load factor and the optimum mixing time of a V-mixer in production of additive premixes.

V型混合机是预混合饲料厂和药厂最常采用的混合机,为了研究不同装载系数和混合时间对预混料混合均匀度的影响,探求V型混合机在添加剂预混料生产中合理的装载系数和最佳的混合时间。

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