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The invention provides an anhydrous hydrogen fluoride production process; reaction raw materials fluorite powder and sulfate are mixed by an external mixer and enter into a converter with jacket; hot air with the temperature of 350 DEG C to 600 DEG C is fed in the jacket; the fluorite powder and the sulfate have chemical reaction and produce hydrogen fluoride; the produced hydrogen fluoride enters into a scrubber from a furnace header to be washed; the washed hydrogen fluoride enters into an intermediate tank from a condenser, and then receives distillation and degasification to prepare the finished product anhydrous hydrogen fluoride; solid residue is emitted from a furnace tail.

本发明提供一种无水氟化氢生产工艺,反应原料萤石粉及硫酸经外混器混合后进入带有夹套的转炉,向夹套内通入350~600℃的热风,萤石粉和硫酸在发生化学反应生成氟化氢,生成的氟化氢气体由炉头进入洗涤塔进行洗涤,洗涤后的氟化氢由冷凝器进入中间槽,然后经过精馏、脱气制得成品无水氟化氢;固体残渣由炉尾排出。

Compared with the conventional optical coupler, the hybrid refractive-diffractive systems offer considerable reduction in the apparent size ,weight, and improve the imaging quality.

对设计结果的分析表明,折-衍混合耦接器不仅在光学性能方面优于传统的光学耦接器,而且在尺寸和重量上有非常显著的减少。

A steel bar is washed and dried, and then put into a glass pipe which is sealed to obtain stirring magneton; a mixed solvent of Gamma-methacrylate oxide propyl trimethoxy silane and methanol is prepared and added with an organic base to obtain a pre-bonding solvent; the stirring magneton is immerged into the pre-bounding solvent, and the outer surface of the glass pipe of the stirring magneton is bonded with a layer of silane substance with alkenyl; a reactive monomer mixture and a pore-forming agent mixed solvent are evenly mixed and then added into a container, the stirring magneton after the pre-bounding is put into the container which is sealed and then put into a water bath; after reaction, the container is removed, the stirring magneton coated with a polymer is taken out and put into a extractor and extracted by using a solvent; or the stir bar is immersed into the solvent till no impurity can be checked in the solvent, thereby obtaining the product.

将铁条清洗干燥,放入玻璃管内,密封得搅拌磁子;配制γ-甲基丙烯酸氧丙基三甲氧基硅烷与甲醇的混合溶液,加入有机碱得预键合溶液,将搅拌磁子浸入预键合溶液,在搅拌磁子的玻璃管外壁键合一层带烯基的硅烷化物质;将反应单体混合剂和致孔剂混合溶液混匀后倒入容器中,将预键合后的搅拌磁子放入容器,密封后置于水浴中,反应后除去容器,取出涂有聚合物的搅拌磁子,置于提取器中,以溶剂提取,或将搅拌棒置于溶剂中浸泡至溶剂中无杂质检出,得产物。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小,进行综合分析,确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量,测定条件:加入100ml浓度为8.0±0.1%的氢氧化钠,在恒温水浴中煮沸回流6h;采用溶剂萃取法测定JOB-1C中TATB的含量,选择TATB饱和的二甲基甲酰胺为萃取溶剂,用G4坩埚式过虑器进行萃取分离;采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量,通过实验确定了多波长组合:λ=267nm,275nm,283nm,291nm,299nm;朗波—比耳定律的适用范围为PNP浓度:0.005~0.025mg/ml,HMX浓度:0.06~0.30mg/ml;在测定波长下,对PNP、HMX标准溶液的吸光度—浓度进行线性回归,由回归曲线的斜率得出PNP、HMX的吸收系数;根据朗波—比耳定律和吸光度加和性原理,在测定波长下,对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归,回归曲线的斜率即为混合溶液中PNP的浓度。

The effects of impeller types, baffles, gas sparger, rotational speed, gas volumetric flow rate and particle fraction on mixing time were systematically investigated in three-phase gas-liquid- floating particle systems by measuring the temperature difference using thermocouples.

在釜径386mm的搅拌釜内,采用热电偶温差法考察了搅拌桨型、挡板、气体分布器等结构因素和转速、气量、颗粒分率等操作因素对自浮颗粒三相搅拌混合的液相混合时间的影响。

The laser diode and the chip of the laser diode driver and the 4∶1 multiplexer,which are realized in different materials and processes,are fabricated on one same ceramic substrate using a film circuit to make up one opto-electronic integrated circuit,i.e.,an OEIC.The chip and the diode are realized with a 0.35μm CMOS process and with wet etching,polymer planar, and lift-off technologies, respectively.The module is encapsulated with a wing shell.

该发射机采用薄膜电路和激光焊接耦合技术将高速集成电路和光电子器件进行混合集成,其中高速集成电路是采用0.35μm硅CMOS工艺实现的单片4∶1复接器加激光驱动器芯片,光电子器件是采用湿法腐蚀、聚合物平坦和lift-off等技术实现的激光器芯片,最终混合集成模块采用蝶形管壳进行封装,体积小、性能优良。

Ancillary equipment: wet material mixer, dry powder mixer, particle machine, the hot air circulating oven, powder shaker machine, packets of sugar-coated, suction powder boxes, tablet In addition to flour, etc..

配套相关设备:湿料混合机、干粉混合机、颗粒机、热风循环烘箱、振动筛粉机、包糖衣机、吸粉箱、片剂除粉器等。

The frequency synthesizer includes a completely on-chip LC VCO and a 90 degrees phase splitter for generating the I and Q LO signals to the down-conversion mixers in receive mode and up-conversion mixers in transmit mode.

频率综合者在-芯片LC VCO上-完全包含a和一产生我和 Q北美印第安人90度分相器为向挫折-转换混合者发信号示意在朝派收到方式和沿着-转换混合者在朝派传送方式。

The association effect of inert gas and gas phase acetic acid-water in condensing process was considered, the heat and mass transfer behavior of the heat exchangers at every step and the influence of heat and mass transfer on the design of heat exchangers were analyzed for the condensing process of acetic acid, water, and mixed nitrogen vapor in the condenser in the PTA oxidation process.

针对PTA氧化反应中冷凝器内的醋酸、水和氮气混合蒸气冷凝过程,考虑冷凝过程中惰性气体和气相醋酸-水缔合效应,分析了各级换热器内传热传质行为以及传递对换热器设计的影响。

In the design of W band double-balanced mixer, a novel structure using Magic-T and two baluns, which all realized by ratrace, is proposed with no crossing of transmission line.

在W频段双平衡混频器的设计中,本文提出由混合环构成的魔T与巴伦级连而成的功率混合电路,这种新颖的电路结构使整个电路单平面化,避免了任何跳线。

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