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The method of water distill and the alcohol precipitates was adopted to withdraw the ointments from the Hirudo ,the microcrystaline cellulose being used in manufacturing Naoxuekang dispersible tablets,and review three batch samplet.

方法采用水提醇沉方法从水蛭中提取浸膏,以微晶纤维素作为主要辅料制备脑血康分散片,并对三批中试放大试验样品进行考察。

Results: The optimal preparing process is: making Panax to be powder; extracting Rheum and Coptis respectively with ethanol; decocting Astragalus, Hirudo and Polyporus with water; then making all the extractions to be powder and mixing with Panax powder, then putting them into capsules. The content of Ginsenoside 〓 in one capsule should be not less than 0.235mg. Panax and Coptis are the main compositions that make Liuwei Tangshen Capsule reducing the blood sugar.

结果:确定最佳制备工艺为:人参粉碎成细粉,黄连、大黄分别用乙醇提取,黄芪、水蛭、猪苓三药用水共煎,各提取物干浸膏细粉与人参细粉混匀,装胶囊;有效成分含量的控制标准为:每粒胶囊中含人参皂苷〓不低于0.235mg;人参、黄连是六味糖肾胶囊发挥降糖作用的主要药味;六味糖肾胶囊中小檗碱在动物体内的分布和消除速度均较适中,但病理模型动物与正常动物相比吸收较差。

METHODS:The compounding of adjuvant and the technology were optimized by orthogonal experiment,and the hydroscopicity and fluidity of powdered extract were investigated.

以正交试验法筛选最佳辅料配方以及最佳工艺条件,并考察浸膏干粉的吸湿性和流动性因素。

OBJECTIVE:To improve hydroscopicity and fluidity of traditional Chinese drug extractum by spray drying and to improve affixes to the wall of the drier during drying for providing reasonable relative humidity of production.

目的:利用喷雾干燥法改善中药浸膏的吸湿性和流动性,最大限度地改善喷雾干燥的黏壁现象,为中药工业现代化提供合理的相对湿度环境及生产条件。

Osmanthus fragrans and Jasminum sambac were extracted with supercritical CO_2 at different conditions of pressure,temperature and contact time to estimate the yield and quality.

用超临界CO2对桂花、茉莉花进行了萃取研究,考察萃取时间、温度、压力对浸膏得率和质量的影响。

A comparison study of constituents of the absolute extracted from flower of Jasminum sambac by supercritical CO 2 and petroleum ether was made using GC and GC MS.

利用 GC和 GC- MS联用仪对超临界 CO2 萃取茉莉浸膏的净油进行化学成分分析,分离出 131个组分,鉴定出其中的 35个化合物,所鉴定的成分占分离成分的 85%以上。

A quick and nondestructive method using near infrared diffuse reflectance spectroscopy was presented to determine the contents of berberine, palmatine, jatrorrhizine and total alkaloid of Coptis extract.

采用近红外漫反射光谱法对黄连浸膏粉中小檗碱、巴马亭、药根碱和总生物碱含量进行快速无损检测。

Discussed the micromeritic characteristies of CS extracted powder and the FT-207 powder, inspected the excipient proportion, the wettibility, the drying temperature factors through prescription screening as well as the orthogonal test to determine granulation process.

考察了CS浸膏粉和FT-207的粉体学性质,通过处方筛选以及正交试验考察了辅料配比、润湿度、烘干温度3个因素,确定了制粒的工艺路线。

We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR), among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-(2'-glycerin)-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl)-β-D-galactopyranoside; ethyl rosemarinate.

我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究,利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物,经化学方法和波谱技术(红外,质谱,一维和二维核磁共振谱)鉴定了二十五个化合物的结构,其中四个为新的化合物,它们分别是:异海松-15-烯-3β,8β,20-三醇;苯乙醇-3-O-(2'-甘油基)-5-O-β-D-吡喃葡萄糖甙;3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙;迷迭香酸乙酯。

Results The optimum conditions for the extraction of Peucedanum praeruptorum Dunn was as follow: 80 % alcohol was used as solvent, and 8 times the amount of alcohol was added, the mixture was kept refluxing for 1.0 h for the first time; then 6 times the amount of alcohol was added and the mixture was kept refluxing for 0.5 h for the second time; Four times the amount of alcohol for 0.5 h for the last time.

结果 白花前胡的最佳提取工艺为用质量分数80 %的乙醇提取3次,提取时间分别为1.0、0.5、0.5 h,3次所用溶媒量分别为药材质量的8、6、4倍;按照筛选出的最佳工艺条件进行的3次重复性实验,测得浸膏中8-甲氧基补骨脂素含量质量分数为0.094 %,折合1 g生药中含量为0.171 2 mg,与预测值基本一致。

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