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浸渍剂

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The present invention adopts the technical proposal of adopting ZSM-5 mesoporous molecular sieve raw powder with a silicon-aluminum mol ratio SiO2Al2O3 of 20 to 1000 and a weight percentage of 20 to 100 percent as well as at least one caking agent selected from SiO2, clay and Al2O3 to extrude, tablet or spray into shape; then treating for 1 to 8 hours by 0.1 to 3 mol/l of at least one ammonium liquor from ammonium nitrate, ammonium chloride or ammonium sulphate or 0.1 to 8.5 mol/l of at least one acid liquor from muriatic acid, nitric acid, vitriol or acetic acid under a temperature of 20 to 90 DEG C; then using steam to treat for 2 to 15 hours under the temperature condition of 400 to 700 DEG C; using a liquor of 0.1 to 3mol/l selected from at least one of oxalic acid, citric acid or maleic acid under a temperature condition of 20 to 90 DEG C to dip for 2 to 5 hours to obtain the modified molecular sieve catalyst, thus better solving the problems.

本发明通过采用硅铝比SiO2/Al2O3为20~1000重量百分比计20~100%的ZSM-5介孔分子筛原粉与余量的选自SiO2、粘土或Al2O3中至少一种粘结剂挤条、压片或喷球成型;再经过0.1~3摩尔/升选自硝酸铵、氯化铵或硫酸铵中的至少一种铵溶液或0.1~8.5摩尔/升选自盐酸、硝酸、硫酸或乙酸中的至少一种酸溶液在温度20~90℃下处理1~8小时;然后在温度为400~700℃条件下水蒸汽处理2~15小时;再用0.1~3摩尔/升选自草酸、柠檬酸或马来酸中至少一种在温度为20~90℃条件下浸渍2~5小时得所需改性分子筛催化剂的技术方案较好地解决了该问题,可用于甲醇转化制丙烯的工业生产中。

The results show that the optimal value of CoCl2 concentration is 0.2 mol/L and the maximum adsorbed amount is 19.674 mg/g onto this adsorbent. The adsorption capacity of phosphine onto CoCl2-modified ACF decreases with the increase of temperatures. The maximum absorbed amounts are 19.674 mg/g at 298 K, 13.537 mg/g at 313 K and 11.087 mg/g at 328 K, respectively. It is found that the Freundlich equation is more suitable for the description of phosphine adsorption process than the Langmuir equation. The isosteric heat of adsorption decreases with the increase of the surface loading on CoCl2-modified ACF, which means that CoCl2-modified ACF adsorbent has an energetically heterogeneous surface. Meanwhile, adsorptive phosphine removal performance may be a dominant of physical adsorption when the heat of adsorption is 16-24 kJ/mol, the CoCl2-modified ACF adsorbent will be one of the candidates for tail gas purification of airtight calcium-carbide furnace and recycle of phosphine.

研究结果表明:浸渍液浓度最佳值为0.2 mol/L,此改性ACF对PH3的饱和吸附量为19.674 mg/g;PH3在CoCl2改性ACF上的吸附量随温度升高而迅速降低,在298,313和328 K时PH3的饱和吸附量分别为19.674,13.537和11.087 mg/g;Freundlich吸附等温方程较好地模拟了PH3在改性ACF上的等温吸附;PH3气体在改性ACF上的等量吸附热随吸附量的增大而减小,表明改性ACF吸附剂表面能量的不均匀性;吸附热在16~24 kJ/mol范围内,过程为物理吸附,有利于密闭电石炉尾气的净化。

The therapeutic effects were evaluated in the clinical efficacy and mycological culture examina-tion.

目的 观察不同剂型的抗真菌药物治疗夏季水疱型、浸渍型足癣的临床疗效,好地指导临床用药提供实验依据方法 80例临床实验室确诊的足癣患者分4组,分别外用特比萘芬喷雾剂、乳膏,达克宁乳膏、散剂,根据临床疗效及真菌培养判定其效果。

The experimental results show that the optimum preparation conditions of catalyst of SO42-/Zr-CLC are achieved :pillaring material is 0.5mol/l ZrOCb,Zr/clay is 3mmol/g,accelerant is (NH4)2SO4 and the quantity of SO42- is 30%, the precursor of Zr-CLC is dipped by SO42- and is calcinated at temperature of 500 癈 for 2h.

将聚合羟基锆阳离子交联剂通过离子交换引入膨润土层间域撑柱膨润土,同时通过浸渍将SO42-引入到膨润土层间的锆阳离子表面,高温焙烧活化,合成了催化性能良好的中孔固体酸催化剂SO42/Zr-CLC,同时对催化剂的性能和结构进行了研究。

A modified semicoke desulfurizer for FCC gasoline was prepared by hydrothermal and nitric acid activation and dipping with activate component using Zhalainuoer semicoke as raw material.

以扎赉诺尔半焦为原料,采用硝酸活化、水热活化和浸渍活性组分等改性方法,制备了改性半焦脱硫剂,并用于脱除FCC汽油中的各种硫化物。

The method includes the following steps: getting specific amount of knitted or unknitted natural fiber and dipping the natural fiber in the aqueous solution of silane coupling agent for 1-100min, taking out and drying the natural fiber, thus producing natural fiber with modified surface; then pressing the polylactic acid into sheet in a plate vulcanization machine; disposing 2-10 polylactic acid sheets into a die and arranging one modified natural fiber sheet between every two polylactic acid sheets; pressing and molding the sheets; in this way totally biologically degradable polylactic acid composite material can be made.

该方法为:先取一定量的经过编织或未编织天然纤维,将其浸渍在偶联剂水溶液中1~100分钟后取出,经干燥后得到表面改性的天然纤维。然后,将聚乳酸在平板硫化机中压制成薄板;将2~10片聚乳酸薄板放在模具中,且每2片之间放置1片改性的天然纤维,然后模压成型,得到可完全生物降解聚乳酸复合材料。

Ceramic-veneer Composites is a three-layers plywood prepared by heat pressing, which composes of ceramic-veneer on the surface and unworked veneer inside. Ceramic-veneer is a material prepared by Sol-Gel method and Vacuum-Pressure method, and constitutes with veneer and ceramic emulsion.

摘 要:陶瓷化单板表层复合材料是以陶瓷化单板为表层材料,未处理木材单板为芯材,经热压工艺制备而成的三层胶合板;陶瓷化单板是以木材单板为基材,陶瓷前驱液为浸注剂,采用溶胶-凝胶法经真空加压浸渍处理而成。

A method for impregnating wood as claimed in claim 15, wherein said curing is in the presence of a polymerization initiator.

一种方法为浸渍木材所宣称的那样,在索赔15 ,其中,固化是在出席会议的一位聚合引发剂。

The invention provides a method for preparing a tube-shaped cathode of a direct methanol fuel cell, belonging to the fuel cell field and comprising the steps of: dispensing a single solution for gel injection molding at first, then adding a mesophase bituminous coal micro ball into the single solution and stirring evenly to obtain stable slurry, then casting the slurry into a die, preserving heat until the single solution reacts with a cross-linker completely to obtain a carbon-biscuit, after drying and sintering the biscuit in vacuum, preparing a diffusion layer and a catalyst layer on the surface by dipping process, and then coating polyester electrolyte membrane with a burette, rolling the carbon on a warm table to solidify the electrolyte membrane.

一种制备直接醇燃料电池管状阴极的方法,属于燃料电池领域。本发明首先配制凝胶注模用单体溶液,之后将中间相沥青炭微球加入到单体溶液中,搅拌均匀得到稳定的浆料,然后将浆料浇注到模具中,保温至单体与交联剂完全反应,得到炭管素坯,将素坯烘干、真空烧结后,在其表面采用浸渍工艺制备扩散层、催化剂层,然后采用滴管涂覆聚合物电解质膜,在加热台上对炭管进行滚压,使电解质膜固化。

The results showed that the use of ultrasond increased the content of active ingredient in the sorbents, improved the pore structure, and thinned the particles.

研究结果表明,超声浸渍促进活性成分的负载,丰富脱硫剂的孔隙结构,并具有细化和均化颗粒的效果。

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