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A fully automated simultaneous determination of nitrate and nitrite in water samples by sequential injection analysis based on the Griess diazo-coupling reaction and the formed azo dye for nitrite at 540nm and reduction to nitrite using coppered cadmium column.

用顺序注射分光光度法,通过一次进样。同时测定硝酸根和亚硝酸根。亚硝酸根是根据格里斯重氮-偶联反应,形成偶氮染料后在波长540nm下进行检测。而硝酸根则通过镀铜镉粒还原柱还原为亚硝酸根后进行测定。

The C-curves of the cyanided case of 18CrMnTi and 18CrMnMo steels austeni-tized at 860℃ were determined by metallographic methods.

用金相法测定了18CrMnTi与18CrMnMo钢高温氰化层经860℃奥氏体化后的恒温C-曲线与马氏体开始转变温度M_H,同时也测定了A_1温度。

To determinate the concentration of TiO_2 in functional fiber for labeling purpose,the sample was nitrified with burning and dissolved in mix acid as pretreatment and then its concentration of TiO_2 was determined by spectrophotometric method with ascorbic acid as shelter reagent of Fe~(3+) and Cu~(2+) and diantipyryl methane as developer at wavelength λ=390 nm.

针对功能纤维中添加TiO2的含量测定问题,对功能纤维样品采用高温消化、混酸溶解的前处理方式,以抗坏血酸作Fe3+、Cu2+的掩蔽剂,二安替比林甲烷作为显色剂,用分光光度法在λ=390 nm波长处测定功能纤维中纳米TiO2的含量。

With best condition of parallex spectrophotometric determination, the amount of soluble sugar in pomelos and sweet oranges were determined...

最后,作者应用这种改良法测定了文旦和甜橙果实中的总糖含量,经t检验,其测定值与采用费林法无显著差异。

SDS-PAGE, biochemical determination of triglycerideand HPLC can be used for detection of milk protein, milk fat and lactose. It reflects lactationfunction of insulin and probating impacting on dairy goat mammary gland epithelial cells.

此外,SDS-PAGE、甘油三酯生化测定及HPLC法对乳蛋白、乳脂和乳糖的测定反映了激素对乳腺上皮细胞泌乳功能的影响。

For the determination of five carbamate pesticide residues by high performance liquid chromatography with gel permeation chromatography purification, sample was extracted with acetonitrile and purified with gel permeation chromatography. Methanol-water was used as the mobile phase by gradient elution, flow rate of 1.0mL/min, using a fluorescence detector and quantitating with external standard method.

凝胶渗透色谱-液相色谱法测定5种氨基甲酸酯类农药残留中,实验采用乙腈提取,凝胶渗透色谱柱对样品进行净化,以甲醇-水为流动相,进行梯度洗脱,流速1.0mL/min,荧光检测器检测,外标定量测定。

The structure of synthesized epoxidized cottonseed oil was characterized by means of' 1H NMR and FT-IR. Epoxy value,iodine value,acid value,and color of the product were determined by Chinese national standards.

通过核磁共振氢谱、红外光谱及黏度测定方法对产物的结构进行了表征,并采用国标法对产物的环氧值、碘值、酸值和色泽进行了测定。

Right Through adopting the Acid Dye Colorimetry in the determination of matrine permeation quantity, the interference by amino acids and proteins in skin can be eliminated.

Chinese 采用酸性染料比色法测定苦参碱渗透量,可以消除皮肤中的氨基酸、蛋白质对测定的干扰。

Methods: Spectrophotometric determination of the condiment amino nitrogen, the results of the impact analysis of factors, and with formaldehyde titration method of comparison.

采用分光光度法测定调味品中的氨基酸态氮,对影响测定结果的因素进行分析,并与甲醛滴定方法进行了比较。

Aiming at the problems occurred in the analytical process of determining the total phosphorus in industrial circulating cooling water by ammonium molybdate spectrophotometry and based on the experience summary,the original analytical method has been improved.

针对用钼酸铵分光光度法测定循环冷却水中的总磷在实际分析过程中遇到的一些问题,经过总结经验,改进了原有的分析方法,降低了测定中的干扰因素,提高了一次分析结果的准确可靠性,使分析结果更为准确可靠。

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