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A new method using microwave digestion technique was developed for the determination of cadmium, chromium and lead in Lycoris radiata by graphite furnace atomic absorption spectrometry.

采用微波消解技术处理样品,用石墨炉原子吸收光谱法测定,对消解试剂和微波消解条件进行了筛选和优化,研究了石墨炉原子吸收的测定条件。

Aiming at the disturbing of trace tin and trace germanium in existing simultaneous, using Artificial Neural Networks spectrometry determined simultaneously trace tin and trace germanium in extraction raffinate and stripping raffinate, tested the effect of these two metal separation and extraction.

针对微量锡与微量锗同时存在下相互干扰测定的困难进行研究,利用人工神经网络光度法比较准确的同时测定出萃余水相和反萃取水相中的微量锡与微量锗的含量,验证了两者的分离富集的效果。

Ion exclusion chromatography was used for the determination of organic acids in both beer and white wine with common HCl solution as an eluent and tetrabutylammoniun hydroxide as a regenerant.

研究了离子排斥色谱法分离测定啤酒和白葡萄酒中有机酸;选用常见的盐酸溶液作淋洗液,以四丁基氢氧化铵为再生液,考察了淋洗液浓度、流量等因素对分离和测定的影响,对啤酒和白葡萄酒中常见有机酸在阴离子排斥色谱柱上的保留行为进行了系统的研究;通过试验确定最佳的色谱条件为盐酸浓度1。

When the glancing—tilt method is used, the linearity of 2θ—sin〓Ψ can be remarkedly improved.

X射线应力测定的sin〓Ψ法在测定PCVD TiN的残余应力时,2θ—sin〓Ψ发生严重弯曲,如果沿用线性拟合求斜率的方法计算残余应力,误差必然很大。

objective:to determine total flavonoids content in the leaves of acer saccharum.methods:we determined total flavonoids contents in leaves of acer saccharum by ultraviolet and visible spectrophotometry.results:the flavonoids content was 1.035mg/g in the leaves of acer saccharum.conclusion:the flavonoids content is rich in the leaves of acer saccharum and the leaves have pharmic value.

目的:本文对糖槭叶中的总黄酮含量进行测定。方法:采用紫外-可见分光光度法对糖槭叶中总黄酮含量进行测定。结果:糖槭叶中总黄酮含量为1.035mg/g。结论:糖槭叶中含有丰富的黄酮类化合物,具有可观的药用开发价值。

It was showed that microwave technique could accelerate extracting polysaccharide from Saururus Chinensis Baill and glucose oxidase method provide a new convenien...

实验结果显示运用微波技术从三白草中多糖提取速度加快;以葡萄糖氧化酶法进行多糖含量测定,为多糖含量测定方法寻找一种新的简便的途径;药理实验说明三白草中的多糖可使四氧嘧啶型糖尿病兔体内血糖值降低,超氧化物歧化酶的活力增强,丙二醇下降。

Methods: The use of high-performance liquid chromatography, and so on through testing conditions on the choice of extraction method of identification, and the determination of the method of inspection, to determine Schisandra in Deoxyschizandrin content.

运用高效液相色谱法等通过对检测条件的选择、提取方法的确定、以及含量测定的方法学考察,来测定五味子中五味子甲素的含量。

METHODS: Seralbumin, serum creatine, blood sugar, total cholesterol, total triacylglycerol, high-density lipoprotein cholesterol, and low-density lipoprotein cholesterol were detected after more than 12 hours of fasting.

测定过夜空腹12 h以上血白蛋白、血肌酐、血糖、总胆固醇、总三酰甘油、高密度脂蛋白胆固醇、低密度脂蛋白胆固醇;用放射免疫法测定早晨第1次尿中白蛋白。

Study the bioactivity of the n-HA/PA66 composite and the effects it would be to body's metabolism of calcium and phosphorus ion in vivo.(3) Study the osteo-conductivity and the ability to repair bone defect of the porous n-HA/PA66 composite and the feasibility use it as the scaffold of bone tissue engineering. Objects and Methods as follows: 1.To evaluate the biocompatability of nano-hydroxyapatite crystals and polyamide composite (n-HA/PA66) with the L929 cells.To proceed the morphological observation and take pictures of L929 cells after 1d,2d,4d,and 7d of co-cultured with extract of n-HA/PA66 ,and direct contact with n-HA/PA66.To determine light absorbtion value of every hole under 500 nm with enzyme linked immunity instrument after 1 d,2 d,4 d,and 7 d of contact of n-HA/PA66 extract with L929 cells,and direct contact with n-HA/PA66.In the meanwhile calculate the relative multiplication rate of cells,and evaluate them by six degree tests for cytotoxicity. To investigate the acute and chronic toxic reaction on the whole body induced by the new nano-hydroapatite crystals and polyamide composite(n-HA/PA66)after implanting in vivo and its effects on partial constitution of animal organs after implanting in vivo,and evaluate the potential and degree of subcuticular stimulation reaction.

本实验主要由以下三部分组成:一、n-HA/PA66 复合材料在动物体内、体外的生物相容性及生物安全性评价二、n-HA/PA66 复合材料植入动物体内的生物活性及近期对机体钙、磷代谢影响的实验研究三、网孔 n-HA/PA66 复合材料作为支架修复兔桡骨节段缺损的动物实验研究主要研究目标及方法如下:参照 GB/T16886.5-1997-ISO 10993-5:1992《医疗器械生物学评价细胞毒性试验体外法》之评价标准和要求,采用规定的 L929 细胞(小鼠结缔组织成纤维细胞),分别经直接接触和材料浸提液与细胞共培养等方式对 n-HA/PA66 复合材料进行细胞毒性测试,采用细胞形态观察法观察两种细胞各组在 24h、48h、72h、5 天后各时相点的细胞形态学变化,并在显微镜下照相,从而对细胞与材料的生物相容性进行定性评价;同时采用细胞生长抑制法,以酶标仪定量测定评价各组 1,2,4,7 天 L929 细胞的相对增殖率,以定量测定并判别材料对细胞的毒性程度。

Water samples were extracted and purified and collected by solid-phase extraction LC-18 column. Soil samples were extracted by ethyl acetate/petroleum ether (2:1, by vol) and purified by sulphonation. Wheat sample was extracted by acetonitrile/water (4:1, by vol) and purified and collected by SPE- Florisil column.

水样直接用LC-18固相萃取小柱分离、净化和富集;采用乙酸乙酯/石油醚(体积比2:1)振荡提取,磺化法净化,测定土壤中氯氟吡氧乙酸残留量;以乙腈/水(体积比4:1)为提取剂,氟罗里硅土固相萃取小柱分离、净化,测定小麦样品中氯氟吡氧乙酸的残留量。

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