测定法

Introduce the composition of naphthenic acid and two methods about the determination of acid number .

介绍了石油酸的组成及国内测定原油酸值的两种方法，对采用不同方法测定原油酸值产生的差异进行分析，建议采用电位滴定法测定原油的酸值。

According to the characteristic that the isoflavonoids of Derris elliptica Benth have a distinctive absorption spectrum within the ultroviolet wave length range (210￣ 345 nm, 290￣305 nm), a new method for determining the total isoflavonoids in Derris elliptica Benth by Ultroviolet Spectrometry has been put forward.

根据鱼藤中异黄酮类化合物在紫外光210～245nm及290～305nm处具有吸收峰这一特性，提出了用紫外分光法测定鱼藤中异黄酮类总含量的方法。在300nm波长处，浓度低于6×2.618×10－3／mol·L－1时，测定了标准系列的吸光值，结果表明吸光值与浓度近乎直线相关，相关系数为0.9977；标准系列吸光值准确性高；加样回收率达99％以上；测定样品时，重现性好

The extent of nitridation is evaluated by the nitrogen content determined by a LECO Nitrogen/Oxygen determinator.

采用氮/氧分析仪测定产物氮含量，评价氮化反应程度；以BET氮气吸附法测定比表面积，分析粉体活性；以扫描电镜分析样品表面形貌；以热重分析仪测定碳含量，X射线能谱仪估计元素组成。

When proceeding the research of drug identification by ultraviolet spectrophotometry, this paper adopts the approaches below: to identify Metronidazole Buccal Tablets and Potassium Sodium Dehydroandroan Drographolide Succinate by ulviolet maximum absorbent wavelength; to identify Metronidazole Disodium Phosphate for Injection by ulviolet maximum absorbent wavelength and minimum absorbent wavelength; to identify Ceftriaxone Sodium for Injection and Clarithromycin Tablets by retention time of high performance liquid chromatography- ultraviolet spectrophotometry.

通过测定紫外最大吸收波长λ_(max鉴别甲硝唑口颊片和炎琥宁、测定紫外最大吸收波长λ_(max和最小吸收波长λ_(min鉴别注射用甲硝唑磷酸二钠，结合高效液相色谱(high performance liquid chromatography-ultraviolet detector，HPLC-UV)中保留时间的测定鉴别注射用头孢曲松钠和克拉霉素片，本文建立了药物鉴别的紫外分光光度法。

Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上，开展了如下未见文献报道的创新性的研究工作：(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究，建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法，与以前的报道相比，灵敏度和分析时间均有很大改善；(2)使用荧光素钠作为背景荧光试剂，建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法，扩大了激光诱导荧光检测的应用范围，对难衍生化合物的分离分析提供了一种新思路和新途径；(3)以荧光素钠作为背景荧光试剂，建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法；(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物，为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

The correlation coefficient is 0.9991. The method has been applied to the determination of trace cadmium in galvanization waste water with the relative standard deviation of 2.5%-3.2% and the recovery of 98.0%-102.0%. The results of this method are in good agreement with those of AAS.

方法用于电镀废水中微量锡的测定，相对标准偏差为2.5%~3.2%，加标回收率为98.0%-102.0%，测定结果同原子吸收光谱法的测定结果相吻合。

Methods The porous glass plate absorber valve was used to sampling, the contents of hydrogen chloride and sulfate was determined by hydronium chromatography method at the best determination condition and suitable mobile phase.

以多孔玻板吸收管采样，离子色谱法测定，选定最佳测定条件，确定适宜的流动相，测定氯化氢和硫酸的含量。

There is a large deviation to measure lower BOD5 of wastewater treatment plant using standard method and respirometry method.

活性污泥经过洗涤去除吸附的有机物后，将其制成浓度为200 mg/L左右的接种溶液用于低值BOD5测定，测量结果介于采用稀释法测定和差压计直接测定结果之间。

To produce medicine serum of Liu-Shen-Wan with different dose, different time of pouring medicine, different time of blood sampling.2. To measure content of arsenic in serum with atomic absorption method, to qualitative analysis toadfish in medicine serum of Liu-Shen-Wan with thin layer chromatography.3. MTT and trypan blue assay detects the growth inhibition effect of Liu-Shen-Wan on HL-60 cells and to make certain the best scheme of making method of medicine serum of Liu-Shen-Wan.4. Gimsa dying assay observes morphology changes of apoptosis .In situ end-labeling method and flow cell machine quantificationally probes apoptosis phenomena.

1 分不同的给药剂量、给药天数和不同的采血时间制备含药血清。2 用原子吸收法测定血清砷含量；薄层色谱法定性检测六神丸含药血清中蟾酥成分。3 用MTT法、胎盘蓝染色法观察六神丸对HL-60细胞的增殖抑制作用，确定最佳血清制备方案。4 用吉姆萨染色法观察细胞凋亡的形态学变化，流式细胞仪、原位末端标记法定量检测细胞凋亡程度。

The comparison analysis of nitrate nitrogen determination is conducted with the same standard solution and natural water samples by two methods of spectrophotometric method with phenol disulfonic acid and ultraviolet spectrophotometer.

测定水中硝酸盐氮含量有多种方法，主要包括酚二磺酸光度法、锅柱还原法、戴氏合金还原法、离子色谱法、紫外分光光度法和电极法等。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。