测定法

A method for AAS determination of Palladium in Aluminum oxide matrixs by microwave digestion was reported in this paper.

报道了微波消解- AAS 法测定氧化铝为载体的钯催化剂中钯的新方法，试验了微波消解溶样条件(溶解试剂、压力、时间和功率等)，研究了测定介质的影响，通过在样品测定液中加入铝基体至铝浓度为4 mg/mL，消除了铝对钯测定的干扰。

We also study characteristic index and its determination of complex flocculant, put forward the new concept of total basification degree and present the determined method of B〓.In this paper, the author studied and improved on the Ferron Timed Complex Colorimetry, put forward the determination principle and determined method of the improved Ferron Timed Complex Colorimetry, and determined successfully the iron and aluminum hydrolysis-polymerized species of FMA complex flocculation at the same time.

研究了复合絮凝剂的特性指标及其分析测定方法、复合絮凝剂的絮凝特性评价方法，提出了总碱化度作为复合絮凝剂特性指标的新概念，并给出了分析测定方法；研究改进了Ferron逐时配合比色法，提出了复合体系中铁铝水解聚合形态同时测定的测定原理及方法，成功地将其用于FMA中铁铝水解聚合形态的同时测定。

Methods: Adopting pig bile culture medium, the inhibiting or killing effects on pig bladder worm in vitro were observed;by using the methods of xylene-induced ear inflammation in mice and granuloma swelling induced by cotton ball in rats, the effects of anti-inflammation were observed;by using the methods of body twisting and hot-plate in mice, the effects of analgesia were observed. Through the mice auricle microcycle, the rats thrombus law in vitro and bleeding time, clotting time determination to the mice, the function of invigorating the blood were observed;adopting the penicillin abdominal cavity injection method, the mice epilepsy model were prepared, and epilepsy mice brain organization MDA content and SOD, ATPase vigor be measured by using chemical colorimetry.

利用猪胆汁培养基观察该方在体外对猪囊尾蚴的抑制或杀灭作用；采用二甲苯所致小鼠耳肿胀法、大鼠棉球肉芽肿法以观察该方的抗炎作用；采用热板法和化学刺激扭体法观察该方的镇痛效果；通过小鼠耳廓微循环法、大鼠体外血栓法和对小鼠出、凝血时的测定观察该方的活血作用；采用青霉素腹腔注射法制备小鼠癫痫模型，并利用化学比色法检测癫痫小鼠脑组织中MDA的含量及SOD、ATPase的活力。

HPLC, and its chemical structure elucidated on the basis of spectral analysis. A new method of RP-HPLC was established for the analysis of the contents of oleuropein, which is the main effective constituent. The contents of oleuropein in different positions of Syringa pubescens Turcz.

建立了测定橄榄苦甙含量的RP-HPLC法，并且利用这种方法测定了小叶丁香的不同部位——花、叶、茎和根之中的橄榄苦甙的含量；测定了不同条件下培养所得的培养物中橄榄苦甙的含量；测定了伴生菌培养物中橄榄苦甙的含量。

The pulse heating coulombic titration was applied to the determination of oxygen in titanium diboride,the titrimetry was studied to determine amounts of oxygen in titanium diboride,the determine method was established.

采用脉冲加热库仑滴定法测定二硼化钛中的氧，研究了二硼化钛中氧量的测定条件，建立了分析方法，能准确、快速地测定二硼化钛中的氧含量，并能推广应用于金属陶瓷材料中氧含量的测定。

The precision, linearity, anti -interference ability, recovery rate were compared among the 4 methods according to the standard method of NCCLS, and relativity between each of the 4 methods and modified diazotate J - G was calculated. Results

结果改良化学氧化法、钒酸氧化法、胆红素氧化酶法的批内精密度均小于3.0％；4种方法的回收率均在95.0％～105.0％之间；KHC3法、改良化学氧化法、钒酸氧化法和胆红素氧化酶法的线性范围分别是：0～424μmol／L、0-675μmol／L、0-629μmol／L、0-575μmol／L；胆红素氧化酶法和改良化学氧化法均有较强的抗干扰能力，和改良J-G法的测定结果有高度一致性。

Methods 1. The mice were divided into control and 3 Ganodermalucidum spores oil groups (at low, moderate and high doses), orally given forconsecutive 30 days. The body, spleen, thymus weight were observed, study on theeffect of the drug on the cellular immune function by proliferation and transformationof spleen lymphocytes test; study on the effect of the drug on the humoral immunefunction of mice by serum erythrocytolysin test; study on the effect of the drug on themononuclear macrophage function by carbon clearance and neutral red test.

实验方法 1设玉米油对照组和低、中、高三个灵芝孢子油剂量组，连续灌胃30天后观察小鼠体重、胸腺、脾脏重量指数；采用吞噬中性红和碳廓清实验测定对小鼠单核-巨噬细胞功能的影响；血清溶血素实验测定对小鼠体液免疫功能的影响；ConA诱导脾淋巴细胞转化实验测定对小鼠细胞免疫功能的影响；MTT法测定对小鼠NK细胞杀伤活性、脾细胞产生TNF-α和IL-2含量的影响。

The glyoxal and glyoxalic acid contents in the solution of oxidation of acetaldehyde to glyoxal by nitric acid were determined by this method, the repeatabilities of analysis results were excellent and the relative error compared to chemical analysis of glyoxal was 1.77%.

用HPLC测定乙醛硝酸氧化法制乙二醛反应液中乙二醛和乙醛酸的含量，结果的重复性好；对乙二醛的测定结果与应用化学分析法测定结果的平均相对误差为1.77%；对反应液中乙二醛、乙醛酸含量的测定有着较高的加标回收率，分别为99.6%～103.3%和98.1%～102.4%。

In this study, NBPT mixed proportionally with urea and NBPT without urea were applied to the soybean plants to analyze the effect of NBPT on the soybean root growth in root vigor, root nodule number and weight, and the activity of nitrogen fixation of root nodule.

为探索利用NBPT提高大豆生长发育的途径，对施用NBPT的大豆，利用氧化还原法，乙炔还原法和凯氏定氮法分别测定了大豆根系活性，根瘤固氮活性和植株含氮量，并测定了大豆根瘤的数量和重量。

We collected Leishmania promastigotes,washed its with 0.01mol/LpH7.2 buffers ,smashed its,and then measured protein content and titrated work concentration.2.We tested Kala-azar patients"serum and healthy persons"serum of epidemic area by ELISA. The results of three antigensmethods were the same, work concentration of serum was the same(l :100).Results:The protein content of three antigens is, 901 strain with 1000ug/ml,801 strain with 960ug/ml and 951 strain with 1100ug/ml. Suitable work concentration is, 901 strain with 10ug/ml ,801 strain with 12ug/ml and 951 strain with 11ug/ml.

1、抗原的提取：收集新疆不同地区分离得到的利什曼原虫前鞭毛体，经培养，用0.01mol/L pH7.2的磷酸盐缓冲液漂洗，超声粉碎，比色法测定其蛋白质含量，间接ELISA法滴定出抗原的工作稀释度。2、检测：用提取的三株抗原，分别进行间接ELISA法测定黑热病病人血清和疫区健康人血清抗体，并以肺结核病人血清、非疫区健康人血清做对照，三株抗原所用检测方法一致，血清工作稀释度均为1∶100。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。