测定时间

When proceeding the research of drug identification by ultraviolet spectrophotometry, this paper adopts the approaches below: to identify Metronidazole Buccal Tablets and Potassium Sodium Dehydroandroan Drographolide Succinate by ulviolet maximum absorbent wavelength; to identify Metronidazole Disodium Phosphate for Injection by ulviolet maximum absorbent wavelength and minimum absorbent wavelength; to identify Ceftriaxone Sodium for Injection and Clarithromycin Tablets by retention time of high performance liquid chromatography- ultraviolet spectrophotometry.

通过测定紫外最大吸收波长λ_(max鉴别甲硝唑口颊片和炎琥宁、测定紫外最大吸收波长λ_(max和最小吸收波长λ_(min鉴别注射用甲硝唑磷酸二钠，结合高效液相色谱(high performance liquid chromatography-ultraviolet detector，HPLC-UV)中保留时间的测定鉴别注射用头孢曲松钠和克拉霉素片，本文建立了药物鉴别的紫外分光光度法。

Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上，开展了如下未见文献报道的创新性的研究工作：(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究，建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法，与以前的报道相比，灵敏度和分析时间均有很大改善；(2)使用荧光素钠作为背景荧光试剂，建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法，扩大了激光诱导荧光检测的应用范围，对难衍生化合物的分离分析提供了一种新思路和新途径；(3)以荧光素钠作为背景荧光试剂，建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法；(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物，为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

Dynamic respiratory compliance and total respiratory resistance were measured before surgical incision, after sternal closure in the operating room, and after arrival in the intensive care unit. The following data were recorded: age, weight, preoperative pulmonary infiltrates, preoperative mechanical ventilation, evidence of increased PBF before surgery, duration of CPB, duration of aortic cross-clamp, duration of deep hypothermic circulatory arrest, use of steroids, and volume of ultrafiltrate removed.

分别在麻醉诱导后、手术结束关胸后和返回ICU后3个时间点测定患儿的肺动态顺应性和全肺阻力，并记录患儿年龄，体重，术前胸片浸润性改变情况，术前机械通气情况，术前肺血流量增高情况，体外循环时间，主动脉阻闭时间，深低温停循环时间和体外循环中超滤量等参数。

During using anaerobic fermentation slurry as insecticide, there had many problems that are random using, non-strictly prevention and curing time, non-suitable temperature and consistency mixture ratio ctc. In this research, fristly the different mixtures are made according to the different ratio of slurry to additive. Then the insecticidal effects of the mixture are tested in different conditions so as to find the good matches of slurry and additive in laboratory. According to the up result of the good matches extents of mixture, the field experiment is made to test the mixture's insecticidal chraricter and is further found new dosage form which has many good indexes such as good insecticidal effectiveness, little additive dosis ctc. So as to looking for the dosage form's synergism, the significant analysis is done and the characters of the dosages are tested which are ecological and environmental and the new types of dosage are determined. At last, for proving the dosage's field insecticidal potency, the wide field area experiments are done and four new style dosages are triturated which adapt ecological agriculture development. Aadditionally the effective period of the mixtures are tested when other experiments are done.

本文针对厌氧发酵液作为杀虫剂施用时，随用即配和无严格的增效剂种类、喷施时间及温度、浓度配比等现象，首先对各添加剂与厌氧发酵液配成的不同浓度的混和剂在不同条件下进行实验室测试，确定杀虫率高的浓度范围，进一步细化各混和剂浓度范围作田间试验，选出杀虫效果好，添加剂量少等各项指标都好的剂型并进行显著测定，确定出各剂型的增效情况；然后对选出的剂型进行生态和环保特性测定，以便确定新剂型，最后对选定剂型作大区试验来验证田间杀虫药效，最终研制出了4种适合生态农业发展的新型无污染药肥，并对选出的混合剂进行了有效期实验测定。

Methods 96 cases were devied into early stage group (60 cases, within three weeks )and later period group(36 cases, over three weeks).In early stage group, the time and degree of enophthalmos were observed. In later period group, the orbital volume behind the axis of the globe and degree of the enophthalmos were measured. The relation between the changes of orbital volume behind the axis of the globe and the degree of the enophthalmos was assessed by using Pearson correlation coefficients.

将96例患者按发病时间分为早期病例组（60例、受伤时间1周以内）和晚期病例组（36例、受伤时间3个月以上），早期组除进行后部眼眶容积测量外，分别于1周、2周、3周测定眼球突出度（相差＞1mm为阳性），记录眼球内陷出现时间，用卡方检验进行统计学分析；晚期组测量后部眶容积增大值和眼球内陷量，对其相关性采用Pearson统计方法进行统计学分析，并得出回归方程及相关系数。

Different samples' absorbent was determined in the condition of different colorimetric time ,different samples' temperature and different freshness,it prove that the result was relative to different experiment conditions in order to master the key point and ensuer the accuracy of the result in experiment.

啤酒双乙酰的含量是啤酒质量评价中的一项非常重要的指标，通过对不同样品在不同的比色时间、不同的样品温度及新鲜程度条件下测定其吸光度，得出不同实验条件对测定结果的影响，以求在实验中掌握好其关键点，确保测定结果的准确性。

Methods Several tests including primary eye care, tear break time, refractive analysis, facility of accommodation, phoria and FCC were done on 121 patients respectively.

方法分别对121例电脑终端病患者进行了眼科一般检查、泪膜破裂时间测定、屈光状态分析、调节灵活性测定、隐斜视及FCC测定。

Total gastrointestinal transit time, left colonic transit time, right colonic transit time and rectosigmoid colonic transit time were measured by the simplified method of radiopaque makers.Meanwhile, anorectal vector manometry was performed. The Constipation group was subdivided into Slow-transit group and Normal transit group according to the TGITT to explore the value of anorectal manometry in different types of constipation.

对28例便秘儿童和43例正常儿童进行全胃肠传输时间、左半结肠传输时间、右半结肠传输时间和直肠乙状结肠传输时间测定和直肠肛管向量测压(包括肛管压力、向量容积和对称指数)。

Phthalic acid esters are widely used in the many fields of industry. So many countries including China have come to pay attention to them and make up the codes for limiting the content in some products such as textile. By combining international codes, the thesis selects coating and textile that have close relative with people as objections. The research results are as follows:1. The thesis has established the textiles preparation method by a series of experimentations such as extraction solvent, extraction time, solid-phase extraction. The average recoveries of eleven phthalates are from 80.30% to 98.00%, and the relative standard deviations from 0.59% to 2.56%, the results show that this method is accurate and credible.2. The thesis set up the simultaneous determination of benzene, toluene, xylenes and phthalates in coatings.

邻苯二甲酸酯类化合物被广泛地应用在工业领域的各个方面，国际上已经开始重视邻苯二甲酸酯作为一种内分泌干扰素的危害性，对在一些产品中的用量作出了限制，但没有具体的分析测定方法，本论文结合国际法规选择了与人们生活密切相关的涂料和纺织品来研究其中邻苯二甲酸酯类环境激素的测定方法，研究内容如下：(1)通过对提取溶剂、提取方式、提取时间的选择实验以及固相萃取的一系列条件实验，首次建立了纺织品中测定邻苯二甲酸酯类环境激素的前处理方法，并对分析方法作了准确度、精密度验证。

The main research work of this dissertation is as follows: Based on the chemical reaction engineering theory and the nitrobenzene electroreduction mechanism, the plate and frame electrolyzer was designed and applied to the process of electroreduction nitrobenzene to p-aminophenol. This dissertation measured the residence time distribution data of the electrolyzer by means of the pulse response method and studied the rule of flow pattern along with the current capacity change. Under different conditions ,this dissertation studied the cyclic voltammetry properties of nitrobenzene on different electrodes by means of the dynamic cyclic voltammetry method and the electrode materials applied to the NB electroreduction have been selected primarily.Baseed on the results of cyclic voltammetry tests, this dissertation used p-electrode systems to measure the steady-state- polarization curves of nitrobenzene on different electrodes in H-type diaphragm cell, and obtained each primary factor s influence rule and the exchange current density value of each electrode.And then on the basis of the conclusions of fundamental researchs upword, the effects of influence factors on the the yield of p-aminophenol and the current efficiency,such as electrode material, current density, quantity of electricity circulated, nitrobenzene concentration . sulpuric acid concentration and so on, have been studied in detail in the systems of hign temperature , strong acidity and oxygen-poorthrough a series of electrolysis experiments in this paper.After all using Pb as anode Monel metal as cathode Dupont Nafion 417 cation-exchange membrane as membrane, this dissertation obtained the optimum technological condition: reaction temperature about 85C, current density 500A m-2, sulphuric acid concentration 20%wt.

论文的主要研究工作为：运用化学反应工程理论，结合硝基苯的电还原机理，设计出用于硝基苯直接电还原合成对氨基苯酚实验的板框式电解槽，并利用脉冲响应法测定了该板框式电解槽的停留时间分布数据，研究了流型随流量变化的规律；通过动态循环伏安法研究了硝基苯在不同电极上、不同条件下的循环伏安特性，初步评选出了用于硝基苯电还原的电极材料；结合循环伏安的测定结果，在H型隔膜电解槽中采用三电极体系测定了硝基苯在不同电极上、不同条件下的稳态极化曲线，得到了各主要因素的影响规律及硝基苯在各个电极上电还原的交换电流密度数值；在基础研究结论指导下，采用板框式电解槽，在高温、强酸、贫氧系统中，进行了一系列的电解实验，分别考察了电极材料、电流密度、通电量、硝基苯浓度、硫酸浓度等因素对收率及电流效率的影响，最终选择以蒙乃尔合金电极作为阴极、铅合金为阳极、Dupont Nofion 417阳离子交换膜为隔膜，得到由硝基苯直接电还原制对氨基苯酚的最佳电解工艺条件：反应温度85℃，电流密度500A·m~(-2)，硫酸浓度20％wt。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了