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A method for AAS determination of Palladium in Aluminum oxide matrixs by microwave digestion was reported in this paper.

报道了微波消解- AAS 法测定氧化铝为载体的钯催化剂中钯的新方法,试验了微波消解溶样条件(溶解试剂、压力、时间和功率等),研究了测定介质的影响,通过在样品测定液中加入铝基体至铝浓度为4 mg/mL,消除了铝对钯测定的干扰。

In the test range homogenizing speed and time and the centrifuge time all had small effect to the results.

在测定的范围内均质速度、均质时间、离心时间对测定结果的影响都很小。

The maximum relative standard deviation is 3.23%, which is close to that of the determination to low concentration COD samples.

本文利用顺序注射的特点,在COD测定加热的等待时间里,进行氨氮和pH的测定,使三项测量的时间大大缩短。

In the period of radish to grow leaf the fresh weight unit area was menstruate; and then in the period of radish to grow root the leaf heat injury index and death rate of plant in summer were menstruate, also the electric conductivity percentage or high temperature cause death time; Finally radish yield and effective root rate were menstruated in the harvests and accomplish to synthesize evaluation heat tolerance of radish.

由此形成在萝卜长叶期进行苗期单位面积叶鲜重测定;长根期测定叶片热害指数和越夏死株率,或进行电导百分率和高温致死时间测定;萝卜收获期测定有效根率,最后综合评价萝卜耐热性。

Methods By radioimmunoassay,we measured the contents of CGRP in mesencephalon and pituitary after reperfused 5 minute following 5 minute ischemia; reperfused 45 minute following 15 minute ischemia; reperfused 30 minute following 30 minute ischemia;and compared with controls(pseudo-operation, same time of ischemia and the same total time but only ischemia).

采用放射免疫测定方法,测定大鼠全脑缺血5 min再灌注5 min、缺血15 min再灌注45 min、缺血30 min再灌注30 min中脑及垂体CGRP含量变化,并与相同缺血时间组、假手术组及总时间相同但仅有缺血组相比。

breast cancer cell line MCF-7 were marked killed by trametes robiniphila murr in certain concentration. The IC50 of trametes robiniphila murr in three days to MCF-7 was about 0.05mg/ml. Its cell toxin were increased while the touched time was delayed or the concentration was advanced. Trametes robiniphila murr also can advance cell toxin of adriamycin and reverse resistance of MCF-7/Adr.

用MTT 法测定不同浓度的槐耳浸膏作用不同时间下对乳腺癌细胞系MCF-7 的杀伤作用,同时测定应用槐耳浸膏时对阿霉素的增敏作用和耐药逆转作用;结论:金克在一定范围内对乳腺癌细胞系具有明显的杀伤作用,其作用3 天时,IC50 在0.05mg/ml 左右,随着药物浓度升高和作用时间的延长其杀伤作用相应的增强,对阿霉素化疗具有增敏作用和逆转耐药作用。

A new method of disease area mensuration and the percentage of diseases area of tea leaves with computer has been established by using Photoshop software to scan many leaves at the same time, and the further investigation also has been fulfilled. The results showed that when scanned with resolution 150 dpi,there were be short time to scanning and less disk space beenoccupied, and the effect as same as scanned with high -resolution. The results of disease area mensuration and percentage of diseases area of tea leaves using the new method also as same as the results using artificial mensuration, and the efficiency of the new method is much higher than the efficiency of artificial method.

摘 要:建立了通过对茶树叶片进行扫描,利用Photoshop软件同时获得多张叶片及其受害部位的像素值,从而快速计算茶树叶片受害面积以及受害面积百分率的测定方法,并对此方法进行了系统的研究,结果表明:扫描分辨率为150dpi时,扫描时间和存储占用空间较优,测定效果和高分辨率扫描效果基本一致,该方法测定结果与人工测定结果无显著差异,其效率远远高于人工测定。

This paper introduced a single antioxidant extraction system--5% sulphosalicylic acid which could extract and assay ASA/DHA and GSH/GSSG simultaneously. Through analysis of kinetic curve of DTNB-GR recycling, the suitable time parameter was selected for the measurement GSH/GSSG. This system made the extraction of antioxidant quick and easy, and enhanced the accuracy, reproducibility and comparability for the antioxidant measurement through it compared to original method of extraction and measurement.

文章介绍了在一个单一提取系统—— 5 %磺基水杨酸中同时提取并测定了抗氧化剂 ASA/DHA和 GSH/GSSG,通过 DTNB— GR循环的动力学分析固定了 GSH/GSSG测定的最佳时间参数;通过与原提取和测定方法的比较,此法对于测定抗氧化剂有很好的准确性、重复性和可比性,使抗氧化剂的提取和测定变得简便快速。

A new blasting vibration method,which is different from the traditional method to measure the delay time of detonating cord detonator,is proposed through studying the testing process and principle.

通过观察导爆管雷管延期时间的测定过程和研究测定控制原理,提出了与传统测定方法不同的爆破振动测定方法。

METHODS Acute incomplete ischemia was induced by ligaturing bilateral carotid arterise and cutting heads in mice, the survival time and asthmatic time were observed; the coagulation timewas measured by sheet glass method,and the blood viscosity was also assayed; the platelet aggregation induced by collagen were studied by turbdimetry in vitro.

采用结扎小鼠双侧颈总动脉造成急性不完全性脑缺血模型,观察平均存活时间;另取小鼠断颅后测定断颅喘息时间;采用玻片法,观察胡芦巴总皂苷对凝血时间的影响;采用比浊法;观察其对体外血小板聚集率的影响,并测定全血粘度。

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