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The dilatometric curves of low-carbon micro-alloyed steel with Mo at different cooling rates were detected on Gleeble-3800 thermo-mechanical simulator.

在Gleeble-3800热模拟试验机上,测定了含Mo 低碳微合金钢在不同冷却速度下连续冷却时的膨胀曲线,利用热膨胀法并结合金相-硬度法,测定了该钢的连续冷却转变曲线;研究了冷却速度对该钢组织及硬度的影响。

By dilatometric change referencing microscopic test and hardness measurement, the critical point at Ac1, Ac3 and Ms of 27CrMo27S steel was determined in Gleeble-3800 thermal mechanical simulator, By measuring the different expanding curves of CCT in different cooling rate, CCT diagram was obtained.

利用膨胀法结合金相-硬度法,在Gleeble-3800热模拟机上测定了27CrMo27S钢的临界点Ac1、Ac3以及Ms;测定了该钢在不同冷却速度下连续冷却时的膨胀曲线,获得了连续冷却转变曲线;研究了冷却速度对该钢组织及硬度的影响。

By dilatometric change and microscopic test, the critical point at Ac1、Ar1、Ac3 and Ar3 of ML40Cr steel was detemined in Gleeble-3800 the thermal-mechanical simulator. The continuous cooling transformation diagram of ML40Cr steel was obtained by measuring the expanding curves of different cooling rates. The mechanical property and transformation of austenite were analyzed. The proper range of control cooling rate about ML40Cr cold heading steel was found. All those provide the reference for productive practice to develop cold heading steel.

在Gleeble-380热模拟试验机上采用热膨胀法-金相法测定了ML40Cr钢的临界点Ac1、Ar1、Ac3、Ar3,同时测定了在不同冷却速度下过冷奥氏体连续冷却时的膨胀曲线,获得了该钢的连续冷却转变曲线;研究了ML40Cr连续转变冷却过程中奥氏体转变过程和转变产物的组织和性能,初步确定了ML40Cr盘条的控制冷却范围,为冷镦钢ML40Cr盘条的开发提供了参考依据。

Because of rock formation drillability is very important to our dilling program,we need to design one equipment to test the rock formation drillability,which is rock formation drillability experment equipment..this equipment is delight and dependentable,which can quickly testing the rock formation drillability,This equipment has wide useful feature.

因为岩石可钻性对钻井工程有很重要的作用,所以我们需要设计一台测定岩石可钻性的实验设备,即岩石可钻性试验机。该设备轻便、可靠,能方便、快捷的测定岩石的可钻性,具有广阔的应用前景。

The standard is suitable for testing the density of benzene, toluene and dimethylbenzene of air in living district, and also suitable for density testing on benzene, toluene and dimethylbenzene of air indoor.

本标准适用于居住区大气中苯、甲苯和二甲苯浓度的测定。也适用于室内空气中苯、甲苯和二甲苯浓度的测定

Methods: European Pharmacopoeia and the content assay method enacted by State Food and Drug Administration (P. R. China) were employed to test and compare the content of diosmin produced by different companies. In present study, the content was used as the investigation index.

分别用欧洲药典和中国国家食品药品监督管理局标准制定的含量测定方法进行测定,从含量上对两种地奥司明片进行质量分析比较。

Of different seasons, and select the best herborization time. Then we compare the contents of general flavone, Diosmin, Palustroside and CHA in 10 samples, draw a conclusion that flavone, Diosmin and Palustroside are the representative index components in Quality standard, steady in different source.

对其质量标准进行了系统的研究,在不同采收期采集了蓬子菜样品,以总黄酮为指标,进行含量测定,确定了最佳采收期;还对不同产地的10个样品中总黄酮、香叶木苷、喇叭茶苷、绿原酸等活性成分进行含量比较,结果蓬子菜中黄酮类成分含量稳定,适于在制定质量标准时作为含量测定的指标成分。

A new method for determination of Pd using precipitation separation by butanedione dioxime as a selective reagent and complexometic titration EDTA released from EDTA-Pd complex was established.

建立了丁二肟选择性沉淀分离和析出EDTA-Pd络合物中的EDTA,Pb(NO3)2返滴定测定Pd的新方法,系统地研究了在硝酸或盐酸介质中测定Pd的条件,并对比了本法与《国家标准》分析方法的结果。

spectrophotometric method with phenol disulfonic acid ; ultraviolet spectrophotometer ; nitrate nitrogen ; comparison

本文通过对常用的酚二磺酸光度法和紫外分光光度法进行实验比对,同时调查云南省内两种分析方法考核的情况,从而找出两种方法的优缺点,供分析人员在实践中借鉴。l原理1.1酚二磺酸光度法测定的原理方法依据:GB7480一87《水质硝酸盐氮的测定酚二磺酸分光光度法》。用浓硫酸与苯酚作用生成酚二磺酸

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂,甲醇为溶剂的回流提取法来提取植物多酚,用显色反应检识酚羟基;采用紫外分光光度法对多酚粗体物进行总多酚含量的测定;选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌,采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验,并测定其最低抑菌浓度;采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析,根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

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