测定

Methods To determine the serum PCT of 35 patients with bacteriosis and 15 patients with nonbacterial disease by gold immunochromatographic assay,and determine C-reactive protein and alkaline phosphatase of neutrophilic granulocyte in corresponding period.

方法采用半定量的胶体金免疫结合法，测定35例细菌感染性疾病住院患者及15例非细菌感染性疾病住院患者的PCT，并同期测定患者C-反应蛋白与中性粒细胞碱性磷酸酶。

The contents of Mn, Cu, Fe, Zn in the leave, flower, seed of Impatiens balsamina induced by space flight are determined by flame atomic absorption spectrometry. The measure parameters for FAAS are optimized.

采用火焰原子吸收分光光度法测定了航天诱变凤仙花的茎、叶、花、种子中Mn、Cu、Fe、Zn四种微量元素的含量，优化了原子吸收分光光度法测定参数。

There are two methods to detect and quantitative analysis Neu5Ac, one is high performance liquid chromatography with the use of Aminex87H column, the other one is barbituric acid method.

对Neu5Ac的检测和定量也有两种方法，一种是利用Aminex87H酸性糖基柱，通过高效液相色谱测定；另一种是硫代巴比妥酸法测定。

The BAW detector combined with ion exclusion chromatography is used to determine short-carbon-chain organic acids in beehoney and beverages. NA and NAD in foods is also determined by IC-BAW.

本文以离子排斥色谱分离结合BAW检测，对峰蜜和饮料中的低分子有机酸进行了测定；也用离子交换色谱-BAW测定了常用食品中烟酸、烟酸胺的含量，实现质量监控。

This thesis includes five parts as follows.1. The backgrounds and some relative concepts of this work are briefly introduced. The photochemistry of benzamides and compounds with thiourea functional group is also concisely reviewed.2. Total of fourteen benzamides with different substituted groups have been synthesized and structurally characterized. Better photoreaction time for that kind of compounds at given concentrations is confirmed by tracking its'UV spectrum and GC chromatogram. A representative dibenzophenone photoproduct has been determined by X-ray crystallography. The mechanisms of photoreaction of benzamide have been proposed.3. Total of seven N-chloro(phenylmethylenebenzenamines with different substituted groups and sixty-one thiourea derivatives have been synthesized and structurally characterized.

论文的主要内容如下：1、简要介绍本论文工作的研究背景，并对苯甲酰胺和具有硫脲官能团类化合物的光化学研究进展进行简要的总结。2、合成与表征了14个具有不同取代基的苯甲酰胺类化合物，利用紫外光谱和气相色谱确定了此类化合物较佳光照时间，测定了一个具有代表性光解产物的单晶结构，提出了苯甲酰胺类化合物的光反应机理。3、合成与表征了7个带有不同取代基的氯代苯甲酰亚胺中间体及61个硫脲衍生物，测定了两个具有代表性化合物的单晶结构。

The SSAO activity was determined by using a radiochemi-cal assay based on 14C-labeled benzylamine as a sub...

SSAO活性用同位素标记法以14C-苯甲胺为底物进行测定，血糖则采用己糖激酶法测定。

In this thesis, a S~(2-) modified B-Z oscillating system has been successfully used to determine some heavy metal ions and through examining the influence of S~(2-) and benzylpenicillin sodium on B-Z chemical oscillating reaction highly sensitive detection methods of them have been developed.

本文主要研究了利用硫离子修饰的B-Z化学振荡体系对一些重金属离子的测定；同时利用经典的B-Z化学振荡体系对非金属硫离子进行了测定，并考察了药物青霉素G钠盐对该体系的动力学扰动行为。

The results show that the change in the oscillating period was linearly proportional to the concentration of Benzylpenicillin Sodium over the range from 2.47mg/L- 0.0123mg/L. Using the procedure, the content of the antibiotic in a bought production is determined and the result was consistent with that by HLPC.

实验结果表明，当体系中青霉素浓度在2.47mg/L-0.0123mg/L之间时，青霉素的浓度与进样后周期的变化率存在良好的线性关系，以此作为定量分析的基础，去测定市售注射用青霉素G钠的有效含量，与高效液相色谱测定结果一致。

Levels of lead, cadmium and copper in blood and urine were determined by atomic absorption spectroscopy, and frequencies of micronucleated binucleated cells in peripheral blood lymphocyte were measured by cytokinesis-blocked micronucleus assay.

采用石墨炉原子吸收光谱法检测血铅、血镉和尿铅、尿镉、尿铜含量，火焰原子吸收光谱法测定血清铜含量；胞质阻滞双微核实验测定淋巴细胞双微核率。

Blood and urine routine, blood biochemics were unchanged before and after treatment ; the adverse reactions were mild.

治疗前后做人工血压测定、24h动态血压测定、血生化检验、血常规、尿常规及心电图。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。