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Chapter 4 gives a micellar electrokinetic chromatography method for the quantitative analysis of seven podophyllum lignans in podophyllum emodi wall.

第四章:建立了胶束电动毛细管色谱法分离测定抗癌药物桃儿七中七种主要有效成分的新方法;利用二阶导数电泳图定量测定低含量和在实际样品没有达到基线分离的组份。

Polarimetry, the measurement of optical rotation, of a pharmaceutical article may be the only convenient means for distinguishing optically active isomers from each other and thus is an important criterion of identity and purity.

药用物质的旋光测定法,即测定光学旋转的方法,也许是用于区分具有光学活性的异构体的方法中唯一简便的方法。因此,该方法是鉴别和纯度的一个重要标准。

During the course of the experiment, the student will be exposed to fractional distillation under vacuum, gas chromatography, refractometry, polarimetry, and IR absorption spectroscopy.

气相色层分析,折光率的测定,旋光度的测定和红外吸收光谱。

The method shows wave polarogram law to determine uric lead, hand-in-hand travel analyses the data data that lead of make water of collect of hematic lead;, blood lead determines.

方法示波极谱法测定尿铅,血铅;汇总尿铅、血铅测定的数据资料并进行分析。

Based on the method of standard curve, the mathematical model of evaluation on uncertainty for determination of SudanⅠ in food by single scan polarography has been established in this paper. The related components of uncertainty were analyzed.

本文依据标准曲线法建立了单扫描极谱法测定食品中苏丹红Ⅰ的不确定度评定的数学模型,对影响测量结果的不确定度分量进行了分析,较全面地评定了测定结果的不确定度。

Of uncertainty were analyzed. A comprehensive evaluation on uncertainty of measured results of SudanⅠ in food by single scan polarography was carried out.

本文依据标准曲线法建立了单扫描极谱法测定食品中苏丹红Ⅰ的不确定度评定的数学模型,对影响测量结果的不确定度分量进行了分析,较全面地评定了测定结果的不确定度。

Methods The serum sICAM-1 was measured by ELISA in 20 patients with pollinosis and in 2 0 healthy persons as normal control group.The serum tIgE was analyzed with the P harmacia Uni-CAP System for two groups but Artemisia pollen-specific IgE was a ssayed only for patents group.

对20例花粉症患者及20名健康人采用酶联免疫吸附实验测定血清sICAM-1,用荧光免疫法测定血清tIgE和蒿草花粉特异性IgE(W6)。

It was applied to analyze the structures of ashless dispersants and their derivatives. The results were obtained and correlated. The molecular weight distribution and dipersity of ashless dispersant, number of polyisobutene R and polymeric degree of R polymerism in addition agent were obtained.

以Ultrastyragel为固定相,四氢呋喃作流动相,用普适标准校正曲线及凝胶渗透色谱法对无灰分散剂及其对应衍生物的结构进行了分析测定,并将测定结果相关联,计算出了无灰分散剂的相对分子质量分布、分散度及添加剂所含聚异丁烯R基的个数及R基聚合度。

The protein content was measured by using Ponceau S method and analyzed by one way ANOVA.

目前已有多种测定尿中蛋白含量的方法,临床应用较多的是 2 4h尿蛋白测定

Shenyang Research Institute of Chemical Industry, Shenyang 110021, China Abstract: Spectrophotometric analysis showed that the peak absorbance for food dye of Allura Red and biological dye of Ponceau-G occurred at 501 and 510 nm. In sunlight after 2, 4, 6, 8, 10 hours, the decomposition rates of Allura Red and Ponceau G were between 2.4 to 5.8% and 3.4 to 10.8%, so they are stable in sunlight. The recovery rates on cottons and glasses were very high, so they are easily recoveried from targets. Further studies showed that the recovery rates of two dyes on the leaves of wheat, cabbage, cucumber and tomato were different, so it need previously determine the recovery rate of tracer on the target crop to adjust the result. Field experiment showed it was easy to measure the pesticide spray distribution of high volume spay and low volume spray to use Allura Red and Ponceau-G as tracers.

沈阳化工研究院,沈阳 110021 摘要:光谱分析表明,食品染色剂诱惑红和生物染色剂丽春红-G的最大吸收波长分别为501 nm和510 nm ;在连续2、4、6、8、10 h阳光照射下,分解率分别在2.4%~5.8%和3.4%~10.8%之间,见光稳定性良好;两种染色剂在棉花叶片和玻璃片上的洗脱回收率都很高,说明易于从靶标上洗脱下来;进一步测定表明,两种染色剂在小麦、甘蓝、黄瓜、番茄叶片上的洗脱回收率各不相同,所以对准备进行测试的作物应先做一次洗脱回收率试验,用以校正测试结果;田间应用表明,用两种染色剂做示踪剂,可以方便地测定常量喷雾和低容量喷雾过程中农药在麦田的沉积分布情况。

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