测定

METHODS AK was purified by DEAE ion-exchange cellulose(DEAE-52) and sepharose Cl-4B .The component of the saccharide was determined by GC and TLC.Its MW was measure d by gel filtration.The form of glucosidic bond was detrermined by IR.The conten t of the saccharide was measured by colorimetry.

采用DEAE纤维素(DEAE-52)柱层析和凝胶柱层析分离纯化草乌多糖，气相色谱法和薄层层析法测定其多糖组成，凝胶过滤法测定其相对分子质量，红外光谱测定其苷键类型，比色法测定其糖含量。

The glyoxal and glyoxalic acid contents in the solution of oxidation of acetaldehyde to glyoxal by nitric acid were determined by this method, the repeatabilities of analysis results were excellent and the relative error compared to chemical analysis of glyoxal was 1.77%.

用HPLC测定乙醛硝酸氧化法制乙二醛反应液中乙二醛和乙醛酸的含量，结果的重复性好；对乙二醛的测定结果与应用化学分析法测定结果的平均相对误差为1.77%；对反应液中乙二醛、乙醛酸含量的测定有着较高的加标回收率，分别为99.6%～103.3%和98.1%～102.4%。

He sample is dissolved in a mixture of nitric acid and potassium chlorate.The determinations of Te,Bi,Fe and Cu are performed on a flame atomic absorption spectrophotometer.The selenium is determined photormetrically with 3,3'-diaminobenzidine,and the sulfur is determined gravimetrically as barium sulfate,precipitated frorm an EDTA-citric acid medium.

辉碲铋矿物经HNO＿3－KCIO＿3溶解，用火焰原子吸收法或乙二胺四乙酸二钠络合滴定法测定Bi，火焰原子吸收法测定Te、Fe、Cu，3，3＇二氨基联苯胺光度法测定Se，硫酸钡重量法测定S。

Based on the analysis and comparison of various methods of mensuration of effective ingredients of indigowoad root,phenol-vitriolic colorimetry has been choosen to be the method of mensuration of amylose in indigowoad root, and standard amylose graph has been made,in which c=22.476A+0.5309, correlation rate r=0.9970; Direct colorimetry has been choosen to be the method of mensuration of indigotin and Indirubin,and based on all above,the maximal absorb wavelenghes of indigotin and Indirubin have been determined through experiment.

在分析比较各种板蓝根有效成分测定方法的基础上，选用苯酚-硫酸比色法作为板蓝根多糖的定量测定方法，作山了多糖的标准曲线：c=22.476A+0.5309，其相关系数r=0.9970；选择直接比色测定法作为靛蓝、靛玉红的测定方法，并在此基础上通过试验确定了靛蓝、靛玉红的最大吸收波长及显色稳定性。

Analysis on main points for determination of chlorine dioxide by iodometric method ;2. The experiment results show: To measure sulfide in wastewater by iodometric method may have errors because the interferent can not be removed.

用碘量法测定废水中的硫化物，可能因无法消除干扰而使测定结果存在较大误差；对于同一废水样品，当碘量法和亚甲基蓝分光光度法的测定结果存在显著性差异时，可用Pb2半定量法进行判定；对于某些化纤企业的废水，用氢氧化钾-乙醇溶液洗涤沉淀，可消除碘量法测定的干扰。

An antibody binding to IGF-IR and inhibiting the binding of IGF-I and IGF-II to IGF-IR which is characterized in that said antibody is a is ofIgG1 isotype, b shows a ratio of IC50 values of inhibition of the binding of IGF-I to IGF-IR to the inhibition of binding of IG-II to IGF-IR of 1:3 to 3:1, c inhibits for at least 80% at a concentration of 5 nM IGF-IR phospohrylation in a cellular phosphorylation assay using 3T3 cells providing 400,000 to 600,000 molecules IGF-IR per cell in a medium containing 0.5% heat inactivated fetal calf serum when compared to such an assay without said antibody, and d shows no IGF-IR stimulating activity measured as IGF-IR phophorylation at a concentration of 10 M in a cellular phosphorylation assay using 3T3 providing 400,000 to 600,000 molecules IGF-IR per cell in a medium containing 0,5% heat inactivated fetal calf serum when compared to such an assay without said antibody has improved properties in antitumor therapy.

一种已经提高了抗肿瘤治疗的特性的抗体，所述抗体结合IGF-IR并且抑制IGF-I和IGF-II与IGF-IR结合，其特征在于所述抗体a是IgG1同种型，b显示其对IGF-I与IGF-IR结合的抑制的IC 50 值与其对IGF-II与IGF-IR结合的抑制的IC 50 值的比率为1∶3-3∶1，c当与没有所述抗体的这种测定比较时，其在5nM的浓度上，在包含0.5％的热灭活胎牛血清的培养基中，使用3T3细胞的细胞磷酸化测定中，抑制至少80％的IGF-IR磷酸化，所述3T3细胞提供400，000-600，000分子IGF-IR/细胞，和d当与没有所述抗体的这种测定相比，在包含0.5％的热灭活胎牛血清的培养基中，使用3T3的细胞磷酸化测定中，其在10μM的浓度上没有显示作为IGF-IR磷酸化所测量的IGF-IR刺激活性，所述3T3提供400，000-600，000分子IGF-IR/细胞。

The techniques for measuring Hevea laticiferous turgor pressure which have been reported are summarized. The commonly used three methods used for measuring Hevea laticiferous turgor pressure have their limitation in deep and systematic observation of the variation of Hevea laticiferous turgor pressure and are not involved in the study of the variation of laticiferous turgor pressure under the normal ethrel stimulated tapping system. A possibility of using an improved cell pressure probe method which has been recently established for other plants is discussed in accurate measurement of the real time variation of Hevea laticiferous turgor pressure.

本文综述了橡胶树乳管膨压的测定技术及其变化规律的研究结果，发现现有的几种乳管膨压测定技术均存在一定缺憾，对乳管膨压变化规律的研究也因测定方法等的限制不够深入、系统，且未与目前生产上普遍使用的乙烯利刺激割胶制度联系起来；并展望了将植物细胞压力探针技术改进后用于橡胶树乳管膨压测定研究的可能性。

In the paper, the multidentate carboxylic acid ligands were used to combine with Cd, resulting in the three dimensional MOCPs single crystals—C12H16CdN2O8, with a low temperature hydrothermal synthesis method. The sample was characterized with IR spectra to affirm the organic groups in the frameworks, single-crystal X-ray diffraction to determine the crystal structure and composition of the frameworks, N2 adsorption isotherms at low temperature to measure the specific surface area and pore size distribution, and with TGA/DGA analysis to scale the thermal stability. Furthermore, the dissolution property and the photocatalytic activity of MOCPs under the ultraviolet ray condition were explored.

本文用低温水热合成法，用多齿羧酸配体异烟酸和Cd配位合成出[Cd(C6H4O2N)2(H2O)4]∞三维晶体并进行了表征：采用红外光谱法确认骨架中的有机官能团；用单晶X射线衍射分析法测定MOCPs的晶体结构，并确定其骨架的组成；通过低温氮气吸附等温线测定了其比表面积和孔径分布；以热重分析和差热分析测定材料骨架的热稳定性；测定了晶体的溶解性能；最后以亚甲基蓝为目标降解物，对[Cd(C6H4O2N)2(H2O)4]∞的光催化活性及亚甲基蓝的氧化动力学进行了探索(来源：A2444BC论文网www.abclunwen.com)。

This research determines the change that analysed patient of mobile sex tuberculosis to treat around CRP, medium clinical import is evaluated in order to discuss CRP in phthisical curative effect. 1.1 average data choose 1 data and method to come from January 2005 August 2007 the patient of mobile sex tuberculosis of my courtyard be in hospital 120, all case of illness all combine the phlegmy smear, diagnose such as germiculture according to sternum of line of clinical expression, X or bosom CT, the tuberculosis that chooses case of illness to all accord with China cure to learn tuberculosis to learn branch to make is diagnosed and treat a guideline [2] , 120 all are patient of mobile sex tuberculosis is treated first, male 78, female 18 ～ is 73 42; age years old, average age (40 ± 6) year old. 1.2 methods are all patient early morning is hollow vein collects blood, the United States is used after detached serum elegant earth up Ci8200 full automatic biochemical analyzer determines, use scattering immunity to determine than chaotic law serum CRP level, and determine at the same time red blood cell sedimentations rate , bacterium of phlegmy n/med tuberculosis is checked of education of n/med tuberculosis bacterium...

本探究测定分析了活动性肺结核患者治疗前后CRP的变化，以探索CRP在肺结核疗效评估中的临床意义。1资料和方法1.1一般资料选自2005年1月至2007年8月我院住院的活动性肺结核患者120例，所有病例均根据临床表现、X线胸片或胸部CT结合痰涂片、细菌培养等确诊，所选病例均符合中华医学会结核病学会分会制定的肺结核诊断和治疗指南[2]，120例均为初治活动性肺结核患者，男78例，女42例；年龄18～73岁，平均年龄(40±6)岁。1.2方法所有患者清晨空腹静脉采血，分离血清后采用美国雅培Ci8200全自动生化分析仪测定，采用散射免疫比浊法测定血清CRP水平，且同时测定红细胞沉降率，痰结核菌检查。。。

In addition, a pre-column derivatization HPLC method was applied to the determination of Astragaloside Ⅳ; the flavonoids was determined by full-range HPLC scanning; a colorimetric method was developed for the determination of flavonoids and saponins. Hierarchical cluster analysis was performed on three constituents of different Radix Astragali species, and its result was compared with those of traditional phytoecological identification and the pharmacological quality assessment.

本研究以比色法测定了黄芪中总皂苷的含量，以柱前衍生化高效液相色谱法测定了黄芪中黄芪甲苷的含量；以比色法测定了黄芪中总黄酮成分的含量，以反相高效液相色谱法测定了黄芪中毛蕊异黄酮和毛蕊异黄酮苷的含量；以黄芪中的黄芪甲苷、毛蕊异黄酮和毛蕊异黄酮苷为主要特征对不同品种的黄芪进行了系统聚类分析，并将聚类结果与传统生药学鉴定和药理质量评价结果进行了比较。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。