测定

Therefore, trying to use nitrogen protection or in the condition of low temperature in the process of comminution are recommended, which can provide more reliable results than that in the air.

因此，建议在植物多酚的测定过程中，尽量采用氮气保护的方式，或者在低温的环境中进行，从而使测定的结果更加接近植物内的真实含量。

The impacts of different methods of comminution on the concentrations of condensed tannins in Tamarix rasosissima branches is investigated.

中文摘要：就目前植物多酚测定过程中不同的粉碎方法对测定结果的影响进行了研究。

The letterpress adopts the suitable solid reagent to take the place of the liquid sour and the organic reagent in the Diphenylcarbazide hydrazine intensity of light method (GB7467-87) to mensurate. hexavalent chromium in water.. It has carried out the rapid mensuration of chromium in water using entire solid commixture reagent and it selects affecting condions of the mensuration and maks the optimization .

为应对突发性水污染事故的现场应急监测， 2006年我中心购置的美国哈希便携式DR/2400型多参数仪，该设备适用于地表水和地下水等环境水中铬的测定，是一种准确、灵敏、快速、简便的测定仪，在2006年陕西镇安5-30水污染事故的应急监测中发挥的极其重要的作用，但由于该仪器所使用的试剂是专用的试剂，其价格昂贵、购置麻烦。

In this work, the digital analysis of six Al-based standard alloy samples with different content of Mg has been performed. Using spectra of Mg 518.36 nm as the analysis spectrum line, Cu 510.55 nm and Fe 510.75 nm as comparison spectrum lines separately, quantitative analysis has been made.

对6种不同镁元素含量的铝合金标准样品进行了数字化分析测定，探索了选用Mg 518.36 nm作为分析谱线，分别选用Cu 510.55 nm和Fe 510.75 nm作为比较谱线进行定量测定的方法。

The digital analysis of the three standard samples of the Al-based alloy with different content of Cu, and the probe into the quantitative analysis that employs the spectrums of Cu 510.55 nm and Fe 510.75 nm as the analysis spectrum and comparison spectrum, indicate the positive relationship between the content of copper and the intensity ratio of the analysis and comparison of spectrum.

对3种不同Cu元素含量的铝合金标准样品进行数字化分析测定，探索选用Cu 510.55nm谱线和Fe 510.75nm谱线分别作为分析谱线和比较谱线进行定量测定的方法，数据显示分析谱线和比较谱线的强度比值与Cu元素含量呈正比关系。

The digital analysis of the six standard samples of the Al-based alloy with different content of Cd, and the probe into the quantitative analysis that employs the spectrums of Cd 508.5 nm as the analysis spectrum, Cu510. 55 nm and Fe510.75 nm as comparison spectrum separately, indicate the positive relationship between the content of cadmium and the intensity ratio of the analysis and comparison of spectrum.

对6种不同Cd元素含量的铝合金标准样品进行了数字化分析测定，探索了选用Cd 508.58nm谱线作为分析谱线，分别选用Cu510.55nm和Fe510.75nm谱线作为比较谱线进行定量测定的方法，数据显示分析谱线和比较谱线的强度比值与Cd元素含量成正比关系。

Linear solvation energy relation was firstly introduced in the paper, and the method and step of gaining the special parameters of solvent and solute were introduced in detail, and these special parameters were used to selection and optimization of extractive agent in extractive distillation. The model of predicting activity coefficient at infinite dilution was established by linear solvation energy relation. By the above theory, several candidate solvents were selected to separate C5 fraction, and by experiment of vapor-liquid phase equilibrium at atmosphere pressure, the mixture of N-methyl-pyrrolidone including 4% water was used extractive agent of separating C5 fraction. Then binary vapor-liquid phase equilibrium of the some compound in C5 fraction and N-methyl-pyrolidone were determined at atmosphere pressure and correlated by NRTL equation. Isoprene being objective compound, experiments were operated in the laboratory-scale column; the processes were simulated by RadFrac model in ASPEN PLUS. And by the combination of experiment and simulation, the new process of separation of C5 was established.

本文首先对线性溶剂化能关系进行了分析介绍，也介绍了采用溶剂化能关系得到溶质溶剂特性参数的方法步骤，并将这些参数用于萃取精馏萃取剂的选择与优化；也通过线性溶剂化能关系式建立无限稀释活度系数预测模型，取得了一定的预测精度；将通过上述方法初选的溶剂进行了常压汽液平衡的测定研究，通过实验研究选定含水4%的N-甲基吡咯烷酮溶液做为C5分离的萃取剂，测定了大量N-甲基吡咯烷酮与C5组分的二元平衡数据，并进行关联计算；以异戊二烯为目标产物在实验室规模的精馏塔内进行了C5分离的实验研究，取得大量塔内数据；通过选用合适的热力学模型，采用ASPEN中RadFrac模块对分离过程进行模拟研究，通过实验与模拟相结合，建立了C5分离的新工艺，为将来的工业化打下了坚实的基础。

A series of structural parameters and component parameters of novolac resin were concluded through DEPT 135 spectrum of typical novolac resin with low or high mass fraction,including o-o,o-p and p-p condensation percentage of total condensation reaction;o-,p-percentage of active point in condensation reaction;reaction percentage of different active points;condensation ratioof phenolic resin in double ortho way and the average number of resin.

为准确了解线形酚醛树脂的组成和微细结构，利用高分辨率核磁共振技术中近年发展起来的DEPT135测定方法，测定了线形酚醛树脂的有关结构参数：o-o位缩聚百分率、o-p位缩聚百分率、p-p缩聚百分率；参与缩聚反应活性点中o位占据百分率、p占据百分率以及各个活性点参与反应百分率；同核双邻位缩聚值；不同类型酚醛树脂的平均核体数。

In this article, the effect of matrix on the intensity of RRS is analyzed theoretically based on the matrix negative absorption effect; the effect of pH is analyzed based on the conditional stability constant which is assayed by spectrophotometry; and MG and CV are analyzed qualitatively and quantitatively through detecting the intensity of RRS by the fluorescence spectrophotometer synchronously scanning.

本文采用负吸收效应，从理论上对体系基体的作用进行分析；采用紫外-可见分光光度计测定吸收光强度，求出缔合物的条件稳定常数，对体系酸效应进行分析；采用荧光分光光度计测定共振瑞利散射强度，对孔雀石绿和结晶紫进行定性、定量分析。

A precision device based on the conductance millivolt input notation method, connecting an electrical conductometer to a recorder, and with a deviation of ±5％ is established for the determination of the rate of dissolution of water-soluble polymer ic electrolyte.

采用电导仪连接记录仪，建立了一种测定水溶性高分子电解质溶解速度的精确方法——电导毫伏输出记谱法，测定偏差±5％。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。