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Abbe fold light meter to use passage measurement index of refraction simplicity may measurement water content of honey.

利用阿贝折光器,通过测定折光率可以简便的测定蜂蜜中的含水量。

The content of lipid peroxide was determined with fluorescence method, and the activity of superoxide dismutaseand glutathione peroxidase was determined with self-oxidation method of pyrognllol and Hafenam method, respectively.

脂质过氧化物含量按荧光法测定,超氧化物歧化酶活性应用邻苯三酚自氧化法测定,谷胱甘肽过氧化物酶活性按Hafenam方法测定

After 16 weeks treatment there are different improvements in patients'clinical expression, pain symptoms, blood sedimentation test in laboratory, CRP test and wrist joints' bone video picture ROI with isotope 99Tcm-MDP.

经16周初步临床治疗应用中,患者在临床表现、疼痛症状和实验室血沉测定、CRP测定和腕关节放射性核素99Tcm-MDP骨显像ROI测定均有不同程度的改善。

Modulus of elasticities of five kinds of wood members including purlin on the ridge of the roof, square purlin, round purlin, beam, sprocket from Grand Hall of Golden tile, Kumbum Monastery located in Qinghai Province were measured by using stress wave method.

采用应力波测定仪FAKOPP对塔尔寺大金瓦殿的脊檩、檩、梁、承椽檩、房椽等五种木构件的动弹性模量进行了测定,结果表明应力波无损检测可以有效的测定残余木构件的力学强度,不同种类木构件弹性模量保持率与其承重作用大小相关。

METHODS Dinitrofluorobenzene was used to induce the contact dermatitis in mouse ear, rhIL-11 0.375-1.5 mgkg^(-1)d^(-1) sc for 10 d, the degree of skin inflammatory reaction was observed. At the same time, the serum level of tumor necrosis factor-α and interleukin-6(IL-6) was measured by radioimmunoassay; the serum level of nitrogen monoxidum was detected by biochemical method and the expression of intercellular adhesion molecule-1(ICAM-1) was detected by immunohistochemical method.

采用2,4-二硝基氟苯致小鼠耳部皮肤接触性皮炎试验模型,观察sc rhIL-11 0.375~1.5mgkg^(-1)d^(-1),连续10d后皮肤炎症反应程度,同时采用放射免疫分析法测定血清中肿瘤坏死因子-α和白细胞介素-6(IL-6)的水平,采用生物化学检测法测定血清一氧化氮的水平,采用免疫组化法测定皮肤中细胞间粘附分子(ICAM-1)的表达。

As PTDT does in threshold traits, PTDT is valid not only for different QTL effect level, but also for maker with multiple alleles and multiple tightly linked markers.(2) Under an appropriate selection ratio s (in this study, s is 0.2, 0.4, 0.6, 0.8, respectively), the power of PTDT can be improved and the genotying individuals can be decreased using selective genotyping design. However, the power of PTDT is related with population size and population structure, an appropriate selection ratio can be defined by simulation based on the existing data.(3) Among the three transforming methods, mixed-family selection is the best, full-sib selection has same power to mixed-family selection in many parameter combinations, and Estimated Breeding Value selection is inferior to them.

数量性状QTL定位的模拟研究结果表明:(1)数量性状经有效转化后,PTDT对数量性状QTL定位保持了阈性状QTL定位的稳健与高效,对不同效应大小的QTL(10%,30%,50%)PTDT都是一个有效的分析方法;(2)在多等位基因标记、多标记方面,PTDT的检验功效与阐性状分析时一样高效;(3)在合适的选择率下(本研究的分别为0.2,0.4,0.6,0.8,1.0),选择性基因型测定不仅可以减少基因型测定的数量,而且可以提高PTDT的检验功效,但选择性基因型测定的PTDT检验功效很大程度上与群体大小和结构有关,这个可根据具体情况通过模拟找到一个合适的选择率;(4)三种转化方法的转化效力结果表明,家系内混合家系选择的转化效力最高,家系内全同胞选择次之,估计育种值选择的转化效力较差。

Theresult showed that the stability and accuracy of α-Si-Mo heterophony acid absorption photometry methodwere improved higher than that of β-Si-Mo heterophony acid method can be used for daily rapid analysisof high content of silicon in the ceramic chalk.

硅的测定方法很多,对于高硅(Si≥0.4%)样品的测定,一般采用重量法[1]或氟硅酸钾容量法,由于二者都需要把分解好的样品形成正硅酸沉淀进行过滤,然后分别进行测定

It has streptomycin and dihydrostreptomycin crossing rate of 100 %, simple sample pre-treatment including water dilution of milk sample and extraction with buffering phosphoric acid solution and pH regulation of pork and kidney sample, fast detection, high detection sensitivity up to 11.2 microgram/L and other advantages, and may be used in detection of residual streptomycin and similar medicines in animal food products.

本发明的检测链霉素药物的酶联免疫试剂盒为多残留检测试剂盒,链霉素和双氢链霉素的交叉率为100%;对样品的前处理要求低,样品前处理过程简单,牛奶样品用水稀释后可直接测定,猪肉和肾脏经磷酸缓冲液抽提后调pH即可上样,并且能同时快速检测大批样品;测定方法简单,省时,牛奶样品在1小时之内可得出测定结果;最低检测限达11.2μg/L,具有高特异性、高灵敏度、高精确度、高准确度等特点,可在动物性食品链霉素药物残留检测中发挥重要作用。

Methods:Unconfident Pk deficiency subjects from associate hospitals of Kunming Medical College.PK activity,thermostability, PEP kinetics, ATP inhibition and optimum pH were measured by ICSH recommended methods to confirm deficient in PK.The contents of Na~,K~,Ca~(2+),Mg~(2+) in erythrocyte PK deficiency were quatitated by inductively coupled plasma atomic emission spectrometry.

以昆医附院提供的PK缺陷可疑患者为研究对象,按照国际血液学标准委员会推荐的方法,对PK缺陷一个家系进行活性测定、热稳定性测试、PEP亲和力试验、ATP抑制试验及最适pH值测定,应用电感耦合等离子体原子发射光谱法测定红细胞钠、钾、钙、镁离子浓度。

The main research work of this dissertation is as follows: Based on the chemical reaction engineering theory and the nitrobenzene electroreduction mechanism, the plate and frame electrolyzer was designed and applied to the process of electroreduction nitrobenzene to p-aminophenol. This dissertation measured the residence time distribution data of the electrolyzer by means of the pulse response method and studied the rule of flow pattern along with the current capacity change. Under different conditions ,this dissertation studied the cyclic voltammetry properties of nitrobenzene on different electrodes by means of the dynamic cyclic voltammetry method and the electrode materials applied to the NB electroreduction have been selected primarily.Baseed on the results of cyclic voltammetry tests, this dissertation used p-electrode systems to measure the steady-state- polarization curves of nitrobenzene on different electrodes in H-type diaphragm cell, and obtained each primary factor s influence rule and the exchange current density value of each electrode.And then on the basis of the conclusions of fundamental researchs upword, the effects of influence factors on the the yield of p-aminophenol and the current efficiency,such as electrode material, current density, quantity of electricity circulated, nitrobenzene concentration . sulpuric acid concentration and so on, have been studied in detail in the systems of hign temperature , strong acidity and oxygen-poorthrough a series of electrolysis experiments in this paper.After all using Pb as anode Monel metal as cathode Dupont Nafion 417 cation-exchange membrane as membrane, this dissertation obtained the optimum technological condition: reaction temperature about 85C, current density 500A m-2, sulphuric acid concentration 20%wt.

论文的主要研究工作为:运用化学反应工程理论,结合硝基苯的电还原机理,设计出用于硝基苯直接电还原合成对氨基苯酚实验的板框式电解槽,并利用脉冲响应法测定了该板框式电解槽的停留时间分布数据,研究了流型随流量变化的规律;通过动态循环伏安法研究了硝基苯在不同电极上、不同条件下的循环伏安特性,初步评选出了用于硝基苯电还原的电极材料;结合循环伏安的测定结果,在H型隔膜电解槽中采用三电极体系测定了硝基苯在不同电极上、不同条件下的稳态极化曲线,得到了各主要因素的影响规律及硝基苯在各个电极上电还原的交换电流密度数值;在基础研究结论指导下,采用板框式电解槽,在高温、强酸、贫氧系统中,进行了一系列的电解实验,分别考察了电极材料、电流密度、通电量、硝基苯浓度、硫酸浓度等因素对收率及电流效率的影响,最终选择以蒙乃尔合金电极作为阴极、铅合金为阳极、Dupont Nofion 417阳离子交换膜为隔膜,得到由硝基苯直接电还原制对氨基苯酚的最佳电解工艺条件:反应温度85℃,电流密度500A·m~(-2),硫酸浓度20%wt。

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