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The compositions of complexes were determined as, by chemical and elemental analyses, Mn2CI2, Mn2Cl2, Cu2Cl2-2H2O, Cu(NO3)2-H2O, Cu(CH3COO)2, Zn2Cl2, Zn2(NO3)2-4H2O,ZnSO4 and Zn4(NO3)2, respectively. These complexes were characterized by IR,'H NMR and XPS. The crystal structures of these complexes were determined by single crystal X-ray diffraction techniques. The thermstability of the complexes was investigated by TG-DTG and the processes of their thermal decomposition were speculated. The constant-volume combustion energies of complexes, cU, were determined by a precision rotating bomb calorimeter at 298.15 K. Their standard enthalpies of formation, Hm, were calculated respectively. Finally, their biological activity was researched after the bactericidal activity was determined by selection of 1-2 bacteria.

通过化学分析、元素分析确定化合物分子组成分别为Mn_2Cl_2,Mn_2Cl_2,Cu_2Cl_2·2H_2O,Cu(NO_3)_2·H_2O,Cu(CH_3COO)_2,Zn_2Cl_2,Zn_2(NO_3)_2·4H_2O,ZnSO_4和Zn_4(NO_3)_2;借助IR、~1H NMR和XPS对化合物的键型特征进行了表征,运用X-射线单晶衍射分析法测定了个别化合物的晶体结构;以TG-DTG技术研究了化合物的热稳定性,阐明了它们的热分解机理;用精密转动弹热量计测定了化合物在298.15 K的恒容燃烧能,并计算了它们的标准燃烧焓和标准生成焓;选取1~2种病菌,初步测定了化合物的杀菌活性,进而研究了它们的生物活性。

In this experiment,X-ray diffraction apparatus was used forthe first time to examine and research on microdensity,crystallinity and microfibril angle.Through research on the radial variation of bamboo microdensity,this paper points out the conceptions of bamboo hull density and bamboo pulpdensity,and this provides basis for the multiple layer utilization of bamboo.Using computer image-processing technology to carry on precise examinationvolume fraction of bundle sheath,that is key factor to reveal the relationshipbetween bamboo structure and properties.For the first time using resonantvibration means to test the dynamic elastic module,the result shows very ideal.And for the first time researched on the variability of electric conductivityproperty of bamboo.

在本次实验中,首次使用X射线衍射仪对竹材的微密度、结晶度、微纤丝角进行测定和研究,深入研究了竹材微密度的径向变异规律,首次提出竹青密度和竹肉密度的概念,为竹材的径向分层利用提供依据;首次使用微机图象处理技术对竹材的组织比量,主要是纤维束比量进行了精确测定,从而为揭示竹材结构与材性关系打下基础;首次使用共振法对竹材的动态弹性模量进行测定和研究,测量结果是比较理想的;首次研究了竹材导电性的变异。

The amount of Na(superscript +), NH4(superscript +), K(superscript +), Mg(superscript 2+), Ca(superscript 2+), Zn(superscript 2+) in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography. And pyridine-2, 6-dicarbexylic was used as mobile phase to separated monovalent cations and pyridine-2, 6-dicarbexylic-ethylenedi-amine-oxalic acid was used as mobile phase to separated divalent cations.

采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na、NH4、K、Mg(上标 2+)、Ca(上标 2+)、Zn(上标 2+)的含量,其中一价阳离子以吡啶-2,6-二羧酸为淋洗液测定,二价阳离子以吡啶-2,6-二羧酸+乙二胺+草酸为淋洗液测定

The amount of Na+, NH4+, K+, Mg2+, Ca2+, Zn2+ in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography.

采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na+、NH4+、K+、Mg2+、Ca2+、Zn2+的含量,其中一价阳离子以吡啶-2,6-二羧酸为淋洗液测定,二价阳离子以吡啶-2,6-二羧酸+乙二胺+草酸为淋洗液测定

Methods A routine culture system of melanocytes was established, cells were irradiated with different dosages of UVB(30 and 90mJ/cm2 respectively), and then incubated with different concentrations of TMP for 72h. MTT method, NaOH assay and DOPA oxidization reaction were employed to determine the cell proliferation, melanin synthesis, tyrosinase activity of melanocytes.

常规分离培养正常人黑素细胞,分别用30mJ/cm2、90mJ/cm2的UVB照射细胞,然后加入100μg/ml、300μg/ml、600μg/ml的TMP孵育至72h,采用噻唑蓝法测定细胞增殖情况;多巴氧化法测定酪氨酸酶活性;NaOH裂解法测定黑素含量。

In order to study the seasonal fluctuations of the environmental factors in the burrows of plateau zokors, the temperature and humidity were measured directly by thermo-hygrometer, the water content of the soil was measured by using the drying cabinet, oxygen and carbon dioxide concentrations were measured using oxygen and carbon dioxide radiomete.

为了测定高原鼢鼠洞穴环境因子的季节性变化,我们用温湿度计、干燥箱和O_2、CO_2测定测定了春、夏、秋三个季节中高原鼢鼠洞道内的温湿度、土壤水分含量和气体组成。

The test groups were drenched orally with different dosages of compound Radix scutellariae granules. After being drenched orally for ten days, their thymus-index and spleen-nidex, immune globulins of IgA, IgG, IgM and alexins of C3, C4 of serum were defermined, and experiments in vivo were done. The mice-spleen's lymphocytes which were cultured in vivo were added with different concentrations of compound Radix scutellariae granules. The lymphocytes translation stimulate indexes were measured. The ability of licking up neutral red of the peritoneal macrophages cultured in vivo was measured in the groups.

应用复方黄芩颗粒给小鼠灌胃10d后,分别测定对照组与实验组胸腺指数、脾脏指数和血清中的免疫球蛋白IgA、IgG、IgM和补体C3、C4;并且进行体外实验,用不同浓度的复方黄芩颗粒剂对小鼠脾脏淋巴细胞进行体外培养,测定淋巴细胞转移刺激指数;在体外培养测定细胞吞噬中性红的能力。

Therefore,there were significant differences of amino acids digestibility of plant feedstuffs between cockerels and drakes,and the nutritional parameter of cockerel was not appropriate for drake.

以上结果表明,鸡和鸭对饲料氨基酸消化率存在显著差异,在所测定的7种植物饲料中大多数AAAD和TAAD测定值都是鸭比鸡高,目前以鸡测定各种饲料氨基酸消化率不适宜鸭的生产。

Dosimetry is defined as the measurement of the absorbed dose by the use of dosimeters.

辐射量测定是通过辐射量测定器来测定吸收剂量。

The model plants Arabidopsis and Rice have finished complete genome sequences in two Ecotypes and varieties.

模式植物拟南芥和水稻的全基因组序列测定己经完成,拟南芥有两种生态型完成了全序列测定,水稻有两个品种完成了全序列测定

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