测定

Choosing 50 patients that met the standard of catabatic period after treatment.We also survey the lung-function and the EOS count of peripheral blood of the 50 patients.Comparing with the data of two groups.If FEV1/FVC≥70%,normal;if the velocity of flow of 50% and 25% vital capacity (V50、V25) fact/predict＜70%,symbolizing small trachea functions abnormal.

对57例急性发作期哮喘患者做肺功能测定和取外周血进行EOS的计数，经治疗后选取符合缓解期标准的患者50例，也做肺功能测定和外周血EOS的计数，比较两期患者肺功能及EOS测定结果。

ROM of the following construct fixation with Codman plates, Window plates with grafts and 1 mm shortened grafts were measured respectively, and the graft height were determined for each specimens by physical measurement of discectomy site.

将12例小牛颈椎标本随机分成两组，用生物力学测定仪测定正常颈椎C(下标 4/5)节段在前屈、后伸、左右侧屈、左右旋转时的三维运动范围，然后切除C(下标 4/5)椎间盘，制成损伤模型，测定植骨加钢板，植骨块缩短1mm加钢板固定后C(下标 4/5)节段的ROM，植骨块的长度根据测量椎间隙的高度而定。

The content of Ti, Nb and Ta are colorimetrically determined by using H_2O_2, acetone-potassium sulfocyanate and pyrogallic acid respectively.

实验中采用了H_2O_2比色测定Ti，用丙酮-硫氰酸钾比色测定铌，用焦性没食子酸比色测定钽。

METHODS: The BEC were preincubated with crocetin (1, 0.1 and 0.01 μmol/L) for 12 h, then exposed to AGE (100 mg/L). The RAGE mRNA expression was detected by RT-PCR analysis, the intercellular adhesion molecule-1(ICAM-1) was measured by ELISA. The extracellular superoxide ion and thiobarbituric acid reactive substances were assessed with superoxide ion kit and colorimetric assay, respectively The intracellular I2O2 was also detected using the probe 2,7-dichlorofluorescein. The mitochondrial membrane potential and mitochondrial Succinate dehydrogenase were analyzed by the retention of rhodamine 123 (Rh123) and MTT.

不同浓度的西红花酸(1、0.1、0.01μmol/L)预孵BEC细胞12h后，用AGE(100mg/L)刺激细胞12h，RT-PCR法测定RAGEmRNA的表达水平；ELISA法测定细胞间黏附分子－(ICAM-1)的表达；试剂盒分别检测胞外超氧阴离子和硫代巴比妥酸反应产物浓度；同时，还用2，7-二氯荧光素测定了胞内H2O2的浓度，并用罗丹明123(Rh123)荧光法及MTT法分别检测细胞线粒体膜电位水平和其琥珀酸脱氢酶的活性。

Distillation device was slightly improved,analyzed by carbon dioxide and determined by water for the analysis of acetic acid from cuprammonia ,with recovery of 97%.

用蒸馏法测定醋酸铜氨液中醋酸的分析方法，操作简单，终点明显，但是在测定过程中二氧化碳对测定结果有很大影响。

The mechanism of Si Junzi Tang and panax sapogenol were studied on the effect of gastrointestinal cells protection by applying advanced technology of histochemistry, Holt′s cytodieresis mircocirculation, radio-immunity and subcellular ultrastructure.

进而应用酶组织化学、Holt细胞分裂测定、微循环测定、放射免疫测定、亚细胞超微结构观察等先进技术，研究四君子汤、人参皂甙抗胃肠细胞损伤、保护胃肠细胞的作用机理。

A novel method for determination of benzoyl peroxide with spectrophotometry was developed. Inclusion ratio of β cyclodextrin to dibenzoy peroxide and benzoic acid is obtained with spectrophotometry.The mechanism of the inclusion was studied,too. The results showed that β-CD react with dibenzoyl peroxide to form a 1:1 or 2:1 host-guest complex, with the apparent formation constants of 5.0× 10~2and 2.5× 10~4 , respectively.β-CD reacts with benzoic acid to form a 1:1 host-guest complex with the apparent formation constant of 6.9 × 10~2 after the dibenzoyl peroxide was reduced by hydroxyl ammonium chloride.

建立了用β环糊精测定过氧化苯甲酰的分光光度法，并测定了β环糊精与过氧化苯甲酰和苯甲酸的包结比，随着β-CD浓度的增大，可与BPO分别形成1：1或2：1的包容络合物，包结常数分别为5.0×10~2和2.5×10~4，与苯甲酸形成1：1的包容络合物，包结常数为6.9×10~2；由于包结物的吸光度值比过氧化苯甲酰的吸光度值大大增加，建立了一种当β-CD存在下，在水溶液中测定过氧化苯甲酰的方法。

A modified analysis method based on the determination of ozone—indigo disulphonate spectrophotometer(GB/T 15437-1995) in gas phase has been developed to detect the concentration of ozone in liquid phase. An analytical condition of λmax=612～615 nm,ε=20 000 L/, pH 2 is obtained by the titration of indigo disulphonate. Compared with potassium iodide method,it shows a higher precision and accuracy,CV＜3.0%. The results also prove that blank experiment will bring about 5.0%systematic error.

在气相臭氧浓度的靛蓝二磺酸钠分光光度法(GB/T15437-1995)基础上提出了液相臭氧浓度的测定方法，采用靛蓝二磺酸钠标准曲线法代替采用易分解的臭氧标准曲线法，得出测定条件λmax=612～615 nm、ε=20 000 L/、pH为2，通过碘量法比较实验，说明新的测定方法具有较高的精度和准确度，相对标准偏差小于3.0%；比较结果表明忽略空白实验将引入5.0%的系统误差。

During using anaerobic fermentation slurry as insecticide, there had many problems that are random using, non-strictly prevention and curing time, non-suitable temperature and consistency mixture ratio ctc. In this research, fristly the different mixtures are made according to the different ratio of slurry to additive. Then the insecticidal effects of the mixture are tested in different conditions so as to find the good matches of slurry and additive in laboratory. According to the up result of the good matches extents of mixture, the field experiment is made to test the mixture's insecticidal chraricter and is further found new dosage form which has many good indexes such as good insecticidal effectiveness, little additive dosis ctc. So as to looking for the dosage form's synergism, the significant analysis is done and the characters of the dosages are tested which are ecological and environmental and the new types of dosage are determined. At last, for proving the dosage's field insecticidal potency, the wide field area experiments are done and four new style dosages are triturated which adapt ecological agriculture development. Aadditionally the effective period of the mixtures are tested when other experiments are done.

本文针对厌氧发酵液作为杀虫剂施用时，随用即配和无严格的增效剂种类、喷施时间及温度、浓度配比等现象，首先对各添加剂与厌氧发酵液配成的不同浓度的混和剂在不同条件下进行实验室测试，确定杀虫率高的浓度范围，进一步细化各混和剂浓度范围作田间试验，选出杀虫效果好，添加剂量少等各项指标都好的剂型并进行显著测定，确定出各剂型的增效情况；然后对选出的剂型进行生态和环保特性测定，以便确定新剂型，最后对选定剂型作大区试验来验证田间杀虫药效，最终研制出了4种适合生态农业发展的新型无污染药肥，并对选出的混合剂进行了有效期实验测定。

METHODS: FRC and LCI were measured using a SF6 multibreathwashout technique while respiratory resistance and elastance were extracted from the input impedance obtained by forced oscillationtechnique in 18 children (3–8 yr) before and after oralpremedication with midazolam.

功能残气量和肺清除指数通过六氟化硫多次呼吸-洗出技术测定，而呼吸道的阻力和弹性回缩力则通过用力震荡技术中阻抗变化测定。研究共测定了18名儿童（3-8岁）使用咪唑安定前后的上述指标。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。