测定

We also study characteristic index and its determination of complex flocculant, put forward the new concept of total basification degree and present the determined method of B〓.In this paper, the author studied and improved on the Ferron Timed Complex Colorimetry, put forward the determination principle and determined method of the improved Ferron Timed Complex Colorimetry, and determined successfully the iron and aluminum hydrolysis-polymerized species of FMA complex flocculation at the same time.

研究了复合絮凝剂的特性指标及其分析测定方法、复合絮凝剂的絮凝特性评价方法，提出了总碱化度作为复合絮凝剂特性指标的新概念，并给出了分析测定方法；研究改进了Ferron逐时配合比色法，提出了复合体系中铁铝水解聚合形态同时测定的测定原理及方法，成功地将其用于FMA中铁铝水解聚合形态的同时测定。

A method for determinating the activities of pectinase was proposed in this paper. It can produce the red-brown amino compounds when 3,5-dinitrosalicylic acid and aldehyde were heated together. The amino compounds had maximum absorbency at 540nm. In certain range, there was a good linear relationship between the amount of reducing sugar and the color of the reaction mixture.

针对QB1502-92标准测定方法测定高活力果胶酶、固定化果胶酶活力存在的实验误差大，重现性及灵敏度差的缺陷，提出了利用3，5-二硝基水杨酸与醛糖共热产生棕红色的氨基化合物，在一定范围内还原糖的量和含有呈色氨基化合物的反应液颜色深浅成正比的原理，在540nm下测其吸光度，从而计算出果胶酶活力的测定方法，并对测定步骤、影响因素及测定中可能出现的问题进行了试验研究。

Now the research on HPL focus on dicotyledon, and the research on HPL of monocotyledon still havent been reported. In this paper, the research on cloning of rice HPL and enzyme activity assay were carried out and several result were obtained.1. Enzyme activity assay of rice HPLBased on the method of measure HPL Enzyme activity in other plants, the means on preparation of hydroperoxides and measurement rice HPL activity were set up. The 9-HPL arid 13-HPL activity of several rice varieties with different storability and different dormancy were tested.

本试验建立了水稻的HPL酶活性测定体系，测定了水稻萌发过程中的HPL酶活性，并进行了水稻HPL基因的克隆及表达研究，结果如下： 1、水稻HPL的酶活性测定在参考其它植物HPL酶活性测定方法的基础上，建立了水稻的HPL底物发生体系和酶活性测定体系，并测定了不同贮藏性水稻品种萌发过程中的种胚9-HPL、13-HPL活性和不同休眠性水稻品种种子的9-HPL、13-HPL酶活性。

Among them very multinomial and direct or indirect design reachs relevant industry to sensor, detailed situation is as follows: The computer reachs peripheral equipment: Hold pattern recognition of GPS receiver, graph and processing system; Microelectronics and photoelectron yuan parts of an apparatus: Cadmium of parts of an apparatus of coupling of CCD photoelectricity carry on one's shoulder, tellurium is mercuric , infra-red detector; CMOS image sensor; Communication equipment reachs a product: Smooth communication is metric with the instrument that monitor; Civil spacecraft reachs ground facilities: Spacecraft is lukewarm control a product; Automation machinery reachs device: Industrial robot and intelligent robot; Electromechanical key foundation: Intelligent air cylinder, intelligence changes model carapace breaker (voltage 380V, 660V, voltaic 1000A), prevent adopt device of dead apply the brake , the electron controls vehicle of the automatic gear-box, dynamoelectric steering gear that help strength, car to carry diagnostic system, gasoline engine electronic-controlled engine of device, derv is electronic-controlled car of device, alternative fuel changes device, car; Instrument appearance reachs a system: GPS car fixed position, monitoring calls the police attemper system, colliery installs all inspection to measure general management system, hydroelectric station to monitor control system, automatic cruise automatically to control a system (the car is auxiliary drive system), the electron collects fees administrative system (ceaseless car electron pays cost the system), two-phase; New-style medical apparatus and instruments: Medical sensor; Inorganic metalloid material: Component of the pottery and porcelain that suppress report, lukewarm characteristic thermal resistor ; New-style the sources of energy reachs equipment: The solar battery reachs package; The environment monitors an instrument: Monitor appearance, CO automatically to monitor appearance, automatic acid rain automatically sampler and determine appearance, soot, dust is automatic sampler and determine appearance, flue gas is automatic sampler and determine steam of end of appearance, car determines automatically appearance, portable poisonous and harmful gas determines quality of air of type of appearance, flow; The exploration of the sources of energy and mineral products resource develops device: MWD is followed get oil of logging instrument, numerical control monitor below well of deep well logging instrument, colliery reach calamity to forecast; The project measures and equipment of earthly physics observation: Project acceleration measures system, much general to strap weather radar (use be concerned with or double polarization technology), intelligence atmosphere sensor (contain lukewarm, press, irradiation level of wet, wind, precipitation, dew point, sun), personal computer control is automatic and perpendicular artesian well system , marine atmosphere; 1 2 of on one page issues one page

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The main products are: Hammer, thermal conductivity detector, permeameter, contraction of the expansion device, hand-held strain gauge, waterproof material detector, low-bending device, slag ball content in separators, heat load tester, performance test combustion furnace, a variety of thickness, thermal expansion of graphite electrode NG, coal strength meter, electric tamping device, hydrophobicity tester, mineral wool density meter, concrete drilling sampling machines, sawing machines, removed machine, setstube machine, hydraulic bending machine, impervious tester, determination of heat resistance, heating telescopic measuring device, an extension device, penetration tester, small meter, viscometer, drying time tester, pencil hardness tester, pendulum hardness, the adhesion tester, film zoned grid, and resistant to scrubbing detector, solvent resistance detector, wearable device, flat grinding device, wear-resistant coating shakeout device, staining resistance tester, impact tester , piercing instrument, instrument bending film, film coating, and sanding machines, cone-shaped grinding, high-speed dispersion machine, three roller grinder, Scratch tester, indentation tester, gloss Miriam, white tester, fresh video of Miriam, Miriam reflectivity, iron cobalt colorimeter, paint density cup, crack resistance testing apparatus, leveling device, flow hanging device, visual color box, the minimum temperature detector into a grinding, low temperature brittleness tester, visual color boxes, electronic pull machine, Mooney Viscometer, vulcanizing device, the proportion of direct-reading, the cold compression tester, heritage wearable device, Heritage scratch device, the friction coefficient detector, coating Detect zoned grid plate , coating resistance tester, such as burning a variety of test equipment.

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In this research, the activities of CWDE were measured by saccharifying according to the theory that red-brown amino compounds were produced when 3, 5-dinitro salicylic acid and aldehyde were heated together. And the testing conditions were made clear. The activity of Cx should be tested with optimal temperature of 50℃, optimal pH of 4.8, incubation time of 30 min, and optimal substrate of 0.6% CMC-Na. Due to the heat-libality, Cx should be sterilized more than 10 min. The testing conditions of the activity ofβ-G were almost the same with Cx except the substrate of 0.5% salicin and the sterilization time of more than 15 min.

主要取得了一下成果：(1)明确了条锈菌细胞壁降解酶活性测定的条件：羧甲基纤维素酶活性的测定条件为50℃，pH4.8，反应时间30min，底物浓度为0.6%羧甲基纤维素钠，以DNS法测定，且失活酶液的灭活时间应大于10min；β-葡萄糖苷酶活性的测定条件为：50℃，pH4.8，反应时间30min，底物浓度为0.5%水杨苷，以DNS法测定，且失活酶液的灭活时间应大于15min；果胶酶活性的测定条件为：50℃，pH4.8，反应时间1h，底物浓度为0.25%果胶，以DNS法测定，且失活酶液的灭活时间应大于10min。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小，进行综合分析，确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量，测定条件：加入100ml浓度为8.0±0.1％的氢氧化钠，在恒温水浴中煮沸回流6h；采用溶剂萃取法测定JOB-1C中TATB的含量，选择TATB饱和的二甲基甲酰胺为萃取溶剂，用G4坩埚式过虑器进行萃取分离；采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量，通过实验确定了多波长组合：λ=267nm，275nm，283nm，291nm，299nm；朗波—比耳定律的适用范围为PNP浓度：0.005～0.025mg/ml，HMX浓度：0.06～0.30mg/ml；在测定波长下，对PNP、HMX标准溶液的吸光度—浓度进行线性回归，由回归曲线的斜率得出PNP、HMX的吸收系数；根据朗波—比耳定律和吸光度加和性原理，在测定波长下，对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归，回归曲线的斜率即为混合溶液中PNP的浓度。

Potassium, natrium determines it is good that use ion chooses electrode indirect method it is better also with indirect method to determine at calcium of direct way;, it is next occasionally phosphor of; of law of azotic arsenic Ⅲ determines use phosphor molybdic acid is ultraviolet law outcome is better it is better with result of law of personal candy kinase that; blood sugar determines; urea determines use Niao enzymatic ultraviolet anhydride of better; flesh uses rate law result enzymatic law outcome is better; albumin determines, it is vanadium acid next alkalescent phosphoric acid of oxidation law; is enzymatic determine outcome of fluid of use AMP amortize is better; amylase determines law of thing of enzymatic standard background and iodic colorimetric law coefficient of variation all bigger, former a bit small, latter of percent of pass is tallish, each lab can try to choose according to his condition.

结论钾、钠测定使用离子选择电极间接法好于直接法；钙测定用间接法也较好，其次是偶氮砷Ⅲ法；磷测定使用磷钼酸紫外法结果较好；血糖测定用己糖激酶法结果较好；尿素测定用脲酶紫外速率法结果较好；肌酐用酶法结果较好；白蛋白测定用溴甲酚绿法较好；胆红素测定用酶法结果好，其次是钒酸氧化法；碱性磷酸酶测定使用AMP缓冲液结果较好；淀粉酶测定酶法底物法和碘比色法变异系数均较大，前者稍小，合格率后者稍高，各实验室可根据自己的条件加以选用。

Serum alt,ast,and bile acid were observed by enzyme assay and the ratio of ast/alt was worked out. serum bilirubin was measured by peariman and lee method. serum albumin was tested by bromphenol assay and was simultaneously measured to hyaluronic acid, type ⅲ procollagen, laminin and type ⅳ collagen by ria. meanwhile, prothrombin time and platelet count were measured and so on. results: the level of serum aca was raised increasingly in different cirrhotic cases with different classifications of child-pugh, according to severity of the condition.

应用酶联免疫吸附法分别对不同分级的肝硬化患者血清中抗心磷脂抗体的含量进行了测定；用酶法测定了alt、ast与胆汁酸并计算ast/alt值；用peariman和lee改良法测定血清胆红素；用溴甲酚氯比色法测定血清白蛋白；用放射免疫分析法测定透明质酸、ⅲ型前胶原氮端肽、层粘连蛋白与ⅳ型胶原；并测定了凝血酶原时间与血小板计数等相关指标。

Using dual energy X-ray bone density instrument XR-36 model to detect the bone mineral density of the left femur of the rats. Using the strain test system, we examined the biomechanics index according the tension and three-spot bending test; we also examined the bone calcium of the lumbar vertebra through plasma emission spectroscopy . We examined the serum calcium and magnesium by using the nomal biomechanics method,and examined the serum acid phosphatase and osteocalcin by using the Elisa method.

使用NORLAND公司XR-36型双能X线骨密度仪，采用小动物骨密度测定软件，测定大鼠左后肢股骨的骨密度；使用应变测试系统，按股骨拉伸和三点弯曲试验，测定股骨生物力学指标；以等离子体发射光谱法测定腰椎骨骨钙含量；以常规生化法测定血清钙、镁含量及血清酸性磷酸酶含量；以Elisa法测定骨钙素含量。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。