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洗涤瓶

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The molecular sieve is prepared in the steps: at the room temperature, hexadecyl trimethyl ammonium bromide is mixed and dissolved with the sodium hydroxide, and is added with TEOS in dropping way, and simultaneously added with Me metal salt water solution and lanthanum nitrate solution in dropping way; the pH value of the mixed solution is adjusted by acetic acid to be 10 to 11, and is mixed for 1 to 2 hours after being stabilized; the sol is moved into a polyfluortetraethylene bottle to be heated and crystallized for 2 days in the oven at the temperature of 100 DEG C; after filtering, washing and drying for nights, and being calcined in a muffle at the temperature of 550 DEG C for 3 to 7 hours, the dual-metal-atom improved MCM-41 mesoporous molecular sieve is obtained.

该分子筛的制备为室温下,将十六烷基三甲基溴化铵和氢氧化钠混合溶解,搅拌并滴加入TEOS,同时滴加入Me金属盐水溶液和硝酸镧溶液并搅拌,用乙酸调节pH值至10~11,稳定后搅拌1~2小时,溶胶转入聚四氟乙烯瓶中在100℃下烘箱水热晶化2天,经过滤、洗涤、干燥过夜,马弗炉550℃焙烧3-7h,得双金属原子改性MCM-41介孔分子筛产品。

Specific products include: vacuum system cream machine, vacuum homogeneous emulsifying machine, mixer, reactor type, such as Cream, washing type, spices class production equipment; automatic aluminum composite hoses and plastic hose pipe production line, the kinds of specification type hose filling Sealing Machine, color filling Sealing Machine, hoses and other hose-type printing press production equipment; have liquid Filling Capping, capping machine, eye drops, oral liquid filling torinese plus spin to build machines and other types of packaging equipment bottle; have all kinds of liquid, cream, powder, granule packaging machine pouch; all kinds of stainless steel conveyor table; water treatment equipment; a variety of specifications for the pipeline system mold; stainless steel Clean Benches, cabinets, aircraft; soap production lines.

具体产品有:真空制膏机、真空均质乳化机、搅拌机、反应釜等膏霜类、洗涤类、调料类的生产设备;全自动铝塑复合软管和塑料软管的制管生产线、各种规格类型软管的灌装封尾机、彩条灌装封尾机、软管印刷机等软管类生产设备;有液体灌装旋盖、轧盖机,眼药水、口服液的灌装加内塞旋盖机等瓶类包装设备;有各类液体、膏霜、粉剂、颗粒的小袋包装机;各类不锈钢输送工作台;水处理设备;各种规格制管线模具;不锈钢超净工作台、柜、架;香皂生产线等。

The process includes the following steps: dissolving bromine in halogenated hydrocarbon, dropping the bromine solution into reactant system comprising pentabromo toluene, halogenated hydrocarbon, free radical initiator and hydrogen peroxide at 50-65 deg.c, and heating to 60-78 deg.c for reflux reaction until the reactant system becomes transparent; filtering the resultant to obtain solid product, washing with carbon tetrachloride and water separately and vacuum drying to obtain pentabromo benzyl bromide.

具体步骤为:将五溴甲苯、卤代烃、自由基引发剂和过氧化氢组成的反应体系加入到三颈瓶中,将0.07~0.1mol的溴溶于50ml卤代烃配成溶液,在50-65℃温度下滴加到反应体系中,滴加时间为50-70分钟,然后升温至60-78℃温度下回流反应,至反应体系逐渐变透明,且不再产生气泡时,将所得产物过滤,得到固体产物,分别用CCl 4 和水洗涤,真空干燥,即得到五溴苄基溴;其中,五溴甲苯与溴的摩尔比为1∶0.7-1∶1.0,溴与过氧化氢的摩尔比为1∶1.0-1∶1.4,自由基引发剂加入量为五溴甲苯重量的1-10%,卤代烃的加入量为反应体系体积的40%-100%,所用溶剂可以直接进行下一批反应,不需要更换溶剂或蒸馏提纯。

Automatic multilayer-extruding bottle-blowing machine can be widely applied to produce hollow plastics like cosmetic bottles, washing bottles, milk bottles, medicine bottles, toy bottles, chemical bottles, etc. There are two kinds: pneumatic system and hydraulic system.

多层共挤自动瓶机广泛用于生产各种档次的化妆品瓶、洗涤瓶、牛奶瓶、药瓶、玩具瓶、化工瓶等中空塑料制品,有气动系统及液压系统两种。

Methods Cells were maintained in DMEM medium with 10% fetal bovine serum. Five days before the beginning of experiments, the cells were seeded in phenol red-free DMEM medium containing 5% charcoal dextran-treated FBS. The cells were harvested, and seeded in 6-well culture plates or in 75ml flacks. After NP, BisA and DBP treatments for 72h, the cells were harvested, and mRNA and protein expression of PCNA, bcl-2 and bax were detected by reverse transcription-polymerase chain reaction and immunohistochemistry, respectively.

方法]T47D细胞在含10%胎牛血清的DMEM培养液中进行常规传代培养,实验前将细胞转移至无酚红DMEM(含5%活性碳葡聚糖苷处理过的FBS)中继续培养5d,收集细胞,PBS洗涤后接种於内置盖玻片的6孔板或75ml培养瓶中,用32×10^(-7)mol/L NP、32×10^(-7)mol/L BisA及32×10^(-6)mol/L DBP对细胞分别处理72h,用半定量RT-PCR技术观察这3种化合物对核增殖抗原PCNA、bcl-2及bax mRNA表达的影响,并用免疫组化方法对结果进行验证。

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