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The product has green-yellow fluorescence at excitation wavelength of 355 nm and emission wavelength of 478 nm, and the fluorescence intensity could be enhanced in the presence of acetone.

三、流动注射在线氧化荧光法测定氯普噻吨的的研究利用在硫酸介质中二氧化铅可使无天然荧光的氯普噻吨氧化而转变为在最大激发波长和最大发射波长分别为393nm和452nm的强荧光物质,而且丙酮对该荧光体系有强烈增敏作用的现象,建立了以醋酸纤维素固定化的二氧化铅作为固相反应器的流动注射在线氧化荧光法测定氯普噻吨的新方法。

Flow injection fluorometry for the determination of carbamazepine in pharmaceuticals and plasmaA simple, sensitive and specific spectrofluorimetric method has been developed for the determination of CBZ. The method was based on lead dioxide solid-phase reactor flow injection on-line oxidizing CBZ into fluorescent product in medium of phosphoric acid. The product has green-yellow fluorescence at excitation wavelength of 355 nm and emission wavelength of 478 nm, and the fluorescence intensity could be enhanced in the presence of acetone. The reaction conditions and experimental conditions were studied and optimized.

二、流动注射在线氧化荧光法测定卡马西平的研究利用卡马西平自身无荧光,经过氧化后可转变为在最大激发波长为355nm,最大发射波长为478nm的强荧光物质,而且丙酮对该荧光体系有增敏作用的现象,应用流动注射体系建立了以醋酸纤维素固定化的二氧化铅作为固相反应器、在磷酸介质中在线氧化荧光法测定卡马西平的新方法。

UV and NIR were used for online detecting in this study. Furthermore, some chemometrics algorithms such as SMLR, PCR, PLS, SVM, etc. were used to establish the rapid quality evaluation methods of the raw materials, intermediates and preparation of Qingkailing injection. This study provided an example of online quality control of Chinese medicine injection and oral liqid. The formula of Qingkailing injection is composed of cholic acid, hyodeoxycholic acid, Cornu Bubali, baicalin, Radix Isatidis, Fructus Gardeniae, Flos Lonicerae Japonicae and Concha Margaritifera.

本研究采用适合在线检测要求的紫外光谱和近红外光谱分析技术,结合逐步多元线性回归、主成分回归、偏最小二乘和支持向量机等化学计量学方法建立清开灵注射剂生产原料药、中间体和成品的快速质量评价方法,为中药注射剂及口服液的在线质量控制提供研究思路。

According to the function and structure and dimension of junction box , the material capability and injecting technology were analyzed, the structure of injection mold was designed.

根据接线盒盒体的功能、结构与尺寸,进行了材料性能、注射工艺等分析,设计了注射模。

The results of this study show that repeated injection of nicotine can lead to tolerance of hypothermic response, but motor activity response of females was significantly greater than the male rats after sequential nicotine injections.

重复注射烟碱可导致雄性和雌性大鼠出现降温耐受性反应,但连续注射烟碱后,雌性大鼠的活动明显大于雄性大鼠。

The operation takes threee points "z" internal ligations 4cm above the dentate line on rectum's right-front, right-back and left to suspended suture the prolapse of anal cushion , then Xiaozhiling was injected under the ligation point.

目的 探讨应用肛垫悬吊联合消痔灵注射治疗痔的可行性和安全性。方法在齿线上4cm,直肠左侧、右上、右下,用可吸收线&Z&形缝合悬吊肛垫并在黏膜下注射消痔灵。治疗痔50例,其中混合痔32例,内痔18例。

Rats in the group R and group M were exposed to thoracic radiation at a dose of 20 Gy by linear accelerator after intrabdminal injection pentobarbital Sodium by 40 mg/kg.

照射组和治疗组腹腔内注射戊巴比妥钠40 mg/kg给予直线加速器照射,照射剂量单次20 Gy/min,照射前7 d,照射组给予等量生理盐水腹腔内注射,治疗组给予氨溴索35 mg/kg。

Lidocaine and cefazolin sodium solution 1ml each were added to 20ml of HPAG. Then the mixed gel were injected into subdermis or mascle of guinea-pigs 0.5~2ml at each point with 18 gauge needle.

实验组以2%利多卡因1ml与头孢唑啉钠溶液1ml稀释水凝胶后,用18号注射针头将其注入到豚鼠皮下或肌肉层,每个部位注射量为0.5~2ml。

After IP administration of meperidine 50 mg the plasma concentration (median average 55–60 g/L) was approximately half that of an equivalent intramuscular dose (median average 113 g/L).

腹腔内注射50mg 哌替啶后的血浆浓度(中位数为55-60g/L )大约是同等剂量肌内注射时(中位数为113g/L )的一半。

After IP administration of meperidine 50 mg the plasma concentration (median average 55–60 g/L) was approximately half that of an equivalent intramuscular dose (median average 113 g/L).

腹腔内注射50mg 呱替啶后的血浆浓度(中位数为55-60g/L )大约是同等剂量肌内注射时(中位数为113g/L )的一半。

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