波谱

We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR）, among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-（2'-glycerin）-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl）-β-D-galactopyranoside; ethyl rosemarinate.

我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究，利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物，经化学方法和波谱技术（红外，质谱，一维和二维核磁共振谱）鉴定了二十五个化合物的结构，其中四个为新的化合物，它们分别是：异海松-15-烯-3β，8β，20-三醇；苯乙醇-3-O-（2'-甘油基）-5-O-β-D-吡喃葡萄糖甙；3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙；迷迭香酸乙酯。

DATA EXTRACTION: MRS defines the dynamic changes of cerebral metabolic substance following traumatic brain injury, and such changes in the white matter suggest the degree of neuraxon injury, while those in the gray matter indicate the state of brain laceration.

资料提炼：磁共振波谱分析可反映创伤性脑损伤后活体脑组织代谢物质的动态变化。

If you look at the history of research on nonionizing radiation (the energy waves below the frequencies of visible light on the electromagnetic spectrum), you will see that nonthermal effects were first reported decades ago, but were deemed to be research mistakes.

如果你看看历史的研究nonionizing辐射（能量波的频率低于可见光的电磁波谱），你将看到，非热效应首次报道十年前，但被认为是研究的错误。

Finally, this project setup a pile station near Taichung harbor. Monitoring and maintenance will continuously to be done to supply oceanographical data for further application.

本计画除上述时空域方向波谱的探讨外，同时并研究发展波浪量测技术，冀能观测得珍贵波浪资料予各界分析研究。

Based on relative literatures,this part has included five resesearch aspects as below.1 Fifteen compounds were isolated and purified by extraction,column chromatography,and their structures were determined on the basis of spectral analysis: acteoside(Ⅰ-1),isoacteoside(Ⅰ-2),crenatoside(Ⅰ-3),cistanoside F(Ⅰ-4),sinapoyl-4-O-β-D-glucoside(Ⅰ-5),adenosine(Ⅰ-6),β-siterol(Ⅰ-7),oleanic acid(Ⅰ-8), succinic acid(Ⅰ-9),caffeic acid(Ⅰ-10),protocatechuic aldehyde(Ⅰ-11),p-hydro xybenzyl alcohol(Ⅰ-12),β-daucosterol(Ⅰ-13),D-galacitol(Ⅰ-14),D-mannitol(Ⅰ-15).Ⅰ-4～15 were obtained from this plant for the first time,andⅠ-6,7,9,and 13 were isolated from Orobanche genus for the first time.2 The scavenging test of DPPH showed that most compounds have comparative antioxidant activity as L-ascorbic acid and part of them show better activity such as the O.coerulescens extract and phenylethanoid glycosides.Acteoside showed potent free radical scavenging effects with a median inhibition concentration of 25.6μg/ml.3 The anti-HBV activities of acteoside,isoacteoside and crenatoside were measured,and all of them showed suppressive activity on the expression of HBsAg and HBeAg in the HepG2.2.15 cell line.

本论文在文献调研基础上对紫花列当化学成分及生物活性进行了研究，并从免疫抗病毒角度探讨紫花列当中特征性成分类叶升麻苷的肝保护作用及其机制。1采用大孔树脂、硅胶和Sephadex LH-20等色谱技术对紫花列当进行系统的植物化学研究，从中分离得到19个化合物，利用UV和NMR等波谱手段及理化性质鉴定了其中的15个化合物，分别为类叶升麻苷(Ⅰ-1)、异类叶升麻苷(Ⅰ-2)、crenatoside(Ⅰ-3)、cistanoside F(Ⅰ-4)、sinapoyl-4-O-β-D-glucoside(Ⅰ-5)、腺苷(Ⅰ-6)、β-谷甾醇(Ⅰ-7)、齐墩果酸(Ⅰ-8)、琥珀酸(Ⅰ-9)、咖啡酸(Ⅰ-10)、原儿茶醛(Ⅰ-11)、对羟甲基苯甲酸(Ⅰ-12)、β-胡萝卜苷(Ⅰ-13)、D-半乳糖醇(Ⅰ-14)和甘露醇(Ⅰ-15除化合物Ⅰ-1、Ⅰ-2和Ⅰ-3外，其余化合物均为首次从该植物中分离得到。2)通过大孔树脂富集该药材有效部位苯乙醇总苷，并采用HPLC测得其所含特征性成分类叶升麻苷的含量可达80%以上。3DPPH自由基清除试验显示紫花列当提取物及其所含的苯乙醇苷类化合物均具有较好的抗氧化能力，其清除DPPH自由基能力接近于抗坏血酸。4采用卡介苗整体致敏、脂多糖离体攻击构建大鼠原代肝细胞免疫性损伤模型，在体外观察类叶升麻苷的保肝作用。

The molecular structures of these tuned phenanthroline derivatives with triphenylamine and oxadiazole groups and their europium complexes were characterized by element analysis and 1H NMR.

合成得到的功能化邻菲罗啉中性配体及其铕配合物的分子结构通过元素分析、核磁共振波谱进行了表征。

From 500℃ to 550℃, the oxide scale presents a relatively compact morphology, the oxidational wear is the principal wear mechanism and the wear rate is very slow at 500℃ owing to the anti-friction effect of the oxide scale.

本文研究了5CrNiMo在400℃、500℃、550℃及600℃温度下的滑动磨损行为，利用扫描电镜，波谱仪及X射线衍射仪对磨损面形貌及成分进行了分析，结果表明：5CrNiMo钢磨损机制随温度的变化而变化，400℃时表现为疲劳剥落和磨粒磨损，500℃至550℃时表现为氧化磨损，600℃时主要是粘着磨损。

Compounds were identified by means of physic-chemical property and spectral data including three new compounds: platyphyllin A (1), neochlorgeniclatone (2),(2E,6Z)-2,6-dimethyl-8-O-β-D-glucosyl-2,6-octadienoic acid (3). The known compounds included cyclic diarylheptanoids, phenylic acid, ect.

从白桦叶的水提取物中，利用各种色谱分离手段(硅胶柱色谱、聚酰胺柱色谱、凝胶柱色谱及制备薄层色谱等)，分离得到28个化合物，通过理化性质及各种波谱数据(NMR，MS，IR，etc)鉴定了23个化合物的结构，其中新化合物三个：platyphyllin A(1)，新绿原酸内酯(neochlorgeniclatone，2)，(2E，6Z)-2，6-二甲基-8-O--2，6-辛二烯酸(2E，6Z-2，6-dimethyl-8-O-β-D-glucosyl-2，6-octadienoic acid，3。

On the basis of spectroscopic analysis and comparison with the reported data, they were identified as kaempferol-3-O-β-D-glucoside, kaempferol 3-O-β-D-6-p-hydroxycoumaroylglucoside, L-2-O-methyl chiro-insitol and phillyrin.

叶的95%乙醇提取物中分离得到了4个化合物，经波谱分析，其结构分别鉴定为山萘酚－3-O-β-D-葡萄糖苷、山萘酚－3-β-D-（6-对羟基桂皮酰基）葡萄糖苷、L-2-O-甲基－手－肌醇和连翘苷。

Twenty-seven compounds were isolated from the methanol extract of the stems of Pinus massoniana by means of chromatographic methods, and their structures were elucidated as 8(14),15-Pimaradien-19-oic acid (1), Pimaric (2), Podocarpic acid (3), 12-Hydroxydehydroabietic acid (4), Dehydroabietic acid (5), 15-Hydroxydehydroabietic (6), 3β-Methoxyserrat-14-en-21-one (7), 3β-Hydroxy- serrat- 14-en-21-one (8), 3β-Methoxyserrat-14-en-21-one-30-al (9),(24R)-Stigmst- 4-ene-3-one (10),β-sitosterol (11),-3-Hydroxy-5-methoxy-stilbene(12), 4-Hydroxy-3- methoxycinnamaldehyde (13),-Ferulic acidtetracosyl ester (14), Alkylferulates (15), Pinocembin (16), Coniferaldehyde (17), Matairesinol (18),-Nortrachelogenin (19), Balanophonin (20), Cedrusin (21),-Pinoresinol (22), Tanegoside (23), 1,2-Bis-(4-hydroxy-3- methoxyphenyl)-propane-1,3-diol (24),(1S*, 2S*)-1-(4- Hydroxyphenyl) glyceri...

同时对马尾松枝条的甲醇提取物利用各种色谱技术进行了分离纯化，并利用现波谱技术鉴定了27个化合物的结构，分别为：8(14)，15-Pimaradien-19-oic acid (1)、海松酸(2)、罗汉松酸(3)、12-羟基脱氢松香酸(4)、脱氢松香酸(5)、15-羟基-脱氢松香酯(6)、3β-甲氧基-锯齿石松-14-烯-21-酮(7)、3β-Hydroxyserrat-14-en-21-one (8)、3β-Methoxyserrat-14-en-21– one-30-al (9)、(24R)-豆甾-4-烯-3-酮(10)、-3-羟基-5-甲氧基-二苯乙烯(12)、4-Hydroxy-3-methoxycinnamaldehyde (13)、-Ferulic acidtetracosyl ester (14)、Alkylferulates (15)、Pinocembin (16)、Coniferaldehyde (17)、罗汉松树脂酚(18)、 Balanophonin (20)、tanegoside (23)、1，2-Bis-(4-hydroxy- 3-methoxyphenyl)-propane- 1，3-diol (24)、(1S*，2S*)- 1-(4-hydroxyphenyl)glycerins (25)、(1R*，2R*)-1-(4-hydroxy- phenyl)gly-cerins (26)和赤松素(27)。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。