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沉淀剂

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In order to directly detect saccharides during the study on the interaction of glucose and its derivatives with lectins (e.g., concanavalin A), a capillary zone electrophoretic method with detection at a wavelength of 195 nm has been developed.

采用0.8 g/L偏磷酸与18%高氯酸的混合溶液作为生物样本中的蛋白沉淀剂及AA的提取剂,可大大提高AA在血浆中的稳定性。该方法已成功地应用于临床维生素C的常规检验。

The methods of using adsorbent and micropore membrane to decolor and to remove impurity were put forward.

提出了用吸附剂、微滤膜去色、除杂,用金属盐沉淀剂除去脑磷脂的新工艺,从而使产品中卵磷脂含量达到 85%以上。

The methods of using adsorbent and mi cropore membrane to decolor and to remove impurity were put forward.

提出了用吸附剂、微滤膜去色、除杂,用金属盐沉淀剂除去脑磷脂的新工艺,从而使产品中卵磷脂含量达到85%以上。

Melamine in eggs was extracted and the protein in samples was precipitated with acetronitrile, melamine was separated on a Luna SCX column (Luna 5u SCX 250×4.6mm) with monopotassium phosphate(MKP 0.05mol/L, pH=3.00), acetronitrile buffer solution (70:30, by volume) as the mobile phase at flow rate 1.50mL/min and the detection wavelength was 240nm, quantitative with external standard method.

采用乙腈作为样品中蛋白质的沉淀剂和三聚氰胺提取剂,流动相为0.05mol/L(pH=3.00)的磷酸二氢钾乙腈缓冲溶液,检测波长为240nm,流速为1.50mL/min,SCX(Luna 5u SCX250×4.6mm)色谱柱进行分离,HPLC-UV检测,外标法定量。

The invention relates to a fabric nanometer following cleaning agent for obtaining TiO2/ZnO composite hydrosol, and relative production and cleaning method, wherein it uses butyl titanate and zinc acetate as predecessor, uses glacial acetic acid as catalyst and peptizer, uses water as solvent, uses absolute ethyl alcohol as the solvent of butyl titanate, and uses ethanolamine as deposit agent and supplies OH-, to be hydrolysed and polycondensated to form TiO2/ZnO composite hydrosol. And its components and mass percents are: butyl titanate at 1-15%; zinc diethyl at 1-12%; absolute ethyl alcohol at 1-20%; glacial acetic acid at 5-15%; and aminoethyl alcohol at 0.1-5%, and the left is water. The invention has lower cost and simple process.

本发明涉及一种可以得到TiO 2 /ZnO复合水溶胶的纺织品纳米后整理试剂及其制备工艺及对织物的整理方法,以钛酸丁酯和乙酸锌为前驱物,冰乙酸为催化剂和胶溶剂,水为溶剂,无水乙醇为钛酸丁酯的溶剂,乙醇胺为沉淀剂并提供OH -,经过水解、缩聚反应形成的TiO 2 /ZnO纳米溶胶整理剂,其组分和重量百分比含量如下:钛酸丁酯占1~15%;二水乙酸锌占1~12%;无水乙醇占1%~20%;冰乙酸占5%~15%;乙醇胺占0.1%~5%;水余量,具有耐洗性、无毒、无刺激、成本低廉、制作工艺简单可靠的优点,可实现对对织物的抗紫外、抗菌、抗静电功能整理。

A new heat storage material (CH3COONa·3H2O) with a phase change temperature of 55℃ and a sub-cooling temperature of less than 2℃ was developed. This sodium acetate trihydrate based material was obtained by a number of experiments for selecting proper nucleation catalysts and suspension mediums.

以三水醋酸钠(CH3COONa·3H2O)为蓄热基质,通过大量实验,遴选合适的抗沉淀剂和成核剂,配成相变温度约55℃、过冷度小于2℃的蓄热材料。

The optimum conditions were as follows: 1 Fe3+/Fe2+ was 1.70-1.75;2 the precipitant,25% ammonia water was used 20%-30%,under 35℃,pH10-11 and with a stirrer speed of 3000 r/min for 1 h;3 in the first package process with gelatin and agar,the optimum amounts was 0.050-0.060g/150mL at the temperature of 55-60℃ and pH of 9-11;In the f...

最佳工艺条件为:(1)Fe3+/Fe2+之比在1.70~1.75;(2)沉淀剂25%NH3.H2O过量20%~30%,温度35℃,pH值11,反应时间为1h;(3)琼脂的最佳用量为0.050~0.060g/150mL;包覆的最佳温度为50~60℃,pH值为9~11;聚乙二醇作为第二次包裹剂时,最佳温度为55℃,反应时间是1h,pH值为4~5;并用透射电镜、分光光度计、古埃磁天平等进行了初步表征。

Indium Tin Oxide nano-powder was prepared with a convenient solvent thermal method. A hydroxide precursor was first prepared from indium chloride and tin chloride by using ammonia as precipitating agent.

以氯化铟和氯化锡为原料,氨水为沉淀剂,先用化学沉淀法制备了前驱体,然后将该前驱体以乙二醇为溶剂在聚四氟乙烯内衬的反应釜中于低至190 ℃下反应,获得了铟锡氧化物纳米粉体。

The pure and WO3-doped TiO2 nanoparticles photocatalyst was prepared by chemical precipitation, in which titanium tetrachloride was used as Ti-precursor, ammonia as precipitant and sodium tungstate as doping donor.

以TiCl4为钛前驱体,氨水为沉淀剂,钨酸钠为掺杂体给体,采用化学沉淀法,制备了纯的与WO3掺杂的TiO2纳米光催化剂。

GGG polycrystalline material was prepared by co-precipitation method with the metal Ga and Gd2O3 as the starting materials and aqueous ammonia as the preprecipitator.

采用共沉淀方法,以金属Ga和Gd2O3为起始原料,以氨水为沉淀剂,制备了GGG多晶。

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