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沉淀剂

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The preparation of ammonium uranyl gadolinium carbonate using (NH4)2CO3 solution from the mixed solution of UO2(NO3)2 and Gd(NO3)3 by means of co-precipitation was investigated.

本工作试验研究以碳酸铵溶液作沉淀剂从硝酸铀酰和硝酸钆的混合溶液中共沉淀AUGdC的方法。

In the process of evaporation, under the direction of phase diagram method, the main purpose is how to separate kinds of salt by-product, enrich Lithium, decrease the ratio of Mg/Li. The study shows that the Lithium can be concentrated to about 0.8%, the ratio of Mg/Li can be lowed to 10; In the process of precipitating, in order to separate the left Magnesium and Lithium, a lot of experiments were carried out with the Sodium carbonate or Calcium hydroxide and Sodium Sulfate anhydrate as precipitator of Magnesium, where the separation results were compared, and an optimal separation idea was proposed.

在蒸发阶段中,以相图分析为理论指导,着重研究了如何利用自然能源蒸发卤水,提取有用的镁盐和钾盐,并达到富集锂盐的目的,在此研究中,锂的浓度可富集到0.8%左右,镁锂比可降到10以下;在沉淀阶段中,分别研究了用纯碱、石灰乳和芒硝作为沉淀剂来分离镁锂,比较了分离效果、提出了最佳分离方案。

Using bischofite as raw materials, Na_2CO_3 as precipitant, basic magnesium carbonate was prepared by liquid deposition method through studying, the suitable process parameters were obtained.

盐湖提钾后的水氯镁石为原料,以Na_2CO_3作沉淀剂,采用化学方法中的液相沉淀法制备碱式碳酸镁。

Mg-Al oxide catalysts were prepared by co-precipitation method, used ammonia as the precipitating agent. The catalytic performances of these materials were investigated in the gas-phase Aldol condensation of acetone to isophorone. The structure and surface properties of the catalysts were characterized by means of XRD, XPS, ICP, TG-DTA and TPD.

采用共沉淀法,以氨水为沉淀剂制备了一系列具有不同Mg/Al摩尔比的镁铝氧化物催化剂,考察了它们在丙酮气相缩合反应中的催化性能,并通过XRD,XPS,ICP,TG-DTA和TPD等手段对催化剂的结构和性质进行了表征。

Neodymium doped lutetia nanocrystalline powders were synthesized by a wet chemical processing using three different precipitants, i.e . ammonium hydroxide (NH4OH), ammonium hydrogen carbonate (NH4HCO3) and the mixed solution of NH4OH+NH4HCO3, respectively.

采用湿化学共沉淀法合成了Nd3+掺杂的氧化镥纳米晶粉体,研究了三种不同沉淀剂(NH4OH、NH4HCO3、NH4OH+NH4HCO3)对Nd3+∶Lu2O3纳米晶粉体性能的影响。

Layered double hydroxides pillaring with organic anion s CoAl-LDH are directly synthesized by a homogeneous precipitation method using the urea as a precipitiant,and the LDH products have been characterized through XRD,FT-IR,TGA and TEM.

以尿素为沉淀剂用均匀沉淀法直接合成有机阴离子柱撑水滑石(LayeredDoubleHydroxides,LDH)及CoAl水滑石等,并用XRD,FT-IR,TGA,TEM等分析手段对所合成的水滑石进行了表征。

METHODS Pancreatin was extracted from autolyzed pancreas in the water, precipitated by precipitator P60 under the optimal conditions for 6 hours, and then dried at room temperature. The P60 in the solution was used in recycle.

胰脏自溶水提取,以一定浓度的蛋白质沉淀剂P60在最佳筛选条件下沉淀6h,室温干燥得胰酶粉,对上清液中的P60进行回收再利用。

A series of perovskite oxides are synthesized by means of blend deposition using the nitrate of A and B as the raw materials, and ammonia or sodium carbonateas sedimentation .A includes alkaline-earth metals such as Mg, Ca, Sr, Ba and rare-earth metalsLa; while B includes transition metal Cr, Mn, Fe, Co and Ni.

本文以A,B的硝酸盐为原料,以氨水或碳酸钠为沉淀剂,利用混合沉淀的方法合成了系列钙钛矿型氧化物。A选碱土金属元素Mg、Ca、Sr、Ba等及稀土金属元素La;B选过渡金属元素Cr、Mn、Fe、Co、Ni等。

A HPLC method for determination of sorbic acid,benzoic acid and sodium saccharin in dairy drink was studied.The comparison of five methods of precipitating protein showed that the solution of potassium ferrocyanide and zinc sulfate as protein's precipitant was appropriate.

探讨含乳饮料中山梨酸、苯甲酸、糖精钠的HPLC含量测定方法,在比较5种沉淀样品中蛋白质的方法后,确定以亚铁氰化钾与硫酸锌溶液为沉淀剂,采用C18反相柱,以甲醇:乙酸铵溶液(0.02 mol/L)=15∶85为流动相,紫外230 nm检测,结合保留时间及二极管阵列检测器光谱分析信息定性。

The results indicate that the adsorption isotherms are well-fitted by the Freundlich models, and the pH values and initial concentrations are the main influence factors.

结果表明,吸附沉淀剂对Cu(上标 2+)、Pb(上标 2+)的吸附平衡符合Freundlich方程,pH值和初始质量浓度对吸附沉淀量的影响最显著。

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